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    Process for preparing linear monofunctional and telechelic difunctional polymers and compositions obtained thereby
    1.
    发明授权
    Process for preparing linear monofunctional and telechelic difunctional polymers and compositions obtained thereby 失效
    制备线型单官能和遥爪双官能聚合物的方法及由此得到的组合物

    公开(公告)号：US5512635A

    公开(公告)日：1996-04-30

    申请号：US167668

    申请日：1993-12-15

    申请人： Philip O. Nubel ,  Howard B. Yokelson ,  Steven A. Cohen ,  Raymond T. Behrends ,  William G. Bouslog ,  James P. Nelson

    发明人： Philip O. Nubel ,  Howard B. Yokelson ,  Steven A. Cohen ,  Raymond T. Behrends ,  William G. Bouslog ,  James P. Nelson

    IPC分类号： C08C19/28 ,  C08F4/69 ,  C08G18/10 ,  C08G18/65 ,  C08G18/69 ,  C08G61/08 ,  C08G63/00

    CPC分类号： C08G63/00 ,  C08C19/28 ,  C08G18/10 ,  C08G18/6588 ,  C08G18/69 ,  C08G61/08

    摘要： This invention relates to a process for preparation of non-crosslinked linear monofunctional and telechelic difunctional unsaturated polymers wherein the functional groups are reactive terminal groups other than vinyl groups. The average functionality number of the monofunctional unsaturated polymers is at least 0.7, as determined by nuclear magnetic resonance spectroscopy (NMR). The average functionality number of the telechelic difunctional polymers is at least 1.7, as determined by NMR. Monofunctional olefins and difunctional olefins are reacted with cyclic olefins or unsaturated polymers to prepare difunctional polymers. The process is substantially free of side reactions comprising double bond migration and cyclization. The unsaturated functional polymers can be reacted in condensation, addition and transesterification reactions to prepare polyesters, graft copolymers, polyurethanes, polyureas, polyamides, thermoplastic and thermosetting resins, block copolymers, ion exchange resins, adhesives, films, fibers, foams and flocculants.

    摘要翻译： 本发明涉及一种制备非交联线性单官能和遥爪双官能不饱和聚合物的方法，其中官能团是乙烯基以外的反应性末端基团。 通过核磁共振光谱（NMR）测定，单官能不饱和聚合物的平均官能度至少为0.7。 通过NMR确定的遥爪双官能聚合物的平均官能度至少为1.7。 单官能烯烃和双官能烯烃与环烯烃或不饱和聚合物反应以制备双官能聚合物。 该方法基本上不含包含双键迁移和环化的副反应。 不饱和官能聚合物可以在缩合，加成和酯交换反应中进行反应，以制备聚酯，接枝共聚物，聚氨酯，聚脲，聚酰胺，热塑性和热固性树脂，嵌段共聚物，离子交换树脂，粘合剂，薄膜，纤维，泡沫和絮凝剂。

    Process for preparing linear monofunctional and telechelic difunctional polymers and compositions obtained thereby
    2.
    发明授权
    Process for preparing linear monofunctional and telechelic difunctional polymers and compositions obtained thereby 失效
    制备线型单官能和遥爪双官能聚合物的方法及由此得到的组合物

    公开(公告)号：US5621047A

    公开(公告)日：1997-04-15

    申请号：US543080

    申请日：1995-10-13

    申请人： Philip O. Nubel ,  Howard B. Yokelson ,  Steven A. Cohen ,  William G. Bouslog

    发明人： Philip O. Nubel ,  Howard B. Yokelson ,  Steven A. Cohen ,  William G. Bouslog

    IPC分类号： C08C19/28 ,  C08F4/69 ,  C08G18/10 ,  C08G18/65 ,  C08G18/69 ,  C08G61/08 ,  C08G63/00 ,  C08G61/12

    CPC分类号： C08G63/00 ,  C08C19/28 ,  C08G18/10 ,  C08G18/6588 ,  C08G18/69 ,  C08G61/08

    摘要： This invention relates to a process for preparation of non-crosslinked linear monofunctional and telechelic difunctional unsaturated polymers wherein the functional groups are acrylate or methacrylate groups. The average functionality number of the monofunctional unsaturated polymers is at least 0.7, as determined by nuclear magnetic resonance spectroscopy (NMR). The average functionality number of the telechelic difunctional polymers is at least 1.7, as determined by NMR. Alkyl acrylates or alkyl methacrylates are reacted with cyclic olefinic non-conjugated compounds or unsaturated hydrocarbon polymers to prepare monofunctional and difunctional polymers. The process is substantially free of side reactions comprising double bond migration and cyclization.

