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1.发明申请Particulate water absorbing agent with water-absorbing resin as main component 审中-公开颗粒吸水剂以吸水树脂为主要成分公开(公告)号：US20070066167A1
公开(公告)日：2007-03-22
申请号：US10570965
申请日：2005-03-29
IPC分类号： B32B5/02
CPC分类号： C08J3/12 , C08J3/245 , C08J2300/14 , Y10T428/249924 , Y10T428/254 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998 , Y10T442/2344
摘要： The present invention provides a water absorbing agent which maintains excellent water absorbing properties for a long time, even when urine composition of human urine varies depending. A particulate water absorbing agent comprising a water-absorbing resin obtained by crosslinking polymerization of an unsaturated monomer, which exhibits Centrifuge retention capacity in a physiological saline solution of not lower than 32 g/g, mass median particle size (D50) of 200 to 400 μm, ratio of particles with diameter of smaller than 150 μm of 0 to 2% by weight, and increased extractables by deterioration of 0 to 15% by weight and extractables for one hour in deterioration test liquid of 0.1 to 30% by weight.
摘要翻译： 本发明提供一种长时间保持优异的吸水性的吸水剂，即使在尿液的尿组成变化的情况下也是如此。 一种颗粒状吸水剂，其特征在于，含有通过使不饱和单体交联聚合而获得的吸水性树脂，其在生理盐水溶液中的离心保持容量不低于32g / g，质量中值粒径（D50）为200〜400 妈妈，直径小于150μm的粒子的比例为0〜2重量％，通过劣化0〜15重量％的提高物，0.1〜30重量％的劣化试验液中的提取物1小时。
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2.发明授权Water absorbing agent, water absorbent core using the agent, and manufacturing method for water absorbing agent 有权吸水剂，使用该吸水剂的吸水芯，以及吸水剂的制造方法公开(公告)号：US08198209B2
公开(公告)日：2012-06-12
申请号：US12294328
申请日：2007-03-20
申请人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
发明人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
CPC分类号： A61L15/60 , A61L15/18 , B01J20/103 , B01J20/26 , B01J20/261 , B01J20/267 , B01J2220/46 , B01J2220/68 , C08K3/36 , C08L101/14 , Y10T428/253
摘要： A water absorbing agent of the present invention has an internal crosslinking structure obtained by polymerization of a water-soluble unsaturated monomer. The agent satisfies conditions (a) to (d): (a) the agent contains water-insoluble inorganic particles at an amount of from 10 ppm to 1,900 ppm inclusive; (b) the agent contains 5 mass % or less particles which have such a size that they can pass through a sieve having a mesh opening size of 150 μm; (c) the agent has an absorbency against a pressure of 4.83 kPa (AAP) of 18 g/g or more; and (d) the water-insoluble inorganic particles reside on a surface of the water absorbing resin or near the surface.
摘要翻译： 本发明的吸水剂具有通过聚合水溶性不饱和单体获得的内部交联结构。 该试剂满足条件（a）至（d）：（a）该试剂含有10ppm至1,900ppm含量的水不溶性无机颗粒; （b）该试剂含有5质量％以下的粒径，使其能够通过网孔大小为150μm的筛子; （c）该试剂具有相对于4.83kPa（AAP）的压力为18g / g以上的吸收性; 和（d）水不溶性无机颗粒驻留在吸水树脂的表面上或表面附近。
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3.发明申请WATER ABSORBING AGENT, WATER ABSORBENT CORE USING THE AGENT, AND MANUFACTURING METHOD FOR WATER ABSORBING AGENT 有权吸水剂，使用该水剂的吸水芯，以及吸水剂的制造方法公开(公告)号：US20120305842A1
公开(公告)日：2012-12-06
申请号：US13467236
申请日：2012-05-09
申请人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
发明人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
IPC分类号： C08L35/02
CPC分类号： A61L15/60 , A61L15/18 , B01J20/103 , B01J20/26 , B01J20/261 , B01J20/267 , B01J2220/46 , B01J2220/68 , C08K3/36 , C08L101/14 , Y10T428/253
摘要： A water absorbing agent of the present invention has an internal crosslinking structure obtained by polymerization of a water-soluble unsaturated monomer. The agent satisfies conditions (a) to (d): (a) the agent contains water-insoluble inorganic particles at an amount of from 10 ppm to 1,900 ppm inclusive; (b) the agent contains 5 mass % or less particles which have such a size that they can pass through a sieve having a mesh opening size of 150 μm; (c) the agent has an absorbency against a pressure of 4.83 kPa (AAP) of 18 g/g or more; and (d) the water-insoluble inorganic particles reside on a surface of the water absorbing resin or near the surface.
