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    Water-absorbing, cellular, cross-linked polymers with improved distribution effect, method for their production and their use
    3.
    发明授权
    Water-absorbing, cellular, cross-linked polymers with improved distribution effect, method for their production and their use 失效
    吸水，细胞，交联聚合物具有改善的分布效果，其制备方法及其用途

    公开(公告)号：US06750262B1

    公开(公告)日：2004-06-15

    申请号：US09926110

    申请日：2001-09-04

    申请人： Hans-Joachim Hähnle ,  Ulrich Schröder ,  Wolfgang Heider ,  Gunnar Schornick ,  Thomas Anstock

    发明人： Hans-Joachim Hähnle ,  Ulrich Schröder ,  Wolfgang Heider ,  Gunnar Schornick ,  Thomas Anstock

    IPC分类号： C08J928

    CPC分类号： C08J9/30 ,  A61L15/24 ,  A61L15/425 ,  A61L15/60 ,  B01J20/26 ,  C08J9/122 ,  C08J2207/12 ,  C08J2300/10 ,  C09K3/10 ,  C09K17/20 ,  C09K2003/1046 ,  C09K2200/0625 ,  C09K2200/0657 ,  C08L33/00

    摘要： Water-absorbing, expanded, crosslinked polymers obtainable by (I) foaming a polymerizable aqueous mixture which comprises (a) monoethylenically unsaturated monomers which contain acidic groups and are optionally neutralized, (b) optionally other monoethylenically unsaturated monomers, (c) crosslinkers, (d) initiators, (e) 0.1-20% by weight of at least one surfactant, (f) optionally at least one solubilizer and (g) optionally thickeners, foam stabilizers, polymerization regulators, fillers and/or cell nucleating agents, where the foaming takes place by dissolving a gas which is inert to free radicals under a pressure of 2-400 bar in the polymerizable aqueous mixture, and then decompressing the latter to atmospheric pressure, and (II) polymerizing the foamed mixture to form an expanded hydrogel and, where appropriate, adjusting the water content of the expanded polymer to 1-60% by weight, process for preparing the water-absorbing, expanded, crosslinked polymers and use of these polymers in sanitary articles employed for absorbing body fluids, in dressing material for covering wounds, as sealing material, as soil improver, as soil substitute and as packaging material.

    摘要翻译： （I）发泡可聚合水性混合物的吸水膨胀交联聚合物，其包含（a）含有酸性基团并任选中和的单烯属不饱和单体，（b）任选其它单烯属不饱和单体，（c）交联剂， d）引发剂，（e）0.1-20重量％的至少一种表面活性剂，（f）任选的至少一种增溶剂和（g）任选的增稠剂泡沫稳定剂，聚合调节剂，填料和/或细胞成核剂，其中 通过将在2-400巴的压力下对自由基惰性的气体溶解在可聚合的含水混合物中，然后将其减压至大气压来进行发泡，和（II）使发泡混合物聚合以形成膨胀的水凝胶， 在适当的情况下，将发泡聚合物的水含量调节至1-60重量％，制备吸水膨胀交联聚合物的方法，以及在sanitar中使用这些聚合物 用于吸收体液的物品，用于覆盖伤口的敷料材料，作为密封材料，作为土壤改良剂，作为土壤代用品和作为包装材料。

    Water-absorbing, cross-linked polymerizates in the form of a foam, a method for the production thereof, and their use
    4.
    发明授权
    Water-absorbing, cross-linked polymerizates in the form of a foam, a method for the production thereof, and their use 有权
    泡沫形式的吸水交联聚合物，其制备方法及其应用

    公开(公告)号：US06455600B1

    公开(公告)日：2002-09-24

    申请号：US09623590

    申请日：2000-09-05

    申请人： Hans-Joachim Hähnle ,  Ulrich Schröder ,  Martin Beck ,  Wolfgang Heider ,  Gunnar Schornick ,  Thomas Anstock

    发明人： Hans-Joachim Hähnle ,  Ulrich Schröder ,  Martin Beck ,  Wolfgang Heider ,  Gunnar Schornick ,  Thomas Anstock

    IPC分类号： C08J928

    CPC分类号： C08J9/30 ,  A61L15/425 ,  A61L15/60 ,  C08J2300/14

    摘要： A water-absorbing, expanded, crosslinked polymer obtainable by (I) foaming a polymerizable aqueous mixture which comprises (a) monoethylenically unsaturated monomers which contain acidic groups and are optionally neutralized, (b) optionally other monoethylenically unsaturated monomers, (c) crosslinkers, (d) initiators, (e) 0.1-20% by weight of at least one surfactant, (f) optionally at least one solubilizer and (g) optionally thickeners, foam stabilizers, polymerization regulators, fillers and/or cell nucleating agents,  where the foaming takes place by dispersing fine bubbles of a gas which is inert to free radicals in the polymerizable aqueous mixture, and (II) polymerizing the foamed mixture to form an expanded hydrogel, whereby at least 20 mol % of the monomers (a) which contain acidic groups have been neutralized with tertiary alkanolamines and/or the free acidic groups of the expanded hydrogel have been at least 20 mol % neutralized with at least one alkalolamine after the polymerization, and, where appropriate, adjusting the water content of the expanded polymer to 1-60% by weight, the production thereof and the use thereof in hygiene articles employed to absorb body fluids and in dressing material for covering wounds.

