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    Processes for preparing beta-diketone compound, metal complex thereof and metallic compound
    1.
    发明申请
    Processes for preparing beta-diketone compound, metal complex thereof and metallic compound 失效
    制备β-二酮化合物，其金属络合物和金属化合物的方法

    公开(公告)号：US20070098897A1

    公开(公告)日：2007-05-03

    申请号：US10559809

    申请日：2004-05-20

    申请人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani ,  Keiichi Nakumura

    发明人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani ,  Keiichi Nakumura

    IPC分类号： C23C16/00 ,  B05D3/02 ,  C07F7/28 ,  C07C45/45

    CPC分类号： C07C49/92 ,  C07C45/455 ,  C07C45/77 ,  C07C45/80 ,  C07C49/12

    摘要： Disclosed is a process for preparing a β-diketone compound such as 2,6-dimethyl-3,5-heptanedione, which comprises reacting an ester compound such as an alkyl isobutyrate with a ketone compound such as 3-methylbutanone in the presence of an alkali metal alkoxide as a catalyst. The process comprises a step 1 in which an ester compound CR1R2R3COOQ is reacted with a ketone compound CR4R5R6COCH2R7 using an alkali metal alkoxide catalyst to give a β-diketone compound CR1R2R3COCHR4R5R6. (In the formulae, R7 is hydrogen or an alkyl group of 1 to 4 carbon atoms while others are each independently hydrogen or an alkyl group of 1 to 3 carbon atoms, and at least one of R1 to R6 is hydrogen.)

    摘要翻译： 公开了一种制备2,6-二甲基-3,5-庚二酮的β-二酮化合物的方法，该方法包括使异氰酸烷基酯等酯化合物与3-甲基丁酮等酮化合物在 碱金属醇盐作为催化剂。 该方法包括步骤1，其中酯化合物CR 1 R 2 SO 3 COOQ与酮化合物CR 4 使用碱金属醇盐催化剂，得到β5，R 6，R 5，R 7，R 7， 二酮化合物CR 1 R 2 R 2 SO 3 R 4 R 5 R 5 SUP> 6 。 （式中，R 7为氢或1〜4个碳原子的烷基，其余各自独立地为氢或1〜3个碳原子的烷基，R 1〜 SUP> 1至R 6是氢。）

    Processes for preparing β-diketone compound, metal complex thereof and metallic compound
    2.
    发明授权
    Processes for preparing β-diketone compound, metal complex thereof and metallic compound 失效
    制备β-二酮化合物，其金属络合物和金属化合物的方法

    公开(公告)号：US07393982B2

    公开(公告)日：2008-07-01

    申请号：US10559809

    申请日：2004-05-20

    申请人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani ,  Keiichi Nakamura

    发明人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani ,  Keiichi Nakamura

    IPC分类号： C07C45/72

    CPC分类号： C07C49/92 ,  C07C45/455 ,  C07C45/77 ,  C07C45/80 ,  C07C49/12

    摘要： Disclosed is a process for preparing a β-diketone compound such as 2,6-dimethyl-3,5-heptanedione, which comprises reacting an ester compound such as an alkyl isobutyrate with a ketone compound such as 3-methylbutanone in the presence of an alkali metal alkoxide as a catalyst. The process comprises a step 1 in which an ester compound CR1R2R3COOQ is reacted with a ketone compound CR4R5R6COCH2R7 using an alkali metal alkoxide catalyst to give a β-diketone compound CR1R2R2R3COCHR4R5R6. (In the formulae, R7 is hydrogen or an alkyl group of 1 to 4 carbon atoms while others are each independently hydrogen or an alkyl group of 1 to 3 carbon atoms, and at least one of R1 to R6 is hydrogen.)

