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    Olefin oligomerization to produce hydrocarbon compositions useful as fuels
    1.
    发明授权
    Olefin oligomerization to produce hydrocarbon compositions useful as fuels 有权
    烯烃低聚产生用作燃料的烃组合物

    公开(公告)号：US07678954B2

    公开(公告)日：2010-03-16

    申请号：US11342385

    申请日：2006-01-27

    申请人： Keith H. Kuechler ,  Stephen Harold Brown ,  Helge Jaensch ,  Georges M. Mathys ,  Shifang Luo ,  Jane C. Cheng

    发明人： Keith H. Kuechler ,  Stephen Harold Brown ,  Helge Jaensch ,  Georges M. Mathys ,  Shifang Luo ,  Jane C. Cheng

    IPC分类号： C07C2/02

    CPC分类号： C10G50/00 ,  C09K8/32

    摘要： In a process for producing a hydrocarbon composition, a feed comprising at least one C3 to C8 olefin and an olefinic recycle stream rich in C9− hydrocarbons is contacted with a crystalline molecular sieve catalyst having an average crystal size no greater than 0.05 micron and an alpha value between about 100 and about 600 in at least one reaction zone under olefin oligomerization conditions including an inlet temperature between about 150° C. and about 350° C., a pressure of at least 2,860 kPa and a recycle to feed weight ratio of about 0.1 to about 3.0. The contacting produces an oligomerization effluent stream, which is separated into at least a hydrocarbon product stream rich in C9+ hydrocarbons and the olefinic recycle stream.

    摘要翻译： 在制备烃组合物的方法中，将包含至少一种C 3 -C 8烯烃和富含C 9烃的烯烃循环料的进料与平均晶体尺寸不大于0.05微米的结晶分子筛催化剂和α 在至少一个反应区中在约100至约600之间的烯烃低聚条件下，包括入口温度为约150℃至约350℃，压力至少为2,860kPa，循环至进料重量比为约 0.1至约3.0。 接触产生低聚流出物流，其被分离成至少一种富含C9 +烃的烃产物流和烯烃再循环流。

    Process for producing phenol and methyl ethyl ketone
    6.
    发明授权
    Process for producing phenol and methyl ethyl ketone 失效
    苯酚和甲基乙基酮的制备方法

    公开(公告)号：US07834218B2

    公开(公告)日：2010-11-16

    申请号：US12162970

    申请日：2007-02-08

    申请人： Jihad M. Dakka ,  Jon E. Stanat ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jeffrey T. Elks

    发明人： Jihad M. Dakka ,  Jon E. Stanat ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jeffrey T. Elks

    IPC分类号： C07C45/53 ,  C07C37/08

    CPC分类号： C07C409/08 ,  C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  C07C49/10 ,  C07C39/04

    摘要： A process for producing phenol and methyl ethyl ketone comprises contacting benzene and a C4 alkylating agent under alkylation conditions and in the presence of an alkylation catalyst comprising at least one molecular sieve of the MCM-22 family to produce an alkylation effluent comprising secbutylbenzene; wherein the contacting is conducted in a plurality of reaction zones and the C4 alkylating agent secbutylbenzene fraction is recovered from the alkylation effluent and comprises at least 95 wt % sec-butylbenzene, less than 100 wt ppm of C8+ olefins, and less than 0.5 wt % of isobutylbenzene and tert-butylbenzene. The sec-butylbenzene fraction is then oxidized to produce sec-butylbenzene hydroperoxide and the hydroperoxide is cleaved to produce phenol and methyl ethyl ketene.

    摘要翻译： 一种生产苯酚和甲基乙基酮的方法包括在烷基化条件下和在包含至少一种MCM-22族分子筛的烷基化催化剂的存在下使苯和C4烷基化剂接触以产生包含二丁基苯的烷基化流出物; 其中所述接触在多个反应区中进行，并且所述C4烷基化剂仲丁苯部分从烷基化流出物中回收，并且包含至少95重量％的仲丁基苯，小于100重量ppm的C 8+烯烃和小于0.5重量％ 的异丁基苯和叔丁基苯。 然后将仲丁基馏分氧化以产生仲丁基苯氢过氧化物，并将氢过氧化物裂解以产生苯酚和甲基乙基乙烯酮。

    Preparation of alkylaromatic hydrocarbons and alkylaryl sulfonates
    8.
    发明授权
    Preparation of alkylaromatic hydrocarbons and alkylaryl sulfonates 失效
    烷基芳烃和烷基芳基磺酸盐的制备