    摘要翻译： （I）发泡可聚合水性混合物的吸水膨胀交联聚合物，其包含（a）含有酸性基团并任选中和的单烯属不饱和单体，（b）任选的其它单烯属不饱和单体，（c）交联剂， （d）引发剂，（e）0.1-20重量％的至少一种表面活性剂，（f）任选的至少一种增溶剂和（g）任选的增稠剂泡沫稳定剂，聚合调节剂，填料和/或细胞成核剂，其中 通过将可自由基惰性的气体的细小气泡分散在可聚合的含水混合物中，并且（II）使发泡混合物聚合以形成膨胀的水凝胶，从而将至少20mol％的单体（a） 含有酸性基团已经被叔链烷醇胺中和，和/或膨胀的水凝胶的游离酸性基团在聚合后与至少一种烷醇胺中至少20摩尔％ 并且在适当的情况下，将发泡聚合物的含水量调节至1-60重量％，其生产以及用于吸收体液的卫生制品和用于覆盖伤口的敷料中的用途。

    Method and device for determining the swelling behavior of polymer gels under pressure
    6.
    发明授权
    Method and device for determining the swelling behavior of polymer gels under pressure 失效
    用于测定聚合物凝胶在压力下的溶胀行为的方法和装置

    公开(公告)号：US07189575B2

    公开(公告)日：2007-03-13

    申请号：US10399492

    申请日：2001-11-08

    申请人： Wolfgang Schrof ,  Udo Gödert ,  Martin Beck ,  Hans-Joachim Hähnle ,  Gunnar Schornick

    发明人： Wolfgang Schrof ,  Udo Gödert ,  Martin Beck ,  Hans-Joachim Hähnle ,  Gunnar Schornick

    IPC分类号： B01J20/00 ,  A61F13/15 ,  C12Q1/68 ,  G01N15/06 ,  G01N7/00

    CPC分类号： G01N19/10

    摘要： Disclosed is a method for determining the swellability and the swelling kinetics of superabsorbent material (9) such as polymer gels, for example, which comprises introducing a defined volume of the dry superabsorbent material (9) into a measuring vessel (7), using a movable element (4) within said measuring vessel (7) to apply a restraining force (12) to said superabsorbent material (9) and capturing the expansion of said superabsorbent material (9) contactlessly within a chamber (14) in a continuous manner by capturing the change in height of a piston (4) which bounds said chamber (14), travels in a measuring vessel (7) and is marked with a height scale (6).

    摘要翻译： 公开了一种用于测定超吸收材料（9）如聚合物凝胶的溶胀性和溶胀动力学的方法，例如，其包括将限定体积的干燥超吸收材料（9）引入测量容器（7）中，使用 在所述测量容器（7）内的可移动元件（4），以将约束力（12）施加到所述超吸收材料（9），并以连续方式以不间断的方式捕获所述超吸收材料（9）在腔室（14）内的膨胀 捕获限定所述室（14）的活塞（4）的高度变化，在测量容器（7）中行进并用高度刻度（6）标记。

    Foams made from water-absorbing, basic polymers, method for the production and utilization thereof
    7.
    发明授权
    Foams made from water-absorbing, basic polymers, method for the production and utilization thereof 有权
    由吸水性碱性聚合物制成的泡沫体，其生产和利用方法