    摘要翻译： 公开了一种制备2,6-二甲基-3,5-庚二酮的β-二酮化合物的方法，该方法包括使异氰酸烷基酯等酯化合物与3-甲基丁酮等酮化合物在 碱金属醇盐作为催化剂。 该方法包括步骤1，其中酯化合物CR 1 R 2 SO 3 COOQ与酮化合物CR 4 使用碱金属醇盐催化剂，得到β5，R 6，R 5，R 7，R 7， 二酮化合物CR 1 1 R 2 R 2 R 3 SO 3 R 4 R 4 SUP> 5 6 （式中，R 7为氢或1〜4个碳原子的烷基，其余各自独立地为氢或1〜3个碳原子的烷基，R 1〜 SUP> 1至R 6是氢。）

    Process for preparing β-diketone compound and process for preparing metal complex thereof
    3.
    发明授权
    Process for preparing β-diketone compound and process for preparing metal complex thereof 失效
    制备β-二酮化合物的方法及其制备金属络合物的方法

    公开(公告)号：US07084306B2

    公开(公告)日：2006-08-01

    申请号：US10500963

    申请日：2002-12-18

    申请人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani

    发明人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani

    IPC分类号： C07C45/72 ,  C07C11/00 ,  C07F9/00 ,  C07F7/00

    CPC分类号： C07C49/92 ,  C07C45/455 ,  C07C45/77 ,  C07C49/12

    摘要： Disclosed is a process for preparing 2,2,6,6-tetramethyl-3,5-heptanedione, comprising reacting a pivalic acid alkyl ester with pinacolone in the presence of an alkali metal alkoxide catalyst using a pivalic acid alkyl ester as a solvent but using no other solvent or reacting them in an amide type or urea type solvent in the presence of an alkali metal alkoxide catalyst. Also disclosed is a process for preparing a 2,2,6,6-tetramethyl-3,5-heptanesione metal complex using the 2,2,6,6-tetramethyl-3,5-heptanedione obtained by the above process. The process for preparing 2,2,6,6-tetramethyl-3,5-heptanedione is an industrially advantageous process in which an alkali metal alkoxide that is easy to handle can be used as a catalyst for preparing 2,2,6,6-tetramethyl-3,5-heptanedione from a pivalic acid alkyl ester and pinacolone.

    摘要翻译： 公开了一种制备2,2,6,6-四甲基-3,5-庚二酮的方法，包括在碱金属醇盐催化剂存在下，使用新戊酸烷基酯作为溶剂使新戊酸烷基酯与频那酮酮反应，但 不使用其它溶剂或在酰胺型或尿素型溶剂中，在碱金属醇盐催化剂的存在下反应。 还公开了使用通过上述方法获得的2,2,6,6-四甲基-3,5-庚二酮制备2,2,6,6-四甲基-3,5-庚内酯金属络合物的方法。 制备2,2,6,6-四甲基-3,5-庚二酮的方法是一种工业上有利的方法，其中易于处理的碱金属醇盐可用作制备2,2,6,6 四甲基-3,5-庚二酮从新戊酸烷基酯和频那酮酮。

    Process for preparing-diketone compound and process for preparing metal complex thereof
    4.
    发明申请
    Process for preparing-diketone compound and process for preparing metal complex thereof 失效
    制备二酮化合物的方法及其制备金属络合物的方法

    公开(公告)号：US20050119466A1

    公开(公告)日：2005-06-02

    申请号：US10500963

    申请日：2002-12-18

    申请人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani

    发明人： Makoto Saito ,  Takashi Ueda ,  Takashi Tani

    IPC分类号： C07C45/45 ,  C07C45/77 ,  C07C49/12 ,  C07C49/92 ,  C07F5/00

    CPC分类号： C07C49/92 ,  C07C45/455 ,  C07C45/77 ,  C07C49/12

    摘要： Disclosed is a process for preparing 2,2,6,6-tetramethyl-3,5-heptanedione, comprising reacting a pivalic acid alkyl ester with pinacolone in the presence of an alkali metal alkoxide catalyst using a pivalic acid alkyl ester as a solvent but using no other solvent or reacting them in an amide type or urea type solvent in the presence of an alkali metal alkoxide catalyst. Also disclosed is a process for preparing a 2,2,6,6-tetramethyl-3,5-heptanesione metal complex using the 2,2,6,6-tetramethyl-3,5-heptanedione obtained by the above process. The process for preparing 2,2,6,6-tetramethyl-3,5-heptanedione is an industrially advantageous process in which an alkali metal alkoxide that is easy to handle can be used-as a catalyst for preparing 2,2,6,6-tetramethyl-3,5-heptanedione from a pivalic acid alkyl ester and pinacolone.

