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公开(公告)号：US4767850A
公开(公告)日：1988-08-30
申请号：US868403
申请日：1986-05-29
申请人： Peter M. Lange , Erich Rauenbusch
发明人： Peter M. Lange , Erich Rauenbusch
IPC分类号： C08F8/00 , B01J20/281 , B01J20/285 , B01J39/16 , B01J39/18 , B01J39/20 , C07H1/06 , C07H5/06 , C07H15/203 , C08F8/36 , G01N30/88
CPC分类号： C07H15/203 , B01J39/20 , B01J39/26 , B01J49/0008 , B01J49/0069 , C08F8/36 , C08F2800/20 , Y10T428/2982
摘要： In the purification of acarbose by contacting an acarbose-containing solution with a cation exchanger to adsorb the acarbose, eluting the ion exchanger and collecting an eluate fraction enriched in purified acarbose, the improvement wherein the cation exchanger is a polymer obtained by polymerizing an aromatic compound possessing at least one vinyl group and at least one hydrophilic monomer in the presence of a solvent for the monomer which is a precipitant for the crosslinked polymer formed, isolating the resistant polymer, and sulphonating the polymer in the presence of a swelling agent for the polymer. The invention gives sharp separation and other processing advantages.
摘要翻译： 在通过使含有阿卡波糖的溶液与阳离子交换剂接触以吸附阿卡波糖以洗脱离子交换剂并收集富集纯化的阿卡波糖的洗脱液级分的阿卡波糖的纯化中，其中阳离子交换剂是通过使芳族化合物聚合而获得的聚合物 在用于形成的交联聚合物的沉淀剂的溶剂的溶剂存在下，具有至少一个乙烯基和至少一个亲水性单体，分离耐药聚合物，并在聚合物溶胀剂存在下磺化聚合物 。 本发明提供了清晰的分离等加工优点。
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公开(公告)号：US4666776A
公开(公告)日：1987-05-19
申请号：US786263
申请日：1985-10-10
申请人： Peter M. Lange , Erich Rauenbusch
发明人： Peter M. Lange , Erich Rauenbusch
IPC分类号： C08F8/00 , B01J20/281 , B01J20/285 , B01J39/16 , B01J39/18 , B01J39/20 , B01J49/06 , B01J49/53 , C07H1/06 , C07H5/06 , C07H15/203 , C08F8/36 , G01N30/88 , B32B5/16
CPC分类号： C07H15/203 , B01J39/20 , B01J39/26 , B01J49/0008 , B01J49/0069 , C08F8/36 , C08F2800/20 , Y10T428/2982
摘要： In the purification of acarbose by contacting an acarbose-containing solution with a cation exchanger to adsorb the acarbose, eluting the ion exchanger and collecting an eluate fraction enriched in purified acarbose, the improvement wherein the cation exchanger is a polymer obtained by polymerizing an aromatic compound possessing at least one vinyl group and at least one hydrophilic monomer in the presence of a solvent for the monomer which is a precipitant for the crosslinked polymer formed, isolating the resistant polymer, and sulphonating the polymer in the presence of a swelling agent for the polymer. The invention gives shapr separation and other processing advantages.
摘要翻译： 在通过使含有阿卡波糖的溶液与阳离子交换剂接触以吸附阿卡波糖以洗脱离子交换剂并收集富集纯化的阿卡波糖的洗脱液级分的阿卡波糖的纯化中，其中阳离子交换剂是通过使芳族化合物聚合而获得的聚合物 在用于形成的交联聚合物的沉淀剂的溶剂的溶剂存在下，具有至少一个乙烯基和至少一个亲水性单体，分离耐药聚合物，并在聚合物溶胀剂存在下磺化聚合物 。 本发明提供了切割分离等加工优点。
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公开(公告)号：US4563371A
公开(公告)日：1986-01-07
申请号：US565081
申请日：1983-12-23
IPC分类号： C22C1/08 , B01J20/02 , B01J23/44 , B01J37/30 , C23C18/20 , C23C18/28 , C23C20/04 , B05D3/04 , B01J31/08 , B05D1/18 , B05D3/10
CPC分类号： C23C18/28 , C23C18/1644 , C23C18/208 , C23C18/30
摘要： The metallization of porous solid bodies, such as, for example, ion exchange materials, by loading the surfaces of the metal-free substrates with transition metal ions and subsequently treating them with reducing agents can be improved by activating the substrates, before or after the loading with metal ions, with elements of group 1 or 8 of the periodic table or compounds thereof and sensitizing any activating ions still present. The metallization products are useful hydrogenation catalysts.
