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公开(公告)号：US07258795B1
公开(公告)日：2007-08-21
申请号：US11260965
申请日：2005-10-28
IPC分类号： B01D15/00
CPC分类号： B01D15/00 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/186 , B01J20/20 , B01J20/205 , B01J20/28064 , B01J20/28078 , B01J20/3057 , B01J20/3204 , B01J20/3236 , B01J20/3433 , B01J20/3483
摘要： A process and adsorbent for removing contaminants from silicone based solvents is disclosed. The process provides for cleaning a solvent for reuse, and regeneration of the adsorbent. The adsorbents are for adsorbing organic and inorganic compounds that have accumulated in the silicone solvents.
摘要翻译： 公开了一种用于从有机硅基溶剂中除去污染物的方法和吸附剂。 该方法提供清洗溶剂以便再利用和再生吸附剂。 吸附剂用于吸附积聚在有机硅溶剂中的有机和无机化合物。
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公开(公告)号：US5518708A
公开(公告)日：1996-05-21
申请号：US336395
申请日：1994-11-08
CPC分类号： B01J29/046 , B01J29/04 , C01B33/2884 , Y10S423/21 , Y10S423/25 , Y10S423/26 , Y10S423/28
摘要： Molecular sieve compositions are prepared by extracting aluminum and substituting chromium and/or tin for extracted aluminum to give molecular sieve products containing framework chromium and/or tin atoms. The process of preparing the chromium and/or tin-containing molecular sieves involves contacting a starting molecular sieve with a solution or slurry of at least one of a fluoro salt of chromium or a fluoro salt of tin under effective process conditions to provide for aluminum extraction and substitution of chromium and/or tin.
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3.发明授权
公开(公告)号：US5366616A
公开(公告)日：1994-11-22
申请号：US980834
申请日：1992-11-24
CPC分类号： B01J29/04 , B01J29/046 , C01B33/2884
摘要： This invention relates to hydrocarbon conversion processes using novel molecular sieve compositions as the catalyst. These molecular sieves contain chromium in the framework structure along with aluminum and silicon. The process of preparing the chromium-containing molecular sieves involves contacting a starting molecular sieve with a solution or slurry of a fluoro salt of chromium under effective process conditions to provide for aluminum extraction and substitution of chromium.
摘要翻译： 本发明涉及使用新型分子筛组合物作为催化剂的烃转化方法。 这些分子筛在框架结构中含有铬以及铝和硅。 制备含铬分子筛的方法包括在有效的工艺条件下使起始分子筛与铬的氟盐溶液或浆液接触以提供铝的提取和取代铬。
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公开(公告)号：US5192722A
公开(公告)日：1993-03-09
申请号：US729660
申请日：1991-07-15
IPC分类号： C04B35/19
CPC分类号： C04B35/19
摘要： This invention relates to processes for preparing a ceramic article having as its principal crystalline phase a leucite/pollucite solid solution. The process involves the use of a zeolite to form the article. Zeolites which can be used are those that have a SiO.sub.2 /Al.sub.2 O.sub.3 ratio of about 3.5 to about 7.5 such as zeolite Y. The zeolite is exchanged with potassium, rubidium and cesium, then calcined at a temperature of about 900.degree. to about 1100.degree. C. for a time to collapse the zeolite framework and provide an amorphous powder. Next, the amorphous powder is formed into a shaped article and the article is sintered at a temperature of about 1150.degree. to about 1400.degree. C. for a time of about 0.5 to about 12 hours to give a ceramic article whose principal crystalline phase is a leucite/pollucite solid solution, is substantially crack free, has less than 5% porosity, and a coefficient of thermal expansion of about 2.times.10.sup.-6 to about 27.times.10.sup.-60 C.sup.-1. This invention also relates to the leucite/pollucite ceramic article.
摘要翻译： 本发明涉及制备具有白云母/琉璃灰固体溶液作为其主要结晶相的陶瓷制品的方法。 该方法涉及使用沸石来形成制品。 可以使用的沸石是具有约3.5至约7.5的SiO 2 / Al 2 O 3比例的沸石，例如沸石Y.沸石与钾，铷和铯交换，然后在约900℃至约1100℃的温度下煅烧 一段时间来坍缩沸石骨架并提供无定形粉末。 接下来，将无定形粉末形成成型制品，并将制品在约1150℃至约1400℃的温度下烧结约0.5至约12小时，得到主要结晶相为 白云母/白矾土固溶体基本上无裂纹，孔隙率小于5％，热膨胀系数约2×10-6至约27×10-60℃-1。 本发明还涉及白云石/琉璃苣陶瓷制品。
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5.发明授权Hydrocarbon conversion processes using a novel crystalline microporous metal oxysulfide composition 失效使用新的结晶微孔金属氧硫化物组合物的烃转化方法
公开(公告)号：US5128025A
公开(公告)日：1992-07-07
申请号：US803936
申请日：1991-12-09
CPC分类号： B01J29/85 , B01J29/005 , C01B33/2884 , B01J29/84
摘要： This invention deals with a hydrocarbon conversion process using a crystalline oxysulfide composition. The crystalline oxysulfide composition has a three-dimensional microporous framework structure of at least MO.sub.2, MS.sub.2, and MOS tetrahedral units, having an intracrystalline pore system and an empirical formula expressed in molar ratios:(M.sub.s Al.sub.t P.sub.u Si.sub.v)S.sub.w O.sub.2-wwhere M is at least one metal selected from the group consisting of metals which: 1) can be incorporated into the framework structure of a microporous molecular sieve and 2) form hydrolytically stable sulfides; s, t, u, v and w are the mole fractions of M, Al, P, Si and S respectively. The values of s, t, u and v are chosen such that when t is greater than zero u is greater than zero, s+t+u+v=1 and when s=1, M is only a combination of gallium and germanium.