    摘要翻译： 公开了一种制备2,2,6,6-四甲基-3,5-庚二酮的方法，包括在碱金属醇盐催化剂存在下，使用新戊酸烷基酯作为溶剂使新戊酸烷基酯与频那酮酮反应，但 不使用其它溶剂或在酰胺型或尿素型溶剂中，在碱金属醇盐催化剂的存在下反应。 还公开了使用通过上述方法获得的2,2,6,6-四甲基-3,5-庚二酮制备2,2,6,6-四甲基-3,5-庚内酯金属络合物的方法。 制备2,2,6,6-四甲基-3,5-庚二酮的方法是工业上有利的方法，其中可以使用易于处理的碱金属醇盐 - 作为制备2,2,6,6-四甲基-3,5-庚二酮的催化剂， 由新戊酸烷基酯和频哪醇酮制备6-四甲基-3,5-庚二酮。

    Process for producing cyanobenzoic acid derivatives
    6.
    发明授权
    Process for producing cyanobenzoic acid derivatives 失效
    制备氰基苯甲酸衍生物的方法

    公开(公告)号：US06433211B1

    公开(公告)日：2002-08-13

    申请号：US09404362

    申请日：1999-09-24

    申请人： Hiroshi Yasuda ,  Haruaki Ito ,  Takashi Tani ,  Kimitaka Ohshiro ,  Makoto Saito ,  Sumio Soya ,  Kuniomi Marumo

    发明人： Hiroshi Yasuda ,  Haruaki Ito ,  Takashi Tani ,  Kimitaka Ohshiro ,  Makoto Saito ,  Sumio Soya ,  Kuniomi Marumo

    IPC分类号： C07C25500

    CPC分类号： C07C253/30 ,  C07C255/57

    摘要： A process for producing a cyanobenzoic acid compound, a cyanobenzamide compound, an alkyl cyanobenzoate compound, and a cyanobenzoyl chloride compound, which are useful intermediates for a variety of chemicals such as pharmaceuticals, agrochemicals, liquid crystals, and monomers for functional polymers. One nitrile group of an easily available phthalonitrile compound is selectively hydrolyzed to thereby produce a cyanobenzamide compound with high selectivity and yield. The cyanobenzamide compound thus-produced is transformed under acidic conditions into a cyanobenzoic acid compound and a cyanobenzoate ester compound without the cyano group of the benzene ring being damaged.

    摘要翻译： 用于制备用于各种化学品如药物，农业化学品，液晶和功能性聚合物的单体的有用的中间体的氰基苯甲酸化合物，氰基苯甲酰胺化合物，烷基氰基苯甲酸酯化合物和氰基苯甲酰氯化合物的方法。 选择性地水解一种容易获得的邻苯二腈化合物的腈基，从而以高选择性和收率产生氰基苯甲酰胺化合物。 将由此制得的氰基苯甲酰胺化合物在酸性条件下转化成氰基苯甲酸化合物和氰基苯甲酸酯化合物，而苯环的氰基不被损坏。

    Highly concentrated aqueous solutions of N,N-dialkyl-glycines and process for preparation thereof
    7.
    发明授权
    Highly concentrated aqueous solutions of N,N-dialkyl-glycines and process for preparation thereof 失效
    N，N-二烷基甘氨酸的高浓度水溶液及其制备方法

    公开(公告)号：US07056450B2

    公开(公告)日：2006-06-06

    申请号：US10491717

    申请日：2002-10-03

    申请人： Takashi Ueda ,  Makoto Saito ,  Tohru Katoh ,  Katsuhisa Inoue

    发明人： Takashi Ueda ,  Makoto Saito ,  Tohru Katoh ,  Katsuhisa Inoue

    IPC分类号： C07C229/12 ,  C07C227/42 ,  C09K3/00

    CPC分类号： C07C227/18 ,  C07C229/12

    摘要： An aqueous high-concentration solution of N,N-dialkylglycine, economical, easy to handle, and useful for subsequent organic chemical reactions, is provided. Also is provided a process for production thereof. The aqueous high-concentration solution of N,N-dialkylglycine which contains the N,N-dialkylglycine at a concentration of 30–80% by mass, and a metal-mineral acid salt at a content of 0.3–3% by mass can be produced industrially from an aqueous N,N-dialkylglycine alkali metal salt as the source material by the steps of (i) neutralizing an aqueous solution of an N,N-dialkylglycine alkali metal salt with a mineral acid, (ii) condensing the obtained aqueous solution by removal of water, and (iii) separating by solid-liquid separation the deposited alkali metal-mineral acid salt from the resulting slurry of the aqueous N,N-dialkylglycine solution and the alkali metal-mineral acid salt.