摘要翻译： 本发明的吸水剂具有通过聚合水溶性不饱和单体获得的内部交联结构。 该试剂满足条件（a）至（d）：（a）该试剂含有10ppm至1,900ppm含量的水不溶性无机颗粒; （b）该试剂含有5质量％以下的粒径，使其能够通过网孔大小为150μm的筛子; （c）该试剂具有相对于4.83kPa（AAP）的压力为18g / g以上的吸收性; 和（d）水不溶性无机颗粒驻留在吸水树脂的表面上或表面附近。
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4.发明申请Particulate Water-Absorbing Agent Containing Water-Absorbent Resin as a Main Component 有权含有吸水性树脂作为主要成分的颗粒吸水剂公开(公告)号：US20080075937A1
公开(公告)日：2008-03-27
申请号：US11662590
申请日：2005-09-22
申请人： Katsuyuki Wada , Hiroko Ueda , Kazuki Kimura , Kunihiko Ishizaki
发明人： Katsuyuki Wada , Hiroko Ueda , Kazuki Kimura , Kunihiko Ishizaki
CPC分类号： C08J3/24 , A61L15/46 , A61L15/60 , A61L2300/30 , A61L2300/404 , A61L2300/802 , C08J2300/14 , Y10T428/24893 , Y10T428/24942 , Y10T428/2982 , Y10T442/653
摘要： In at least one embodiment, a particulate water-absorbing agent is provided which not only ensures the many conventional physical properties (absorption rate, centrifuge retention capacity, absorbency against pressure, particle size distribution etc.) but also prevents odor which is generated after the resin is swollen by absorption. The water absorbent agent of an embodiment of the present invention therefore does not cause odor in actual use. As a result of intensive study of the foregoing problem, an embodiment of the present invention offers a way of controlling a specific odor component, which is generated from impurities and/or by-product derived from the raw material, after the high temperature process. In this way, an embodiment of the present invention successfully provides a water absorbent agent not causing odor after the resin is swollen by absorption.
摘要翻译： 在至少一个实施方案中，提供了一种颗粒状吸水剂，其不仅确保了许多常规物理性能（吸收速率，离心保留能力，耐压吸收性，粒度分布等），而且还防止了在 树脂通过吸收而膨胀。 因此，本发明的实施方式的吸水剂在实际使用中不会引起气味。 作为对上述问题的深入研究的结果，本发明的实施方式提供了在高温处理之后控制由原料衍生的杂质和/或副产物产生的特定气味成分的方法。 以这种方式，本发明的一个实施方案成功地提供了在树脂通过吸收溶胀而不产生气味的吸水剂。
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5.发明授权Particulate water-absorbing agent containing water-absorbent resin as a main component 有权以吸水性树脂为主要成分的颗粒状吸水剂公开(公告)号：US07510988B2
公开(公告)日：2009-03-31
申请号：US11662590
申请日：2005-09-22
申请人： Katsuyuki Wada , Hiroko Ueda , Kazuki Kimura , Kunihiko Ishizaki
发明人： Katsuyuki Wada , Hiroko Ueda , Kazuki Kimura , Kunihiko Ishizaki
CPC分类号： C08J3/24 , A61L15/46 , A61L15/60 , A61L2300/30 , A61L2300/404 , A61L2300/802 , C08J2300/14 , Y10T428/24893 , Y10T428/24942 , Y10T428/2982 , Y10T442/653
摘要： In at least one embodiment, a particulate water-absorbing agent is provided which not only ensures the many conventional physical properties (absorption rate, centrifuge retention capacity, absorbency against pressure, particle size distribution etc.) but also prevents odor which is generated after the resin is swollen by absorption. The water absorbent agent of an embodiment of the present invention therefore does not cause odor in actual use. As a result of intensive study of the foregoing problem, an embodiment of the present invention offers a way of controlling a specific odor component, which is generated from impurities and/or by-product derived from the raw material, after the high temperature process. In this way, an embodiment of the present invention successfully provides a water absorbent agent not causing odor after the resin is swollen by absorption.
