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公开(公告)号：US20120135210A1
公开(公告)日：2012-05-31
申请号：US13365313
申请日：2012-02-03
申请人： Christopher B. Walker, JR. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
发明人： Christopher B. Walker, JR. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/25 , Y10T428/254
摘要： Antireflective films are described having a surface layer comprising a the reaction product of a polymerizable low refractive index composition comprising at least one free-radically polymerizable fluoropolymer and surface modified inorganic nanoparticles. A high refractive index layer is coupled to the low refractive index layer. In one embodiment, the high refractive index layer comprises surface modified inorganic nanoparticles dispersed in a crosslinked organic material. The antireflective film is preferably durable, exhibiting a haze of less than 1.0% after 25 wipes with steel wool using a 3.2 cm mandrel and a mass of 1000 grams.
摘要翻译： 描述了具有包含包含至少一种可自由基聚合的含氟聚合物和表面改性的无机纳米颗粒的可聚合低折射率组合物的反应产物的表面层的抗反射膜。 高折射率层耦合到低折射率层。 在一个实施方案中，高折射率层包含分散在交联的有机材料中的表面改性的无机纳米颗粒。 抗反射膜优选耐用，在使用3.2cm心轴和质量为1000克的钢丝绒进行25次擦拭之后，其雾度小于1.0％。
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公开(公告)号：US08137801B2
公开(公告)日：2012-03-20
申请号：US12304505
申请日：2007-06-06
申请人： Christopher B. Walker, Jr. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
发明人： Christopher B. Walker, Jr. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/25 , Y10T428/254 , Y10T428/256 , Y10T428/265 , Y10T428/269 , Y10T428/3154 , Y10T428/31935
摘要： Antireflective films are described having a surface layer comprising a the reaction product of a polymerizable low refractive index composition comprising at least one fluorinated free-radically polymerizable material and surface modified inorganic nanoparticles. A high refractive index layer is coupled to the low refractive index layer. In one embodiment, the high refractive index layer comprises surface modified inorganic nanoparticles dispersed in a crosslinked organic material. The antireflective film is preferably durable, exhibiting a haze of less than 1.0% after 25 wipes with steel wool using a 3.2 cm mandrel and a mass of 1000 grams.
摘要翻译： 描述了具有表面层的抗反射膜，该表面层包含包含至少一种氟化可自由基聚合材料和表面改性无机纳米颗粒的可聚合低折射率组合物的反应产物。 高折射率层耦合到低折射率层。 在一个实施方案中，高折射率层包含分散在交联的有机材料中的表面改性的无机纳米颗粒。 抗反射膜优选耐用，在使用3.2cm心轴和质量为1000克的钢丝绒进行25次擦拭之后，其雾度小于1.0％。
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公开(公告)号：US20100232021A1
公开(公告)日：2010-09-16
申请号：US12304505
申请日：2007-06-06
申请人： Christopher B. Walker, JR. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
发明人： Christopher B. Walker, JR. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/25 , Y10T428/254 , Y10T428/256 , Y10T428/265 , Y10T428/269 , Y10T428/3154 , Y10T428/31935
摘要： Antireflective films are described having a surface layer comprising a the reaction product of a polymerizable low refractive index composition comprising at least one fluorinated free-radically polymerizable material and surface modified inorganic nanoparticles. A high refractive index layer is coupled to the low refractive index layer. In one embodiment, the high refractive index layer comprises surface modified inorganic nanoparticles dispersed in a crosslinked organic material. The antireflective film is preferably durable, exhibiting a haze of less than 1.0% after 25 wipes with steel wool using a 3.2 cm mandrel and a mass of 1000 grams.
摘要翻译： 描述了具有表面层的抗反射膜，该表面层包含包含至少一种氟化可自由基聚合材料和表面改性无机纳米颗粒的可聚合低折射率组合物的反应产物。 高折射率层耦合到低折射率层。 在一个实施方案中，高折射率层包含分散在交联的有机材料中的表面改性的无机纳米颗粒。 抗反射膜优选耐用，在使用3.2cm心轴和质量为1000克的钢丝绒进行25次擦拭之后，其雾度小于1.0％。
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公开(公告)号：US08343624B2
公开(公告)日：2013-01-01
申请号：US13365313
申请日：2012-02-03
申请人： Christopher B. Walker, Jr. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
发明人： Christopher B. Walker, Jr. , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/25 , Y10T428/254
摘要： Antireflective films are described having a surface layer comprising a the reaction product of a polymerizable low refractive index composition comprising at least one free-radically polymerizable fluoropolymer and surface modified inorganic nanoparticles. A high refractive index layer is coupled to the low refractive index layer. In one embodiment, the high refractive index layer comprises surface modified inorganic nanoparticles dispersed in a crosslinked organic material. The antireflective film is preferably durable, exhibiting a haze of less than 1.0% after 25 wipes with steel wool using a 3.2 cm mandrel and a mass of 1000 grams.
