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    Epoxy-free hydroxy functional polyether based on oleyl alcohol and solvent-soluble copolymers containing the same
    1.
    发明授权
    Epoxy-free hydroxy functional polyether based on oleyl alcohol and solvent-soluble copolymers containing the same 失效
    基于油醇的无环氧基羟基官能聚醚和含有它的溶剂可溶性共聚物

    公开(公告)号：US4525543A

    公开(公告)日：1985-06-25

    申请号：US24052

    申请日：1979-03-26

    申请人： Kazys Sekmakas ,  Edward J. Murphy

    发明人： Kazys Sekmakas ,  Edward J. Murphy

    IPC分类号： C08L63/10 ,  C09D5/44 ,  C08G59/14 ,  C08L63/02

    CPC分类号： C09D5/44 ,  C08L63/10 ,  Y10S524/901

    摘要： Epoxy-free hydroxy functional polyethers are provided which are the reaction product of a diglycidyl ether of a bisphenol having a molecular weight of about 1000 with a stoichiometric proportion of oleyl alcohol. These oleyl alcohol-based polyethers can be copolymerized in organic solvent solution with monoethylenically unsaturated monomers to form solvent-soluble copolymers. When the monomers include carboxyl-functional monomers providing an acid number in the range of 12-60, the copolymers are particularly adapted to be dispersed in water with the aid of a base and then electrodeposited at the anode together with a heat-hardening formaldehyde condensate to form corrosion resistant coatings.

    摘要翻译： 提供无环氧羟基官能聚醚，它是分子量为约1000的双酚的二缩水甘油醚与化学计量比的油醇的反应产物。 这些基于油醇的聚醚可以在有机溶剂溶液中与单烯属不饱和单体共聚以形成溶剂可溶性共聚物。 当单体包括提供12-60范围内的酸值的羧基官能单体时，共聚物特别适合于借助于碱分散在水中，然后在阳极处与热硬化甲醛缩合物一起电沉积 以形成耐腐蚀涂层。

    D1365 BJ RADIATION CURABLE PRIMARY COATING FOR OPTICAL FIBER
    3.
    发明申请
    D1365 BJ RADIATION CURABLE PRIMARY COATING FOR OPTICAL FIBER 审中-公开
    D1365 BJ辐射可固化主要用于光纤的涂层

    公开(公告)号：US20080226912A1

    公开(公告)日：2008-09-18

    申请号：US11955547

    申请日：2007-12-13

    申请人： Tyson Dean NORLIN ,  Steven R. Schmid ,  Edward J. Murphy ,  John M. Zimmerman ,  Anthony Joseph Tortorello

    发明人： Tyson Dean NORLIN ,  Steven R. Schmid ,  Edward J. Murphy ,  John M. Zimmerman ,  Anthony Joseph Tortorello

    IPC分类号： B32B17/02 ,  C08L75/00 ,  B32B17/10 ,  C03C25/34

    CPC分类号： C09D175/08 ,  C03C25/1065 ,  C03C25/326 ,  C08G18/672 ,  C09D5/002 ,  C09D175/16 ,  G02B6/02395 ,  Y10T428/2964 ,  C08G18/48

    摘要： Radiation curable coatings for use as a Primary Coating for optical fibers, optical fibers coated with said coatings and methods for the preparation of coated optical fibers. The present invention provides a radiation curable Primary Coating composition comprising: an oligomer; first diluent monomer; a second diluent monomer; a third diluent monomer; a first light stabilizer; a first photoinitiator; a second photoinitiator; an antioxidant; a second light stabilizer; and an adhesion promoter; wherein said oligomer is the reaction product of hydroxyl-containing acrylate; an isocyanate; a polyether polyol; a polymerization inhibitor; a catalyst; and a diluent; wherein said oligomer has a number average molecular weight of from at least about 4000 g/mol to less than or equal to about 15,000 g/mol; and wherein said catalyst is selected from the group consisting of copper naphthenate; cobalt naphthenate; zinc naphthenate; triethylamine; triethylenediamine; 2-methyltriethyleneamine; dibutyl tin dilaurate; metal carboxylates, including, but not limited to: organobismuth catalysts such as bismuth neodecanoate; zinc neodecanoate; zirconium neodecanoate; zinc 2-ethylhexanoate; sulfonic acids, including but not limited to dodecylbenzene sulfonic acid, methane sulfonic acid; amino or organo-base catalysts, including, but not limited to, 1,2-dimethylimidazole and diazabicyclooctane; triphenyl phosphine; alkoxides of zirconium and titanium, including, but not limited to Zirconium butoxide and Titanium butoxide; and Ionic liquid phosphonium salts; and tetradecyl(trihexyl) phosphonium chloride; and wherein a cured film of said radiation curable Primary Coating composition has a peak tan □ Tg of from about −25° C. to about −55° C.; and a modulus of from about 0.85 MPa to about 1.10 MPa.