摘要翻译： 在至少一个实施方案中，提供了一种颗粒状吸水剂，其不仅确保了许多常规物理性能（吸收速率，离心保留能力，耐压吸收性，粒度分布等），而且还防止了在 树脂通过吸收而膨胀。 因此，本发明的实施方式的吸水剂在实际使用中不会引起气味。 作为对上述问题的深入研究的结果，本发明的实施方式提供了在高温处理之后控制由原料衍生的杂质和/或副产物产生的特定气味成分的方法。 以这种方式，本发明的一个实施方案成功地提供了在树脂通过吸收溶胀而不产生气味的吸水剂。
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6.发明授权Water absorbing agent, water absorbent core using the agent, and manufacturing method for water absorbing agent 有权吸水剂，使用该吸水剂的吸水芯，以及吸水剂的制造方法公开(公告)号：US09180220B2
公开(公告)日：2015-11-10
申请号：US13467236
申请日：2012-05-09
申请人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
发明人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
IPC分类号： C08G63/91 , C08F20/00 , B01J20/10 , B01J20/22 , B01J20/28 , B01J20/32 , A61L15/60 , A61L15/18 , B01J20/26 , C08L101/14
CPC分类号： A61L15/60 , A61L15/18 , B01J20/103 , B01J20/26 , B01J20/261 , B01J20/267 , B01J2220/46 , B01J2220/68 , C08K3/36 , C08L101/14 , Y10T428/253
摘要： A water absorbing agent of the present invention has an internal crosslinking structure obtained by polymerization of a water-soluble unsaturated monomer. The agent satisfies conditions (a) to (d): (a) the agent contains water-insoluble inorganic particles at an amount of from 10 ppm to 1,900 ppm inclusive; (b) the agent contains 5 mass % or less particles which have such a size that they can pass through a sieve having a mesh opening size of 150 μm; (c) the agent has an absorbency against a pressure of 4.83 kPa (AAP) of 18 g/g or more; and (d) the water-insoluble inorganic particles reside on a surface of the water absorbing resin or near the surface.
摘要翻译： 本发明的吸水剂具有通过聚合水溶性不饱和单体获得的内部交联结构。 该试剂满足条件（a）至（d）：（a）该试剂含有量为10ppm至1,900ppm的水不溶性无机颗粒; （b）该试剂含有5质量％以下的粒径，使其能够通过网孔大小为150μm的筛子; （c）该试剂具有相对于4.83kPa（AAP）的压力为18g / g以上的吸收性; 和（d）水不溶性无机颗粒驻留在吸水树脂的表面上或表面附近。
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7.发明申请WATER ABSORBING AGENT, WATER ABSORBENT CORE USING THE AGENT, AND MANUFACTURING METHOD FOR WATER ABSORBING AGENT 有权吸水剂，使用该水剂的吸水芯，以及吸水剂的制造方法公开(公告)号：US20090298685A1
公开(公告)日：2009-12-03
申请号：US12294328
申请日：2007-03-20
申请人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
发明人： Kazushi Torii , Hirofumi Shibata , Kazuki Kimura , Yasuhisa Nakashima , Motohiro Imura , Hiroko Ueda , Katsuyuki Wada
IPC分类号： B01J20/26
CPC分类号： A61L15/60 , A61L15/18 , B01J20/103 , B01J20/26 , B01J20/261 , B01J20/267 , B01J2220/46 , B01J2220/68 , C08K3/36 , C08L101/14 , Y10T428/253
摘要： A water absorbing agent of the present invention has an internal crosslinking structure obtained by polymerization of a water-soluble unsaturated monomer. The agent satisfies conditions (a) to (d): (a) the agent contains water-insoluble inorganic particles at an amount of from 10 ppm to 1,900 ppm inclusive; (b) the agent contains 5 mass % or less particles which have such a size that they can pass through a sieve having a mesh opening size of 150 μm; (c) the agent has an absorbency against a pressure of 4.83 kPa (AAP) of 18 g/g or more; and (d) the water-insoluble inorganic particles reside on a surface of the water absorbing resin or near the surface.