摘要翻译： 描述了具有包含包含至少一种可自由基聚合的含氟聚合物和表面改性的无机纳米颗粒的可聚合低折射率组合物的反应产物的表面层的抗反射膜。 高折射率层耦合到低折射率层。 在一个实施方案中，高折射率层包含分散在交联的有机材料中的表面改性的无机纳米颗粒。 抗反射膜优选耐用，在使用3.2cm心轴和质量为1000克的钢丝绒进行25次擦拭之后，其雾度小于1.0％。
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公开(公告)号：US20070286994A1
公开(公告)日：2007-12-13
申请号：US11427055
申请日：2006-06-28
申请人： Christopher B. Walker , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
发明人： Christopher B. Walker , Marc D. Radcliffe , Thomas P. Klun , Lan H. Liu , Richard J. Pokorny , William D. Coggio , Chuntao Cao , Mark J. Pellerite , Paul C. Kelley , Robert J. Fleming
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/25 , Y10T428/254 , Y10T428/256 , Y10T428/265 , Y10T428/269 , Y10T428/3154 , Y10T428/31935
摘要： Antireflective films are described having a surface layer comprising a the reaction product of a polymerizable low refractive index composition comprising at least one fluorinated free-radically polymerizable material and surface modified inorganic nanoparticles. A high refractive index layer is coupled to the low refractive index layer. In one emboidiment, the high refractive index layer comprises surface modified inorganic nanoparticles dispersed in a crosslinked organic material. The antireflective film is preferably durable, exhibiting a haze of less than 1.0% after 25 wipes with steel wool using a 3.2 cm mandrel and a mass of 1000 grams.
摘要翻译： 描述了具有表面层的抗反射膜，该表面层包含包含至少一种氟化可自由基聚合材料和表面改性无机纳米颗粒的可聚合低折射率组合物的反应产物。 高折射率层耦合到低折射率层。 在一个实施例中，高折射率层包含分散在交联的有机材料中的表面改性的无机纳米颗粒。 抗反射膜优选耐用，在使用3.2cm心轴和质量为1000克的钢丝绒进行25次擦拭之后，其雾度小于1.0％。
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6.发明授权Low refractive index fluoropolymer coating compositions for use in antireflective polymer films 有权用于抗反射聚合物膜的低折射率含氟聚合物涂料组合物公开(公告)号：US07323514B2
公开(公告)日：2008-01-29
申请号：US11026640
申请日：2004-12-30
申请人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , William D. Coggio , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
发明人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , William D. Coggio , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
IPC分类号： C08F259/00
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/3154 , Y10T428/31663
摘要： An economic, optically transmissive, stain and ink repellent, durable low refractive index fluoropolymer composition for use in an antireflection film or coupled to an optical display. In one aspect of the invention, the composition is formed from the reaction product of a fluoropolymer or reactive fluoropolymer, an amino silane ester coupling agent or ester equivalent, a multi-olefinic crosslinker, and optional surface modified inorganic particles or sol gel precursors.
摘要翻译： 用于抗反射膜或耦合到光学显示器的经济，光学透射，防污和防油墨，耐用的低折射率含氟聚合物组合物。 在本发明的一个方面，组合物由含氟聚合物或反应性含氟聚合物，氨基硅烷酯偶联剂或酯当量的反应产物，多烯属交联剂和任选的表面改性的无机颗粒或溶胶凝胶前体形成。
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7.发明授权Low refractive index fluoropolymer compositions having improved coating and durability properties 有权具有改进的涂层和耐久性的低折射率含氟聚合物组合物公开(公告)号：US07473462B2
公开(公告)日：2009-01-06
申请号：US11972034
申请日：2008-01-10
申请人： William D. Coggio , Thomas P. Klun , George G. I. Moore , Naiyong Jing , Chuntao Cao , Sharon Wang , Patricia M. Savu , Lan H. Liu , Joan M. Noyola
发明人： William D. Coggio , Thomas P. Klun , George G. I. Moore , Naiyong Jing , Chuntao Cao , Sharon Wang , Patricia M. Savu , Lan H. Liu , Joan M. Noyola
CPC分类号： C08F14/18 , C08F259/08 , C08F283/00 , C08L51/003 , C09D151/003 , G02B1/111 , Y10T428/24942 , Y10T428/259 , Y10T428/3154 , Y10T428/31544 , Y10T428/31935 , C08F2/00 , C08L2666/02
摘要： A low refractive index composition that forms a low refractive index layer on an optical display is formed having a co-crosslinked interpenetrating polymer network of a fluoropolymer phase and an acrylate phase. The fluoropolymer phase is preferably formed from fluoropolymers based on THV or FKM and having either a degree of unsaturation and/or containing a reactive cure site monomer in its polymer backbone. The acrylate phase includes a multifunctional acrylate crosslinker, and more preferably includes a perfluoropolyether acrylate crosslinker. The formed low refractive index layer has improved interfacial adhesion to other layers or substrates contained in the optical display. Further, the mechanical strength and scratch resistance of the either of above low refractive index compositions can be further enhanced through the incorporation of surface functionalized inorganic particle into the formed layer.