摘要翻译： 本发明涉及使用结晶氧硫化物组合物的烃转化方法。 结晶氧硫化物组合物具有至少具有MO2，MS2和MOS四面体单元的三维微孔骨架结构，具有结晶孔系统和以摩尔比表示的经验式：（MsAltPuSiv）SwO 2 -w，其中M为至少一个 选自以下的金属的金属：1）可以结合到微孔分子筛的骨架结构中，2）形成水解稳定的硫化物; s，t，u，v和w分别是M，Al，P，Si和S的摩尔分数。 选择s，t，u和v的值，使得当t大于零时，u大于零，s + t + u + v = 1，当s = 1时，M只是镓和锗的组合 。
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6.发明授权Process for separating a mixture of molecular species using crystalline microporous metal sulfide compositions 失效使用结晶微孔金属硫化物组合物分离分子物质的混合物的方法
公开(公告)号：US5013337A
公开(公告)日：1991-05-07
申请号：US507819
申请日：1990-04-12
CPC分类号： B01J31/0254 , B01J27/04 , B01J31/0239 , C01B17/20 , C01B19/007 , C01G17/00 , C09K11/06 , B01J2231/641 , C01P2002/72 , C01P2002/74 , C01P2006/80 , C01P2006/82 , Y10S95/902
摘要： This invention relates to a process for separating a mixture of molecular species based on the molecular size (kinetic diameter) or on the degree of polarity of the molecular species using a crystalline composition having a three-dimensional microporous structure of MA.sub.2 units where A is sulfur or selenium and having the empirical formula expressed in molar ratios: xR:MA.sub.2.+-.0.2 :zH.sub.2 O where R represents at least one organic templating agent present in the intracrystalline pore system, x is the moles of R, z is the moles of water and M is germanium or tin. A composition having the empirical formula expressed in molar ratios: xR:M.sub.1-y M'.sub.y A.sub.2.+-.0.2 :zH.sub.2 O, where M' is a metal such as cobalt, zinc, manganese, iron, nickel, copper, cadmium and gallium may also be used in the process.
摘要翻译： 本发明涉及使用具有MA2单元的三维微孔结构的结晶组合物，基于分子大小（动力学直径）或分子物质的极性的程度来分离分子种类的混合物的方法，其中A是硫 或硒，并具有以摩尔比表示的经验式：xR：MA2 +/- 0.2：zH2O其中R表示晶体内孔体系中存在的至少一种有机模板剂，x是R的摩尔数，z是水的摩尔数， M是锗或锡。 具有以摩尔比表示的经验式的组合物：xR：M1-yM'yA2 +/- 0.2：zH2O，其中M'是诸如钴，锌，锰，铁，镍，铜，镉和镓的金属也可以是 在过程中使用。
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7.发明授权
公开(公告)号：US4973460A
公开(公告)日：1990-11-27
申请号：US218494
申请日：1988-07-06
IPC分类号： B01J29/85 , C01B37/06 , C01B37/08 , C07C2/12 , C07C2/54 , C07C4/06 , C07C5/02 , C07C5/22 , C07C5/27 , C07C5/41
CPC分类号： C07C5/41 , B01J29/85 , C01B37/06 , C01B37/08 , C07C2/12 , C07C2/54 , C07C4/06 , C07C5/02 , C07C5/224 , C07C5/2716 , C07C2527/173 , C07C2529/84 , Y10S423/30
摘要： Molecular sieve compositions having three-dimensional microporous framework structures of LiO.sub.2, AlO.sub.2, PO.sub.2 and SiO.sub.2 tetrahedral oxide units are disclosed. These molecular sieves have an empirical chemical composition on an anhydrous basis expressed by the formula:mR: (Li.sub.w Al.sub.x P.sub.y Si.sub.z)O.sub.2wherein "R" represents at least one organic templating agent present in the intracrystalline pore system; "m" represents the molar amount of "R" present per mole of (Li.sub.w Al.sub.x P.sub.y Si.sub.z)O.sub.2 ; and "w", "x", "y" and "z" represent the mole fractions of lithium, aluminum, phosphorus and silicon, respectively, present as tetrahedral oxides. Their use as adsorbents, catalysts, etc. is also disclosed.