    摘要翻译： 本发明涉及制备非交联线性单官能和遥爪双官能不饱和聚合物的方法，其中官能团是丙烯酸酯或甲基丙烯酸酯基团。 通过核磁共振光谱（NMR）测定，单官能不饱和聚合物的平均官能度至少为0.7。 通过NMR确定的遥爪双官能聚合物的平均官能度至少为1.7。 丙烯酸烷基酯或甲基丙烯酸烷基酯与环状烯属非共轭化合物或不饱和烃聚合物反应以制备单官能和双官能聚合物。 该方法基本上不含包含双键迁移和环化的副反应。

    Methods for preparing ruthenium carbene complex precursors and ruthenium carbene complexes
    3.
    发明授权
    Methods for preparing ruthenium carbene complex precursors and ruthenium carbene complexes 有权
    制备钌卡宾络合物前体和钌卡宾络合物的方法

    公开(公告)号：US08779152B2

    公开(公告)日：2014-07-15

    申请号：US13272788

    申请日：2011-10-13

    申请人： Linda A. Kunz ,  Steven A. Cohen ,  Melvin L. Luetkens, Jr.

    发明人： Linda A. Kunz ,  Steven A. Cohen ,  Melvin L. Luetkens, Jr.

    IPC分类号： C07F15/00

    CPC分类号： C07F15/0046 ,  B01J31/2295 ,  C07F15/0053

    摘要： A method for preparing a ruthenium carbene complex precursor includes reacting a ruthenium refinery salt with a hydrogen halide to form a ruthenium intermediate, and reacting the ruthenium intermediate with an L-type ligand to form the ruthenium carbene complex precursor. A method for preparing a ruthenium vinylcarbene complex includes converting a ruthenium carbene complex precursor into a ruthenium hydrido halide complex, and reacting the ruthenium hydrido halide complex with a propargyl halide to form the ruthenium vinylcarbene complex. A method for preparing a ruthenium carbene complex includes converting a ruthenium carbene complex precursor into a ruthenium carbene complex having a structure (PR1R2R3)2Cl2Ru═CH—R4, wherein R1, R2, R3, and R4 are alike or different, and wherein covalent bonds may optionally exist between two or more of R1, R2, and R3.

    摘要翻译： 制备钌卡宾络合物前体的方法包括使钌精炼盐与卤化氢反应形成钌中间体，并使钌中间体与L型配体反应以形成钌卡宾复合物前体。 制备钌乙烯基卡巴复合物的方法包括将钌卡宾络合物前体转化为卤化钌卤化物络合物，并使卤化钌卤化物络合物与炔丙基卤反应形成钌乙烯基卡巴复合物。 制备钌卡宾络合物的方法包括将钌卡宾络合物前体转化成具有结构（PR1R2R3）2Cl2Ru=CH-R4的钌卡宾络合物，其中R 1，R 2，R 3和R 4相同或不同，并且其中共价键 可以任选地存在于R 1，R 2和R 3中的两个或多个之间。

    Monolithic electrokinetic pump fabrication
    4.
    发明授权
    Monolithic electrokinetic pump fabrication 有权
    单片电动泵制造

    公开(公告)号：US08680311B2

    公开(公告)日：2014-03-25

    申请号：US12447477

    申请日：2007-11-06

    申请人： Moon Chul Jung ,  Edouard S. P. Bouvier ,  Steven A. Cohen ,  Hua Yang

    发明人： Moon Chul Jung ,  Edouard S. P. Bouvier ,  Steven A. Cohen ,  Hua Yang

    IPC分类号： C07F7/00

    CPC分类号： F04B19/006 ,  C08G77/16 ,  C08G77/26 ,  C08G77/388 ,  C08K5/09 ,  C08K5/544 ,  C08L83/04 ,  G01N2030/326 ,  G01N2030/528

    摘要： High-pressure electrokinetic (“EK”) pumps comprising a hybrid monolith provide a high surface charge density and a continuous stable skeleton morphology with micrometer-sized through-pores. The hybrid monolith of the subject invention has superior mechanical strength and better stability in comparison to prior art monoliths with equivalent mechanical stability. The surface charge of the hybrid monolith can be modified and/or made stable by the use of different chemical reagents. The chemical reagents and resulting modification to the monolith serves to expand the usefulness of the hybrid monolith to a variety of pumping applications including chip-based systems and other applications where the ability to pump an acidic solution is required.

    摘要翻译： 包括混合整料的高压电动（“EK”）泵提供高表面电荷密度和具有微米尺寸通孔的连续稳定的骨架形态。 与具有等效机械稳定性的现有技术的整料相比，本发明的混合整料具有优异的机械强度和更好的稳定性。 可以通过使用不同的化学试剂来改变和/或制备稳定的混合整料的表面电荷。 化学试剂和对整料的所得改性用于将混合整料的有用性扩展到各种泵送应用，包括基于芯片的系统和需要泵送酸性溶液的能力的其它应用。

    METHODS FOR PREPARING RUTHENIUM CARBENE COMPLEX PRECURSORS AND RUTHENIUM VINYLCARBENE COMPLEXES
    5.
    发明申请
    METHODS FOR PREPARING RUTHENIUM CARBENE COMPLEX PRECURSORS AND RUTHENIUM VINYLCARBENE COMPLEXES 有权
    制备碳酸亚乙酯复合前体和乙烯基烯烃复合物的方法

    公开(公告)号：US20130096313A1

    公开(公告)日：2013-04-18

    申请号：US13272788

    申请日：2011-10-13

    申请人： Linda A. Kunz ,  Steven A. Cohen ,  Melvin L. Luetkens, JR.

