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    QUATERNIZED COPOLYMER
    2.
    发明申请
    QUATERNIZED COPOLYMER 有权
    季铵化共聚物

    公开(公告)号：US20110315107A1

    公开(公告)日：2011-12-29

    申请号：US13168405

    申请日：2011-06-24

    申请人： Wolfgang Grabarse ,  Hannah Maria König ,  Christian Tock ,  Cornelia Röger-Göpfert ,  Ludwig Völkel ,  Harald Böhnke

    发明人： Wolfgang Grabarse ,  Hannah Maria König ,  Christian Tock ,  Cornelia Röger-Göpfert ,  Ludwig Völkel ,  Harald Böhnke

    IPC分类号： C08F222/06 ,  C08F8/32 ,  F02B43/00

    CPC分类号： C08F222/06 ,  C08F8/44 ,  C10L1/2364 ,  C10L1/2366 ,  C10L10/04 ,  C10L10/08 ,  C10L10/18 ,  C08F220/14 ,  C08F8/32 ,  C08F8/14

    摘要： A quaternized copolymer obtainable by: (A) copolymerization of straight-chain, branched or cyclic, ethylenically unsaturated C2 to C100 hydrocarbons, which may bear oxygen- or nitrogen-functional substituents which cannot be reacted with amines to give amides or imides or with alcohols to give esters, with ethylenically unsaturated C3- to C12-mono- or dicarboxylic acids or acid derivatives, which can be reacted with amines to give amides or imides or with alcohols to give esters, to give a copolymer with a number-average molecular weight of 500 to 20 000; (B) partial or full amidation or imidation or esterification of the carboxylic acid functions by reacting them with oligoamines having 2 to 6 nitrogen atoms or alcoholamines, each of which comprises primary or secondary nitrogen atom or a hydroxyl group and a quaternizable tertiary nitrogen atom; (C) partial or full quaternization of the tertiary nitrogen atom with a quaternizing agent. The quaternized copolymer thus prepared is suitable as a fuel additive in direct-injection diesel engines.

    摘要翻译： 可通过以下方法获得的季铵化共聚物：（A）直链，支链或环状的烯属不饱和C2至C100烃的共聚，其可承载不能与胺反应得到酰胺或酰亚胺或与醇反应的氧或氮官能取代基 得到具有烯键式不饱和C 3 -C 12 - 单 - 或二羧酸或酸衍生物的酯，其可以与胺反应得到酰胺或酰亚胺或与醇反应得到酯，得到具有数均分子量的共聚物 500至20,000; （B）通过使羧酸官能团与具有2-6个氮原子的低聚胺或醇胺进行部分或完全酰化或酰化或酯化，其各自包含伯或仲氮原子或羟基和可季铵化的叔氮原子; （C）叔氮原子与季铵化剂部分或全部季铵化。 如此制备的季铵化共聚物适合作为直接喷射柴油发动机中的燃料添加剂。

    Preparation of derivatives of isobutene copolymers
    6.
    发明授权
    Preparation of derivatives of isobutene copolymers 有权
    异丁烯共聚物衍生物的制备

    公开(公告)号：US09562117B2

    公开(公告)日：2017-02-07

    申请号：US13305132

    申请日：2011-11-28

    申请人： Hannah Maria König ,  Klaus Mühlbach ,  Helmut Mach ,  Ulrich Eichenauer

    发明人： Hannah Maria König ,  Klaus Mühlbach ,  Helmut Mach ,  Ulrich Eichenauer

    IPC分类号： C08F10/10 ,  C08F8/32 ,  C08F8/46 ,  C08F8/30 ,  C08F8/14 ,  C08F290/04 ,  C08F8/42

    CPC分类号： C08F8/30 ,  C08F8/14 ,  C08F8/32 ,  C08F8/42 ,  C08F10/10 ,  C08F290/042 ,  C08F210/12

    摘要： A process for producing an isobutene copolymer derivative by: (I) free-radically copolymerizing (a) 10-90 mol % of a monoethylenically unsaturated C4- to C12-dicarboxylic acid, anhydride, or ester, (b) 10-90 mol % of a high-reactivity isobutene polymer having Mn=110-250000 and obtained by polymerizing isobutene in the presence of an iron-halide-, aluminum trihalide-, or alkylaluminum halide-donor complex, each donor being an ether or carboxylic ester function, or in the presence of a Lewis acid complex containing an organic sulfonic acid, and (c) 0-50 mol % of a monoethylenically unsaturated compound copolymerizable with (a) and (b), to obtain an intermediate isobutene copolymer; and (II) reacting the carboxylic acid functions in the intermediate with at least one of ammonia, an amine, and an alcohol, to form a moiety containing at least one of a hydroxyl, carboxylic ester, amino, quaternized amino, amido, and imido group.