摘要翻译： 公开了具有LiO 2，AlO 2，PO 2和SiO 2四面体氧化物单元的三维微孔骨架结构的分子筛组合物。 这些分子筛具有以下公式表示的无水基础上的经验化学组成：mR：（LiwAlxPySiz）O 2其中“R”表示存在于晶体内孔系统中的至少一种有机模板剂; “m”表示每摩尔（LiwAlxPySiz）O 2存在的“R”摩尔量; 和“w”，“x”，“y”和“z”分别表示作为四面体氧化物存在的锂，铝，磷和硅的摩尔分数。 还公开了它们作为吸附剂，催化剂等的用途。
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公开(公告)号：US4940570A
公开(公告)日：1990-07-10
申请号：US835293
申请日：1986-03-03
IPC分类号： B01J29/84 , C01B25/45 , C01B37/06 , C07C2/12 , C07C2/54 , C07C5/02 , C07C5/22 , C07C5/27 , C07C5/41
CPC分类号： C07C5/41 , B01J29/84 , C01B37/06 , C07C2/12 , C07C2/54 , C07C5/02 , C07C5/224 , C07C5/2716 , C07C2527/173 , C07C2529/84
摘要： Molecular sieve compositions having three-dimensional microporous framework structures of BeO.sub.2, AlO.sub.2 and PO.sub.2 tetrahedral oxide units are disclosed. These molecular sieves have an empirical chemical composition on an anhydrous basis expressed by the formula:mR:(Be.sub.x Al.sub.y P.sub.z)O.sub.2wherein "R" represents at least one organic templating agent present in the intracrystalline pore system; "m" represents the molar amount of "R" present per mole of (Be.sub.x Al.sub.y P.sub.z)O.sub.2 ; and "x", "y" and "z" represent the mole fractions of beryllium, aluminum and phosphorus, respectively, present as tetrahedral oxides. Their use as adsorbents, catalysts, etc. is also disclosed.
摘要翻译： 公开了具有BeO 2，AlO 2和PO 2四面体氧化物单元的三维微孔骨架结构的分子筛组合物。 这些分子筛具有由下式表示的无水基础上的经验化学组成：mR：（BexAlyPz）O 2，其中“R”表示存在于晶体内孔系统中的至少一种有机模板剂; “m”表示每摩尔（BexAlyPz）O 2存在的“R”摩尔量; 和“x”，“y”和“z”分别表示作为四面体氧化物存在的铍，铝和磷的摩尔分数。 还公开了它们作为吸附剂，催化剂等的用途。
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9.发明授权
公开(公告)号：US4917876A
公开(公告)日：1990-04-17
申请号：US195474
申请日：1988-05-17
摘要： Crystalline molecular sieves having three-dimensional microporous framework structures of FeO.sub.2, TiO.sub.2, AlO.sub.2, and PO.sub.2 tetrahedral oxide units are disclosed. These molecular sieves have an empirical chemical composition on an anhydrous basis expressed by the formula:mR:(M.sub.x Al.sub.y P.sub.z)O.sub.2wherein "R" represents at least one organic templating agent present in the intracrystalline pore system; "M" represents iron and titanium, "m" represents the molar amount of "R" present per mole of (M.sub.x Al.sub.y P.sub.z)O.sub.2 ; and "x", "y" and "z" represnt the mole fractions of "M", aluminum and phosphorus, respectively, present as tetrahedral oxides. Their use as adsorbents, catalysts, etc. is also disclosed.
摘要翻译： 公开了具有FeO 2，TiO 2，AlO 2和PO 2四面体氧化物单元的三维微孔骨架结构的结晶分子筛。 这些分子筛具有无水基础上的经验化学组成，由下式表示：mR：（MxAlyPz）O 2其中“R”表示存在于晶体内孔系统中的至少一种有机模板剂; “M”表示铁和钛，“m”表示每摩尔（M×AlyPz）O 2存在的“R”摩尔量; 和“x”，“y”和“z”分别表示作为四面体氧化物存在的“M”，铝和磷的摩尔分数。 还公开了它们作为吸附剂，催化剂等的用途。
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公开(公告)号：US4861743A
公开(公告)日：1989-08-29
申请号：US126192
申请日：1987-11-25
CPC分类号： C01B37/08 , B01J29/84 , C01B37/04 , C01B37/06 , B01J2229/64
摘要： Non-zeolitic molecular sieves are prepared by contacting a body of alumina or silica-alumina (optionally containing reactive sources of phosphorus pentoxide and/or other elements desired in the non-zeolitic molecular sieve) with a liquid reaction mixture containing a reactive source of phosphorus pentoxide (and optionally reactive sources of silica and/or other elements desired in the non-zeolitic molecular sieve), and an organic templating agent, thereby causing the body to react with the liquid reaction mixture and to form crystals of the non-zeolitic molecular sieve within the body.
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