    摘要翻译： 用作光纤的主要涂层的辐射固化涂层，涂覆有所述涂层的光纤以及用于制备涂覆的光纤的方法。 本发明提供了一种可辐射固化的初级涂料组合物，其包含：低聚物; 第一稀释剂单体; 第二稀释剂单体; 第三稀释剂单体; 第一光稳定剂; 第一种光引发剂; 第二光引发剂; 抗氧化剂 第二种光稳定剂; 和粘合促进剂; 其中所述低聚物是含羟基的丙烯酸酯的反应产物; 异氰酸酯; 聚醚多元醇; 阻聚剂; 催化剂 和稀释剂; 其中所述低聚物的数均分子量为至少约4000g / mol至小于或等于约15,000g / mol; 并且其中所述催化剂选自环烷酸铜; 环烷酸钴; 环烷酸锌; 三乙胺 三亚乙基二胺 2-甲基三亚乙基胺; 二月桂酸二丁基锡; 金属羧酸盐，包括但不限于：有机铋催化剂如新戊酸铋; 新癸酸锌; 新癸酸锆; 2-乙基己酸锌; 磺酸，包括但不限于十二烷基苯磺酸，甲磺酸; 氨基或有机碱催化剂，包括但不限于1,2-二甲基咪唑和二氮杂双环辛烷; 三苯基膦 锆和钛的醇盐包括但不限于丁氧基锆和丁醇钛; 和离子液体鏻盐; 和十四烷基（三己基）鏻氯化物; 并且其中所述可辐射固化的初级涂层组合物的固化膜具有约-25℃至约-55℃的峰值tanδTg。 和约0.85MPa至约1.10MPa的模量。

    Adherent ultraviolet cured coatings
    5.
    发明授权
    Adherent ultraviolet cured coatings 失效
    附着紫外线固化涂层

    公开(公告)号：US4532021A

    公开(公告)日：1985-07-30

    申请号：US606527

    申请日：1984-05-07

    申请人： Edward J. Murphy ,  Ronald J. Lewarchik ,  Jeffrey W. Thompson

    发明人： Edward J. Murphy ,  Ronald J. Lewarchik ,  Jeffrey W. Thompson

    IPC分类号： C09D4/06 ,  C08J3/28 ,  C08L31/08

    CPC分类号： C09D4/06

    摘要： Ultraviolet-curable liquid coating compositions are disclosed in which improved adhesion to metal and plastic surfaces is obtained. This improvement is obtained by using, in admixture: (1) from 10% to about 60% of total resin solids of an organic solvent-soluble solution copolymer of monoethylenically unsaturated monomers including from 2.5% to 10% of tertiary amine monomer which is an aminoalkyl ester or amide of an alpha, beta-monoethylenic monocarboxylic acid in which the alkyl group contains 2-4 carbon atoms; and (2) from 40% to 90% of total resin solids of radiation-curable ethylenically unsaturated liquid. The coating composition includes photoinitiators and/or photosensitizers rendering the composition sensitive to ultraviolet light, and the components are present in solution in at least about 10% of inert volatile organic solvent.