    摘要翻译： 提供了经济，易于处理并且用于随后的有机化学反应的N，N-二烷基甘氨酸的高浓度水溶液。 还提供了其生产方法。 含有浓度为30〜80质量％的N，N-二烷基甘氨酸的N，N-二烷基甘氨酸的水溶液高浓度溶液和0.3〜3质量％的金属 - 无机酸盐可以是 以（i）用无机酸中和N，N-二烷基甘氨酸碱金属盐的水溶液，（ii）将得到的水溶液（N，N-二烷基甘氨酸碱金属盐）中和，得到工业上由N，N-二烷基甘氨酸碱金属盐水溶液作为原料， 通过去除水分解溶液，和（iii）通过固液分离沉淀的碱金属 - 无机酸盐从N，N-二烷基甘氨酸水溶液和碱金属 - 无机酸盐的所得浆液中分离。

    Adjustable armrest device
    10.
    发明授权
    Adjustable armrest device 失效
    可调式扶手装置

    公开(公告)号：US08777317B2

    公开(公告)日：2014-07-15

    申请号：US12521356

    申请日：2007-12-04

    申请人： Makoto Saito ,  Takashi Morimoto ,  Ken Suzuki ,  Toshikazu Numazawa ,  Hideko Kitamura

    发明人： Makoto Saito ,  Takashi Morimoto ,  Yoshiharu Kitamura ,  Ken Suzuki ,  Toshikazu Numazawa

    IPC分类号： B60N2/46

    CPC分类号： B60N2/767

    摘要： An armrest device including a stationary shaft 2, fixed to a seat frame, an armrest body 7 in which the stationary shaft 2 is inserted and which is rotatable, a lock spring 3 made of a coil spring tightly wound around the stationary shaft 2, with one end of the coil spring serving as a stationary-side hook 3a locked to the armrest body 7, and the other end of the coil spring serving as a free-side hook 3b A hook-supporting part 12 that supports the free-side hook 3b such that the free-side hook 3b is raised in the axial direction of the stationary shaft 2, a hook-fitting part 13 that enlarges the diameter of the lock spring 3 by dropping the free-side hook 3b on the hook-supporting part 12 downward in the axial direction of the stationary shaft 2, a plate 11 for a hook, where the plate 11 projects from the armrest body 7, and a cam member 5 on the stationary shaft 2. The cam member 5 having (1) an unlocking cam part 5b for unlocking the lock spring 3 by dropping the free-side hook 3b from the hook-supporting part 12 into the hook-fitting part 13 when the armrest body 7 is rotated in the armrest-accommodating direction, and (2) a relocking cam part 5c for locking the lock spring 3 by raising the free-side hook 3b from the hook-fitting part 13 and supporting it by the hook-supporting part 12 when the armrest body 7 is rotated in the armrest-use direction.

    摘要翻译： 一种扶手装置，包括固定在座椅框架上的固定轴2，固定轴2插入其中并且可旋转的扶手本体7，由固定轴2紧密缠绕的螺旋弹簧制成的锁定弹簧3， 用作固定侧钩3a的螺旋弹簧的一端，锁定在扶手本体7上，螺旋弹簧的另一端用作自由侧钩3b。支撑自由侧钩的钩支撑部12 3b，使得自由侧钩3b沿着固定轴2的轴向方向升高;钩配合部13，其通过将自由侧钩3b落在钩支撑部上而扩大锁定弹簧3的直径 12在固定轴2的轴向方向上向下，用于钩的板11，其中板11从扶手主体7突出，以及在固定轴2上的凸轮构件5.凸轮构件5具有（1） 解锁凸轮部5b，用于通过使自由侧钩3bf落下来解锁锁定弹簧3 当扶手本体7在扶手收纳方向上转动时，将钩支撑部分12钩入钩配件13，和（2）用于通过提升自由侧钩来锁定锁弹簧3的重锁凸轮部分5c 3b，并且当扶手本体7在扶手使用方向上旋转时，由钩部件13支撑并由钩支撑部件12支撑。