摘要翻译： 通过用过渡金属离子加载无金属底物的表面并随后用还原剂处理它们的多孔固体物质例如离子交换材料的金属化可以通过在底物之前或之后激活而改善 用金属离子负载周期表中第1或8族的元素或其化合物，并使任何仍然存在的活化离子敏化。 金属化产物是有用的氢化催化剂。
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公开(公告)号：US4511722A
公开(公告)日：1985-04-16
申请号：US466807
申请日：1983-02-16
IPC分类号： B01J41/08 , B01J41/09 , C07D207/26 , C07D207/267 , C07D207/27 , C07D209/48 , C07D233/32 , C07D233/74 , C07D263/22 , C08F26/00 , C08F26/06 , C07D263/20 , C07D209/40 , C07D207/12
CPC分类号： C07D207/267 , B01J41/085 , C07D207/27 , C07D209/48 , C07D233/32 , C07D263/22 , C08F26/06
摘要： Cyclic N-vinylacylamines are prepared by heating carbonic acid esters of cyclic N-2-hydroxyethylacylamines in the presence of a catalytic amount of alkali or alkaline earth metal compound having an alkaline reaction and subsequently distilling the reaction mixture.Cyclic N-vinylacylamines are valuable precursors for preparing plant protection agents and medicaments and serve as polymerization and copolymerization components for preparing plastics, surface coatings, paints and ion exchange materials.
摘要翻译： 在催化量的具有碱性反应的碱金属或碱土金属化合物的存在下，加热环状N-2-羟乙基酰胺的碳酸酯，然后蒸馏反应混合物，制备环状N-乙烯基酰胺。 环状N-乙烯基酰胺是制备植物保护剂和药物的有价值的前体，并且用作制备塑料，表面涂料，油漆和离子交换材料的聚合和共聚组分。
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5.发明授权Process for reducing the wash water requirement of weakly basic anion exchangers 失效降低弱碱性阴离子交换剂洗涤水需求的方法
公开(公告)号：US4705637A
公开(公告)日：1987-11-10
申请号：US740089
申请日：1985-05-31
CPC分类号： B01J49/0013 , B01J41/046
摘要： The invention relate to a process for reducing the wash water required by weakly basic anion exchangers containing primary and/or secondary amino groups when fed with water containing carbon dioxide; in accordance with the process the exhausted, weakly basic anion exchangers are treated with dilute aqueous mineral acids before being regenerated.
摘要翻译： 本发明涉及一种当含有二氧化碳的水时，减少含有伯氨基和/或仲氨基的弱碱性阴离子交换剂所需的洗涤水的方法; 根据该方法，在再生之前用稀释的无机酸水溶液处理耗尽的弱碱性阴离子交换剂。
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6.发明授权
公开(公告)号：US4504688A
公开(公告)日：1985-03-12
申请号：US587094
申请日：1984-03-07
IPC分类号： C07C43/04 , B01J31/00 , C07B61/00 , C07C1/00 , C07C1/20 , C07C7/12 , C07C7/148 , C07C11/02 , C07C11/08 , C07C41/00 , C07C41/06 , C07C41/36 , C07C67/00 , C07C41/05
CPC分类号： C07C41/36 , C07C41/06 , C07C7/14891
摘要： A process for the preparation of pure alkyl tertiary alkyl ethers and hydrocarbon raffinates which are substantially free from tertiary olefins and alkanols. An alkanol and a hydrocarbon mixture containing at least one tertiary olefin are contacted with the alkanol being present in a stoichiometric excess. The reaction product is removed from the reaction zone and excess alkanol in the reaction product or a partial stream thereof is absorbed on a synthetic ion exchanger containing groups which exchange cations or anions or mixtures of such ion exchangers. After absorption of at least a portion of the alkanol on the synthetic ion exchanger, the alkanol is desorbed by contacting the same with a hydrocarbon mixture containing at least one tertiary olefin.
摘要翻译： 一种制备基本上不含叔烯烃和链烷醇的纯烷基叔烷基醚和烃残液的方法。 含有至少一种叔烯烃的链烷醇和烃混合物与化学计量过量存在的链烷醇接触。 将反应产物从反应区中除去，反应产物中的过量链烷醇或其部分物流被吸收在含有交换阳离子或阴离子的基团的合成离子交换剂上，或这些离子交换剂的混合物。 在合成离子交换剂上吸收至少一部分链烷醇之后，通过使链烷醇与含有至少一种叔烯烃的烃混合物接触来解链链烷醇。
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公开(公告)号：US4402947A
公开(公告)日：1983-09-06
申请号：US308725
申请日：1981-10-05
申请人： Heinrich F. Moeschler , Klaus Sasse , Peter M. Lange , Christian Golker , Gerhard Zoebelein , Otto Telle
发明人： Heinrich F. Moeschler , Klaus Sasse , Peter M. Lange , Christian Golker , Gerhard Zoebelein , Otto Telle
IPC分类号： A01N63/02 , A01N43/50 , A01N43/54 , C07H19/044 , C07H19/052 , C07H19/067 , A61K31/71 , C07H19/16 , C07H19/18
CPC分类号： C07H19/052 , A01N43/50 , A01N43/54 , C07H19/044
摘要： Arthropodicidally and fungicidally active heavy metal salts of nikkomicin are produced by reacting nikkomicin with a water-soluble heavy metal salt in an aqueous medium.