    摘要翻译： 异丁烯共聚物衍生物的制备方法：（I）10-90摩尔％的单烯属不饱和C4-至C12-二羧酸，酸酐或酯的自由基共聚合，（b）10-90摩尔％ 的Mn = 110-250000的高反应异丁烯聚合物，并且通过在卤化铁，三卤化铝或卤化烷基铝卤化物供体络合物的存在下聚合异丁烯获得，每个供体是醚或羧酸酯官能团，或 在含有有机磺酸的路易斯酸络合物的存在下，和（c）0-50mol％可与（a）和（b）共聚的单烯键式不饱和化合物，得到中间体异丁烯共聚物; 和（II）使中间体中的羧酸官能团与氨，胺和醇中的至少一种反应，以形成含有羟基，羧酸酯，氨基，季铵化氨基，酰胺基和亚氨基中的至少一个的部分 组。

    Method for the production of composite materials
    7.
    发明授权
    Method for the production of composite materials 有权
    复合材料生产方法

    公开(公告)号：US09234098B2

    公开(公告)日：2016-01-12

    申请号：US13262755

    申请日：2010-04-01

    申请人： Hannah Maria König ,  Hans-Joachim Hähnle ,  Arno Lange ,  Samira Nozari ,  Gerhard Cox ,  Rainer Dyllick-Brenzinger ,  Stefan Spange ,  Tina Löschner

    发明人： Hannah Maria König ,  Hans-Joachim Hähnle ,  Arno Lange ,  Samira Nozari ,  Gerhard Cox ,  Rainer Dyllick-Brenzinger ,  Stefan Spange ,  Tina Löschner

    IPC分类号： B82Y30/00 ,  C08L83/02 ,  C08J5/00 ,  H01B1/04 ,  C08K3/36

    CPC分类号： C08L83/02 ,  B82Y30/00 ,  C08J5/005 ,  C08K3/36

    摘要： The present invention relates to a process for producing a nanocomposite material from a) at least one inorganic or organometallic metal phase; and b) an organic polymer phase; comprising the polymerization of at least one monomer M which have at least one first polymerizable monomer unit A which has a metal or semimetal M, and at least one second polymerizable organic monomer unit B which is joined to the polymerizable unit A via a covalent chemical bond, under polymerization conditions under which both the polymerizable monomer unit A and the polymerizable unit B polymerize with breakage of the bond between A and B, the monomers M to be polymerized comprising a first monomer M1 and at least one second monomer M2 which differs at least in one of the monomer units A and B from the monomer M1 (embodiment 1), or the monomers to be polymerized comprising, as well as the at least one monomer M, at least one further monomer other than the monomers M, i.e. a conventional monomer which does not have a monomer unit A and is copolymerizable with the monomer unit B (embodiment 2).

    摘要翻译： 本发明涉及从a）至少一种无机或有机金属金属相制备纳米复合材料的方法; 和b）有机聚合物相; 包括至少一种单体M的聚合，所述单体M具有至少一个具有金属或半金属M的第一可聚合单体单元A和至少一个第二可聚合有机单体单元B，其通过共价化学键连接到可聚合单元A 在可聚合单体单元A和可聚合单元B两者都聚合并且A和B之间的键断裂聚合的聚合条件下，待聚合的单体M包含第一单体M1和至少一个第二单体M2，其至少不同 在单体M1（实施方案1）的单体单元A和B中的一种中，或要聚合的单体以及至少一种单体M至少一种除单体M以外的其它单体，即常规 不具有单体单元A并且可与单体单元B共聚的单体（实施方案2）。

    PREPARATION OF ISOBUTENE HOMO- OR COPOLYMER DERIVATIVES
    8.
    发明申请
    PREPARATION OF ISOBUTENE HOMO- OR COPOLYMER DERIVATIVES 有权
    ISOBUTENE共聚物衍生物的制备

    公开(公告)号：US20120142868A1

    公开(公告)日：2012-06-07

    申请号：US13305283

    申请日：2011-11-28

    申请人： Hannah Maria König ,  Klaus Mühlbach ,  Helmut Mach ,  Ulrich Eichenauer

    发明人： Hannah Maria König ,  Klaus Mühlbach ,  Helmut Mach ,  Ulrich Eichenauer

    IPC分类号： C08F10/10 ,  C08F8/32 ,  C08F8/00 ,  C08F8/28 ,  C08F8/08 ,  C08F8/34 ,  C08F8/42

    CPC分类号： C08F4/14 ,  C08F4/26 ,  C08F8/00 ,  C08F8/30 ,  C08F8/32 ,  C08F8/34 ,  C08F8/46 ,  C08F10/10 ,  C08F110/10 ,  C08F210/10 ,  C08F4/12 ,  C08F210/08

    摘要： A process for preparing isobutene homo- or copolymer derivatives by (i) polymerizing isobutene or an isobutene-comprising monomer mixture in the presence of an iron halide-donor complex, an aluminum trihalide-donor complex, or an alkylaluminum halide-donor complex, (ii) reacting a resulting high-reactivity isobutene polymer with a compound which introduces a low molecular weight polar group or a substructure thereof, and (iii) in the case of reaction with a substructure, further reacting to complete the formation of the low molecular weight polar group. The homo- or copolymer derivatives include a radical of a hydrophobic polyisobutene polymer having a number-average molecular weight of 110 to 250 000 and low molecular weight polar groups including amino functions, nitro groups, hydroxyl groups, mercaptan groups, carboxylic acid or carboxylic acid derivative functions, sulfonic acid or sulfonic acid derivative functions, aldehyde functions and/or silyl groups.

    摘要翻译： （i）在卤化铁 - 给体络合物，三卤化铝 - 供体络合物或烷基铝卤化物 - 供体络合物存在下聚合异丁烯或含异丁烯的单体混合物来制备异丁烯均聚物或共聚物衍生物的方法（ ii）使所得高反应性异丁烯聚合物与引入低分子量极性基团或其下结构的化合物反应，和（iii）在与亚结构反应的情况下，进一步反应以完成低分子量的形成 极地组。 均聚物或共聚物衍生物包括数均分子量为110至250,000的疏水聚异丁烯聚合物基团和包括氨基官能团的低分子量极性基团，硝基，羟基，硫醇基，羧酸或羧酸 衍生功能，磺酸或磺酸衍生物功能，醛官能团和/或甲硅烷基。