摘要翻译： 本发明的吸水剂具有通过聚合水溶性不饱和单体获得的内部交联结构。 该试剂满足条件（a）至（d）：（a）该试剂含有10ppm至1,900ppm含量的水不溶性无机颗粒; （b）该试剂含有5质量％以下的颗粒，其尺寸可以通过网孔大小为150μm的筛子; （c）该试剂具有相对于4.83kPa（AAP）的压力为18g / g以上的吸收性; 和（d）水不溶性无机颗粒驻留在吸水树脂的表面上或表面附近。
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公开(公告)号：US06187872B1
公开(公告)日：2001-02-13
申请号：US09051313
申请日：1998-04-06
申请人： Toru Yanase , Kazuki Kimura , Shin-ichi Fujino , Kinya Nagasuna , Kunihiko Ishizaki , Hirotama Fujimaru , Nobuyuki Harada
发明人： Toru Yanase , Kazuki Kimura , Shin-ichi Fujino , Kinya Nagasuna , Kunihiko Ishizaki , Hirotama Fujimaru , Nobuyuki Harada
IPC分类号： C08F812
CPC分类号： A61L15/60 , B01J20/26 , C08F8/00 , C08F8/44 , C08F2800/20 , C08F2810/20 , C08F220/06
摘要： A hydrogel polymer obtained by polymerizing a monomer component including acrylic acid (salt) is post-neutralized so that each of polymer particles derived from a polymer produced by neutralizing the hydrogel polymer has an allowable neutralization ratio. The polymer as obtained by neutralizing the hydrogel polymer is reacted with a crosslinking agent reactive to a functional group of the polymer. The allowable neutralization ratio, for example, is a neutralization ratio which is not lower, by not less than 20 mole percent, or more than, at least 55 mole percent, than an average neutralization ratio of a mass of the polymer particles, and the post-neutralization is carried out so that a number of polymer particles having a non-allowable neutralization ratio outside the allowable neutralization range is not more than 10 in 200 polymer particles, thus obtaining a water-absorbent agent having high absorbency under no applied pressure and high pressure wherein the amount of water soluble component is lower compared with the conventional water-absorbent agent and a change in pH of a swollen gel is small.
摘要翻译： 通过使包含丙烯酸（盐）的单体组分聚合而获得的水凝胶聚合物被后中和，使得通过中和水凝胶聚合物产生的聚合物衍生的各聚合物颗粒具有允许的中和比。 通过中和水凝胶聚合物获得的聚合物与与聚合物的官能团反应的交联剂反应。 例如，容许的中和比例是中和比，其比不到聚合物颗粒的质量的平均中和比不低于20摩尔％，或至多55摩尔％，而且 进行中和后，使得在200个聚合物粒子中，许多中和比例不超过允许中和比例的聚合物颗粒数不超过10个，从而获得在无施加压力下具有高吸收性的吸水剂， 其中水溶性成分的量与常规吸水剂相比较低，并且溶胀凝胶的pH变化很小。
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公开(公告)号：US06107358A
公开(公告)日：2000-08-22
申请号：US915557
申请日：1997-08-21
申请人： Nobuyuki Harada , Koji Miyake , Yoshihiro Motono , Hideyuki Tahara , Takumi Hatsuda , Teruyuki Kanto , Akito Yano , Yorimichi Dairoku , Kazuki Kimura , Yasuhiro Fujita
发明人： Nobuyuki Harada , Koji Miyake , Yoshihiro Motono , Hideyuki Tahara , Takumi Hatsuda , Teruyuki Kanto , Akito Yano , Yorimichi Dairoku , Kazuki Kimura , Yasuhiro Fujita
CPC分类号： C08F2/10 , C08F120/06 , C08F220/06
摘要： A method for the production of a water-absorbent resin capable of fast water absorption is disclosed which comprises the steps of dispersing bubbles of an inert gas in an aqueous monomer solution of a mixture of a water-soluble unsaturated monomer and a water-soluble cross-linking monomer and subjecting the mixture to copolymerization under the condition that a volume of the monomer solution wherein the inert gas is dispersed is in the range of 1.02 to 5 times of a volume of non-dispersant state.