    公开(公告)号：US07622621B2

    公开(公告)日：2009-11-24

    申请号：US10509508

    申请日：2003-03-28

    申请人： Carolyn B. Duncan ,  David Wayne Turner ,  Jane C. Cheng ,  Charles M. Yarbrough ,  Raphael Frans Caers ,  Ramzi Y. Saleh ,  James L. Propp

    发明人： Carolyn B. Duncan ,  David Wayne Turner ,  Jane C. Cheng ,  Charles M. Yarbrough ,  Raphael Frans Caers ,  Ramzi Y. Saleh ,  James L. Propp

    IPC分类号： C07C2/66 ,  C07C2/12

    CPC分类号： C07C2/66 ,  C07C15/107 ,  C07C303/06 ,  C07C2527/1206 ,  C07C2527/126 ,  C07C2527/173 ,  C07C2529/70 ,  C07C309/31

    摘要： In a process for preparing an alkylaromatic hydrocarbon composition an olefinic hydrocarbon mixture and an aromatic compound are contacted under alkylation conditions with an aromatic alkylation catalyst selected from a homogeneous acid catalyst and heterogeneous acid catalyst comprising a molecular sieve having an X-ray diffraction pattern including d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstroms. The olefinic hydrocarbon mixture comprises at least 5 wt % by weight of mono-olefin oligomers of the empirical formula: CnH2n wherein n is greater than or equal to 10, the mono-olefin oligomers comprising at least 20 percent by weight of olefins having at least 12 carbon atoms, and the olefins having at least 12 carbon atoms having an average of from 0.8 to 2.0 C1-C3 alkyl branches per carbon chain. Sulfonation of the alkylaromatic hydrocarbon product produces an alkylaryl sulfonate mixture that exhibits advantageous properties, such as biodegradability and hard and cold water performance.

    摘要翻译： 在制备烷基芳族烃组合物的方法中，烯烃混合物和芳族化合物在烷基化条件下与选自均相酸催化剂的芳族烷基化催化剂和包含具有包括d的X射线衍射图的分子筛的多相酸催化剂接触 最大值为12.4±0.25,6.9±0.15,3.57±0.07和3.42±0.07埃。 烯烃混合物包含至少5重量％的经验式为C n H 2n的单烯烃低聚物，其中n大于或等于10，单烯烃低聚物包含至少20重量％的至少具有至少20重量％ 12个碳原子，并且具有至少12个碳原子的烯烃在每个碳链上平均具有0.8至2.0个C 1 -C 3烷基支链。 烷基芳族烃产物的磺化产生显示出有利性质的烷基芳基磺酸盐混合物，例如生物降解性和冷水和冷水性能。

    Method of producing an aromatics alkylation catalyst
    9.
    发明授权
    Method of producing an aromatics alkylation catalyst 有权
    芳烃烷基化催化剂的制备方法

    公开(公告)号：US06051521A

    公开(公告)日：2000-04-18

    申请号：US139226

    申请日：1998-08-25

    申请人： Jane C. Cheng ,  Hye Kyung C. Timken

    发明人： Jane C. Cheng ,  Hye Kyung C. Timken

    IPC分类号： B01J29/04 ,  B01J37/00 ,  B01J37/30

    CPC分类号： B01J29/70 ,  B01J29/7038 ,  B01J37/0009 ,  B01J37/30

    摘要： This invention provides a method of producing an aromatics alkylation catalyst comprising the steps of:(a) synthesizing a layered oxide material MCM-56 in the presence of alkali and/or alkaline earth metal cations;(b) prior to any calcination of the MCM-56, subjecting the MCM-56 produced in step (a) to ammonium ion exchange so as to at least partially replace the alkaline or alkaline earth metal cations associated with the MCM-56 with ammonium ions; then(c) heating the ammonium-exchanged MCM-56 to decompose the ammonium cations and convert the MCM-56 into the hydrogen form; and(d) after step (b), forming the MCM-56 into catalyst particles.The resultant catalyst exhibits enhanced activity in the alkylation of benzene with ethylene and propylene.

    摘要翻译： 本发明提供一种生产芳烃烷基化催化剂的方法，包括以下步骤：（a）在碱金属和/或碱土金属阳离子存在下合成层状氧化物材料MCM-56; （b）在MCM-56的任何煅烧之前，使步骤（a）中产生的MCM-56进行铵离子交换，以便至少部分地用铵与铵相关的碱金属或碱土金属阳离子 离子 然后（c）加热铵交换的MCM-56以分解铵阳离子并将MCM-56转化为氢形式; 和（d）步骤（b）之后，将MCM-56形成催化剂颗粒。 所得催化剂在用乙烯和丙烯烷基化苯中表现出增强的活性。