摘要翻译： 通过在水性介质中使尼克金霉素与水溶性重金属盐反应制备人造丝虫和杀真菌活性的尼克金霉素的重金属盐。
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8.发明授权
公开(公告)号：US4754020A
公开(公告)日：1988-06-28
申请号：US837490
申请日：1986-03-07
IPC分类号： C07C245/20 , C09B29/00 , C09B41/00 , C09B67/26 , C09B29/033 , C09B62/24 , C09B67/44
CPC分类号： C09B41/001 , C09B67/0073
摘要： A new method of diazotization consists in using as the diazotizing agent in an aqueous, aqueous organic or organic medium the system comprising salt of nitrous acid+acid insoluble in the reaction medium, in particular organic or inorganic cation exchangers having acid groups. The diazonium salt solutions thus prepared are immediately reacted with coupling components to give azo dyestuffs, the insoluble acid and/or its salt being separated off before or after the coupling.
摘要翻译： 一种新的重氮化方法包括在含水有机或有机介质中使用重氮化剂，该系统包含在反应介质中不可溶的亚硝酸+酸，特别是具有酸基的有机或无机阳离子交换剂。 如此制备的重氮盐溶液立即与偶联组分反应，得到偶氮染料，在偶联之前或之后将不溶性酸和/或其盐分离出来。
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9.发明授权Process for the preparation of concentrated solutions of anionic dyestuffs and dyestuff additives by cation exchange with cation exchange resin 失效通过与阳离子交换树脂阳离子交换制备阴离子染料和染料添加剂的浓缩溶液的方法
公开(公告)号：US4702744A
公开(公告)日：1987-10-27
申请号：US867855
申请日：1986-05-27
CPC分类号： C09B67/0073 , C09B67/0096 , Y10S8/937
摘要： Stable, concentrated aqueous solutions of, in particular, anionic reactive dyestuffs are obtained in a comparatively simple manner by freeing from salts, preferably by means of membrane separation processes, solutions of these substances just as they are obtained in the course of synthesis, and by replacing, with the aid of ion exchangers, the cations which cause sparing solubility.
摘要翻译： 特别是阴离子活性染料的稳定的浓缩水溶液以相对简单的方式通过从盐中释放而获得，优选通过膜分离方法，这些物质的溶液正如在合成过程中获得的那样，以及通过 在离子交换剂的帮助下，替代引起节省溶解度的阳离子。
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10.发明授权Synthetic resins based on crosslinked copolymers of monovinyl and polyvinyl compounds 失效基于单乙烯基和聚乙烯基化合物的交联共聚物的合成树脂
公开(公告)号：US4319015A
公开(公告)日：1982-03-09
申请号：US81967
申请日：1979-10-04
申请人： Werner Struver , Harold Heller , Peter M. Lange
发明人： Werner Struver , Harold Heller , Peter M. Lange
IPC分类号： C08F12/00 , B01J47/04 , C08F16/00 , C08F16/32 , C08F20/00 , C08F20/10 , C08F36/00 , C08F212/00 , C08F212/04 , C08F220/12 , C08F212/34 , C08F212/36 , C08F220/20
CPC分类号： C08F220/12 , B01J47/04 , C08F212/04 , Y10T428/31931
摘要： New Synthetic resins useful as inert material for separating layers in ion exchanger mixed bed filters. The new synthetic resins are copolymers of(a) substituted styrenes and/or methacrylates,(b) methacrylates of polyhydric alcohols and/or aromatic polyvinyl compounds and(c) unsaturated hydrocarbons which have at least two allyl groupings in the molecule, and/or polyvinyl ethers of polyhydric alcohols, and optionally(d) styrene.
摘要翻译： 新型合成树脂可用作离子交换器混合床过滤器中分离层的惰性材料。 新合成树脂是（a）取代苯乙烯和/或甲基丙烯酸酯，（b）多元醇和/或芳族聚乙烯基化合物的甲基丙烯酸酯和（c）分子中具有至少两个烯丙基的不饱和烃的共聚物，和/或 多元醇的聚乙烯醚，和（d）苯乙烯。
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