摘要翻译： 形成在光学显示器上形成低折射率层的低折射率组合物，其具有含氟聚合物相和丙烯酸酯相的共交联互穿聚合物网络。 含氟聚合物相优选由基于THV或FKM的含氟聚合物形成，并且在其聚合物主链中具有不饱和度和/或含有反应性固化位点单体。 丙烯酸酯相包括多官能丙烯酸酯交联剂，更优选包括全氟聚醚丙烯酸酯交联剂。 所形成的低折射率层具有改善的与光学显示器中包含的其它层或基底的界面粘合性。 此外，通过将表面官能化的无机颗粒并入成形层，可以进一步提高上述低折射率组合物中的任一种的机械强度和耐划伤性。
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公开(公告)号：US07638581B2
公开(公告)日：2009-12-29
申请号：US11305978
申请日：2005-12-19
申请人： Naiyong Jing , Tatsuo Fukushi , Chuntao Cao , Lan H. Liu , Thomas P. Klun , William D. Coggio , Vivian W. Jones
发明人： Naiyong Jing , Tatsuo Fukushi , Chuntao Cao , Lan H. Liu , Thomas P. Klun , William D. Coggio , Vivian W. Jones
IPC分类号： C08L27/12
CPC分类号： C08J3/005 , C08J7/047 , C08J2327/12 , C08J2427/00 , C08L27/12 , C08L27/16 , C08L27/18 , C08L2205/02 , C09D127/12 , C09D127/16 , C09D127/18 , C08L2666/04
摘要： A fluoropolymer coating composition contains a homogeneous mixture of crystalline submicron fluoropolymer particles dispersed in a solvent-borne solution of less crystalline or amorphous fluororesin. The composition may be prepared by blending a latex containing crystalline submicron fluoropolymer particles with a latex containing less crystalline or amorphous fluororesin particles, coagulating and drying the blended latices, and dissolving the dried blend in a solvent for the fluororesin particles. Quasi-homogenous compositions may be prepared by blending dry crystalline submicron fluoropolymer particles with a) dry less crystalline or amorphous fluororesin particles and a solvent for the fluororesin particles, or b) a solvent-borne solution of less crystalline or amorphous fluororesin. Rubbing the disclosed coatings can provide a thin, continuous or nearly continuous fluoropolymer surface layer atop a less crystalline or amorphous fluororesin binder containing crystalline submicron fluoropolymer particles.
摘要翻译： 氟聚合物涂料组合物含有分散在不太结晶或无定形氟树脂的溶剂型溶液中的结晶亚微米含氟聚合物颗粒的均匀混合物。 该组合物可以通过将含有结晶亚微米含氟聚合物颗粒的胶乳与含有较少结晶或无定形氟树脂颗粒的胶乳混合来制备，将混合的胶乳凝结并干燥，并将干燥的共混物溶解在氟树脂颗粒的溶剂中。 准均匀组合物可以通过将干结晶亚微米含氟聚合物颗粒与a）干结晶或无定形氟树脂颗粒和用于氟树脂颗粒的溶剂混合来制备，或b）不太结晶或无定形氟树脂的溶剂型溶液。 摩擦所公开的涂层可以在含有结晶亚微米含氟聚合物颗粒的较少结晶或无定形氟树脂粘合剂的顶部提供薄的，连续的或几乎连续的含氟聚合物表面层。
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公开(公告)号：US20070286992A1
公开(公告)日：2007-12-13
申请号：US11423782
申请日：2006-06-13
申请人： William D. Coggio , Thomas P. Klun , Chuntao Cao
发明人： William D. Coggio , Thomas P. Klun , Chuntao Cao
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/25 , Y10T428/259 , Y10T428/31551 , Y10T428/31935
摘要： Antireflective films and low refractive index compositions are described. The low refractive index layer comprises the reaction product of a composition comprising at least one free-radically polymerizable material having a high fluorine content, and at least one free-radically polymerizable fluoropolyether urethane material.
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10.发明授权Fluoropolymer coating compositions with multifunctional fluoroalkyl crosslinkers for anti-reflective polymer films 失效具有用于抗反射聚合物膜的多功能氟代烷基交联剂的含氟聚合物涂料组合物公开(公告)号：US07351471B2
公开(公告)日：2008-04-01
申请号：US11026754
申请日：2004-12-30
申请人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
发明人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
CPC分类号： G02B1/111 , A63B37/0004 , Y10T428/269
摘要： An economic, optically transmissive, stain and ink repellent, durable low refractive index fluoropolymer composition for use in an antireflection film or coupled to an optical display. In one aspect of the invention, the composition is formed from the reaction product of a fluoropolymer and a fluoroalkyl containing multi-olefinic crosslinker. In another aspect of the invention, the composition further includes surface modified inorganic nanoparticles.
摘要翻译： 用于抗反射膜或耦合到光学显示器的经济，光学透射，防污和防油墨，耐用的低折射率含氟聚合物组合物。 在本发明的一个方面，组合物是由含氟聚合物和含氟烷基的多烯烃交联剂的反应产物形成的。 在本发明的另一方面，组合物还包括表面改性的无机纳米颗粒。
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