摘要翻译： 公开了一种能够快速吸水的吸水性树脂的制造方法，该方法包括以下步骤：将惰性气体的气泡分散在水溶性不饱和单体和水溶性交联剂的混合物的单体水溶液中 在使分散有惰性气体的单体溶液的体积为非分散状态的体积的1.02〜5倍的条件下进行共聚合。
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10.发明授权公开(公告)号：US08182916B2
公开(公告)日：2012-05-22
申请号：US11816200
申请日：2006-02-10
CPC分类号： A61L15/60 , B01J20/26 , B01J20/264 , B01J20/267 , B01J20/28004 , B01J20/2803 , B01J20/28047 , B01J20/30 , B01J20/3028 , B01J2220/68 , C08J3/245 , C08J2300/14 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998
摘要： An object of the present invention is to provide a water absorbing agent having a low amount of residual monomer, small variance of the amount of residual monomer among ranges of particle size distribution and favorable absorption properties, and being sanitary; an absorbing article; and a method for the production of a water absorbing agent. The water absorbing agent of the present invention has the amount of residual monomer of not higher than 500 ppm, and a residual monomer index of not greater than 0.30. The method for the production includes a first step of obtaining a hydrogel polymer by polymerizing an aqueous solution of a monomer including an unsaturated carboxylic acid and/or a salt thereof in the presence of a crosslinking agent; a second step of obtaining a water absorbent resin precursor which is in powder form and includes particles having a particle size of 300 to 850 μm and particles having a particle size of smaller than 300 μm as main components by drying said hydrogel polymer followed by pulverization and classification to adjust the particle size distribution, a third step of obtaining a water absorbent resin by heating a mixture of said water absorbent resin precursor and a surface crosslinking agent, which can form an ester bond around the surface of said water absorbent resin precursor, a fourth step of adding by spraying an aqueous solution that includes a sulfur-containing reducing agent to said water absorbent resin, and a fifth step of subjecting the mixture of the water absorbent resin and said aqueous solution to a heat treatment under an airflow of not lower than 40° C. but not higher than 120° C.
摘要翻译： 本发明的目的是提供一种具有少量残留单体的吸水剂，在粒度分布范围和吸收性能良好之间的残留单体量的变化小，并且是卫生的; 吸收物品 和吸水剂的制造方法。 本发明的吸水剂的残留单体量不高于500ppm，残留单体指数不大于0.30。 制造方法包括在交联剂的存在下，通过使包含不饱和羧酸和/或其盐的单体的水溶液聚合而获得水凝胶聚合物的第一步骤; 第二步是通过干燥所述水凝胶聚合物，然后粉碎，得到粉末形式的吸水性树脂前体，并且包括粒度为300〜850μm的粒子和粒径小于300μm的粒子作为主要成分， 分级调整粒度分布，第三步骤是通过加热吸水性树脂前体和表面交联剂的混合物来获得吸水性树脂，该混合物可以在吸水性树脂前体的表面周围形成酯键， 第五步骤是通过将含有硫的还原剂的水溶液喷雾到所述吸水性树脂中而进行添加，第五步是在吸水性树脂和所述水溶液的混合物在不低于 超过40℃但不高于120℃
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