    公开(公告)号：US07838567B2

    公开(公告)日：2010-11-23

    申请号：US10502212

    申请日：2003-01-30

    申请人： Samantha Champ ,  Hans-Joachim Hähnle ,  Martin Beck ,  Rüdiger Funk

    发明人： Samantha Champ ,  Hans-Joachim Hähnle ,  Martin Beck ,  Rüdiger Funk

    IPC分类号： C08J9/12

    CPC分类号： C08J9/30 ,  C08J9/286 ,  C08J2201/0504 ,  C08J2205/022 ,  C08J2300/14

    摘要： Foams composed of water-absorbing basic polymers, obtainable by (I) foaming a crosslinkable aqueous mixture including (a) at least one basic polymer whose basic groups have optionally been neutralized, (b) at least one crosslinker, (c) at least one surfactant, (d) optionally at least one solubilizer, (e) optionally thickeners, foam stabilizers, fillers, fibers and/or cell nucleators, and (f) optionally particulate water-absorbing acidic polymers, by dissolving a gas which is inert toward free radicals in the crosslinkable aqueous mixture under a pressure from 2 to 400 bar and subsequently decompressing the crosslinkable aqueous mixture to atmospheric or by dispersing fine bubbles of a gas which is inert toward free radicals, and (II) crosslinking the foamed mixture to form a hydrogel foam and if applicable adjusting the water content of the polymer foam to 1-60% by weight. Preparation of the foams by application of the abovementioned measures (I) and (II) and use of the thus obtainable foams in hygiene articles to absorb body fluids, in dressing material to cover wounds, as a sealing material, as a packaging material, as a soil improver, as a soil substitute, to dewater sludges, to absorb aqueous acidic wastes, to thicken waterborne paints or coatings in the course of disposing of residual quantities thereof, to dewater water-containing oils or hydrocarbons or as a material for filters in ventilation systems.

    摘要翻译： 由吸水性碱性聚合物组成的泡沫体可通过（I）发泡可交联水性混合物得到，所述可交联水性混合物包括（a）至少一种碱性基团任选被中和的碱性聚合物，（b）至少一种交联剂，（c）至少一种 表面活性剂，（d）任选的至少一种增溶剂，（e）任选的增稠剂，泡沫稳定剂，填料，纤维和/或细胞成核剂，和（f）任选的颗粒状吸水性酸性聚合物， 在2至400巴的压力下在可交联水性混合物中的基团，随后将可交联的含水混合物减压至大气或通过分散对自由基呈惰性的气体的细小气泡，和（II）将发泡混合物交联以形成水凝胶 泡沫，如果适用，将聚合物泡沫的含水量调节至1-60重量％。 通过应用上述措施（I）和（II）制备泡沫体，并将如此获得的泡沫在卫生制品中的使用以吸收体液，在敷料中覆盖伤口作为密封材料作为包装材料，如 土壤改良剂，作为土壤替代物，去除污泥，吸收含水酸性废物，在处理剩余量的过程中加厚水性涂料或涂料，将含水油或碳氢化合物或用作过滤器的材料脱水 通风系统。

    Hydrophilic, open-cell, elastic foams with a melamine/formaldehyde resin base, production thereof and use thereof in hygiene products
    9.
    发明授权
    Hydrophilic, open-cell, elastic foams with a melamine/formaldehyde resin base, production thereof and use thereof in hygiene products 失效
    具有三聚氰胺甲醛树脂基质的亲水，开孔，弹性泡沫，其生产及其在卫生产品中的用途

    公开(公告)号：US06800666B2

    公开(公告)日：2004-10-05

    申请号：US10380457

    申请日：2003-03-10

    申请人： Hans-Joachim Hähnle ,  Horst Baumgartl ,  Martin Beck ,  Norbert Herfert ,  Bernhard Mohr ,  Jürgen Huff

    发明人： Hans-Joachim Hähnle ,  Horst Baumgartl ,  Martin Beck ,  Norbert Herfert ,  Bernhard Mohr ,  Jürgen Huff

    IPC分类号： C08J9224

    CPC分类号： C08J9/141 ,  A61L15/26 ,  A61L15/42 ,  A61L15/425 ,  C08J9/36 ,  C08J2205/05 ,  C08J2205/06 ,  C08J2361/28 ,  C08L61/28

    摘要： Hydrophilic open-celled resilient foams containing melamine-formaldehyde resins, characterized by a droplet absorption rate of less than 5 seconds and an EU standard EN ISO 14184-1 formaldehyde emission of less than 100 mg of formaldehyde/kg of foam, and obtainable by (a) heating an aqueous solution or dispersion each containing at least a melamine-formaldehyde precondensate, an emulsifier, a blowing agent and a curing agent to form a foam and crosslink the precondensate, (b) then conditioning the foam at from 120 to 300° C. for from 1 to 180 minutes to remove volatiles, and (c) treating the foam during the conditioning or thereafter with at least one hydrophilicizer and/or with ozone, a corona discharge or a plasma, are useful in hygiene articles to acquire, distribute and immobilize body fluids.

    摘要翻译： 含有三聚氰胺 - 甲醛树脂的亲水性开孔弹性泡沫，其特征在于小于5秒的液滴吸收速率和小于100mg甲醛/ kg泡沫的欧盟标准EN ISO 14184-1甲醛排放，并且可由（ a）加热至少含有三聚氰胺 - 甲醛预缩合物，乳化剂，发泡剂和固化剂的水溶液或分散体，以形成泡沫并交联预缩合物，（b）然后将泡沫调节至120至300℃ （c）在调理期间或之后用至少一种亲水剂和/或用臭氧，电晕放电或等离子体处理泡沫，可用于卫生制品中以获得， 分散和固定体液。