    摘要翻译： 公开了可获得改善的对金属和塑料表面的粘附性的紫外线固化液体涂料组合物。 这种改进通过以下方式获得：（1）总树脂固体的10％至约60％的单烯属不饱和单体的有机溶剂可溶性溶液共聚物，包括2.5％至10％的叔胺单体，其为 其中烷基含有2-4个碳原子的α，β-单烯基单羧酸的氨基烷基酯或酰胺; 和（2）可辐射固化的烯属不饱和液体的总树脂固体的40％至90％。 涂料组合物包括光引发剂和/或光敏剂，使组合物对紫外光敏感，并且组分在溶液中存在于至少约10％的惰性挥发性有机溶剂中。

    Production of monomeric etherified bisphenol-formaldehyde condensates
    6.
    发明授权
    Production of monomeric etherified bisphenol-formaldehyde condensates 失效
    单体醚化双酚 - 甲醛缩合物的生产

    公开(公告)号：US4310653A

    公开(公告)日：1982-01-12

    申请号：US195110

    申请日：1980-10-08

    申请人： John J. Krajewski ,  Edward J. Murphy

    发明人： John J. Krajewski ,  Edward J. Murphy

    IPC分类号： C08G8/36 ,  C09D161/14 ,  C08G2/34 ,  C08G8/20

    CPC分类号： C09D161/14 ,  C08G8/36 ,  Y10S524/901

    摘要： A method of producing essentially monomeric etherified formaldehyde condensates with a bisphenol having a plurality of formaldehyde-reactive sites is disclosed in which the bisphenol is reacted with at least about 2 moles of formaldehyde per mole of bisphenol in solution in etherifying alcohol in the presence of an insoluble strong acid cation exchange resin. The reaction is carried out at a reaction temperature of from about 30.degree. C. to about 100.degree. C. to simultaneously provide the desired methylolation and etherification without introducing soluble ionic contaminants.

    摘要翻译： 公开了一种用具有多个甲醛反应性位点的双酚生产基本上单体醚化的甲醛缩合物的方法，其中在醚化醇存在下，双酚与溶剂中每摩尔双酚的至少约2摩尔甲醛反应 不溶性强酸阳离子交换树脂。 反应在约30℃至约100℃的反应温度下进行，以同时提供所需的羟甲基化和醚化，而不引入可溶性离子污染物。

    Ribbon assemblies and radiation-curable ink compositions for use in forming the ribbon assemblies
    8.
    发明授权
    Ribbon assemblies and radiation-curable ink compositions for use in forming the ribbon assemblies 失效
    色带组件和可用于形成色带组件的可辐射固化油墨组合物

    公开(公告)号：US06197422B1

    公开(公告)日：2001-03-06

    申请号：US09158134

    申请日：1998-09-22

    申请人： Edward J. Murphy ,  Edward P. Zahora ,  Johannes C. van den Burg

    发明人： Edward J. Murphy ,  Edward P. Zahora ,  Johannes C. van den Burg

    IPC分类号： D02G300

    CPC分类号： C03C25/106 ,  C03C25/1065 ,  C08F290/064 ,  C08F290/067 ,  G02B6/4482 ,  Y10T428/2933 ,  Y10T428/2938 ,  Y10T428/2964

    摘要： Provided is a ribbon assembly having the functional capability of providing break-out of ink coated or colored outer primary coated optical glass fibers from the ribbon assembly. The ink coating or colored outer primary coating is formulated from a benzophenone compound and at least about 1 wt. % of a homolytic photoinitiator to provide a level of adhesion between the ink coating or colored outer primary coating and matrix material which is less than the level of adhesion between the ink coating or colored outer primary coating and an adjacent underlying coating. Also provided are ink coating and colored outer primary coating compositions adapted to form ink coatings and colored outer primary coatings suitable for use on optical glass fibers contained in a ribbon assembly.

    摘要翻译： 提供了一种带状组件，其具有从带状组件提供油墨涂覆或着色的外部初级涂覆光学玻璃纤维的功能性能。 油墨涂料或着色的外部初级涂料由二苯甲酮化合物配制，并且至少约1wt。 ％的均相光引发剂，以提供油墨涂层或着色的外部初级涂层和基质材料之间的粘附水平，其小于油墨涂层或着色外初级涂层和相邻下层涂层之间的粘合程度。 还提供了适用于形成油墨涂层和适用于包含在色带组件中的光学玻璃纤维上的着色的外部主要涂层的着色的外部初级涂料组合物的油墨涂料和着色的外部初级涂料组合物。