    发明人： Linda A. Kunz ,  Steven A. Cohen ,  Melvin L. Luetkens, JR.

    IPC分类号： C07F15/00

    CPC分类号： C07F15/0046 ,  B01J31/2295 ,  C07F15/0053

    摘要： A method for preparing a ruthenium carbene complex precursor includes reacting a ruthenium refinery salt with a hydrogen halide to form a ruthenium intermediate, and reacting the ruthenium intermediate with an L-type ligand to form the ruthenium carbene complex precursor. A method for preparing a ruthenium vinylcarbene complex includes converting a ruthenium carbene complex precursor into a ruthenium hydrido halide complex, and reacting the ruthenium hydrido halide complex with a propargyl halide to form the ruthenium vinylcarbene complex. A method for preparing a ruthenium carbene complex includes converting a ruthenium carbene complex precursor into a ruthenium carbene complex having a structure (PR1R2R3)2Cl2Ru═CH—R4, wherein R1, R2, R3, and R4 are alike or different, and wherein covalent bonds may optionally exist between two or more of R1, R2, and R3.

    摘要翻译： 制备钌卡宾络合物前体的方法包括使钌精炼盐与卤化氢反应形成钌中间体，并使钌中间体与L型配体反应以形成钌卡宾复合物前体。 制备钌乙烯基卡巴复合物的方法包括将钌卡宾络合物前体转化为卤化钌卤化物络合物，并使卤化钌卤化物络合物与炔丙基卤反应形成钌乙烯基卡巴复合物。 制备钌卡宾络合物的方法包括将钌卡宾络合物前体转化成具有结构（PR1R2R3）2Cl2Ru = CH-R4的钌卡宾络合物，其中R1，R2，R3和R4是相同或不同的，其中共价键 可以任选地存在于R 1，R 2和R 3中的两个或多个之间。

    Screening apparatus with hammermill
    6.
    发明授权
    Screening apparatus with hammermill 有权
    筛分设备与锤磨机

    公开(公告)号：US07121487B2

    公开(公告)日：2006-10-17

    申请号：US10651266

    申请日：2003-08-28

    申请人： Douglas J. Cohen ,  Steven A. Cohen

    发明人： Douglas J. Cohen ,  Steven A. Cohen

    IPC分类号： B02C23/10

    CPC分类号： B07B1/005 ,  B02C13/04 ,  B02C21/02 ,  B02C23/10 ,  B07B1/22 ,  B07B13/16

    摘要： A screening machine on a frame with a hopper having a conveyor belt. The conveyor belt discharges particulate material poured into the hopper into a rotating barrel screen or vibrating planar screen for sifting the material. A hammermill apparatus is pivotably mounted on a hood member to an arm that is pivotably mounted to the frame of the machine. The hammermill is positioned above the conveyor belt at the discharge end. The hammermill can pivot upwardly relative to the arm upon striking a large object on the conveyor belt, and a spring mounted to the arm and the hood biases the hammermill back to its original position. A hydraulic ram is drivingly linked to the arm for manually or automatically displacing the hammermill relative to the conveyor belt.

    摘要翻译： 在具有输送带的料斗的框架上的筛选机。 输送带将倾倒在料斗中的颗粒材料排放到旋转的桶形筛网或振动的平面筛网中以筛选材料。 锤式装置可枢转地安装在罩构件上，臂可枢转地安装到机器的框架上。 锤击器位于输送带上方的排放端。 当撞击传送带上的大物体时，锤锤可以相对于臂向上枢转，并且安装到臂和罩的弹簧将锤马马回到其初始位置。 液压油缸与臂相互驱动连接，用于相对于传送带手动或自动地移动锤磨机。

    Methods for preparing ruthenium carbene complex precursors and ruthenium carbene complexes
    7.
    发明授权
    Methods for preparing ruthenium carbene complex precursors and ruthenium carbene complexes 有权
    制备钌卡宾络合物前体和钌卡宾络合物的方法

    公开(公告)号：US08975414B2

    公开(公告)日：2015-03-10

    申请号：US13606640

    申请日：2012-09-07

    申请人： Linda A. Kunz ,  Steven A. Cohen

    发明人： Linda A. Kunz ,  Steven A. Cohen

    IPC分类号： C07F15/00

    CPC分类号： C07F15/0053 ,  C07F15/0046

    摘要： A method for preparing a ruthenium carbene complex precursor includes reacting a ruthenium refinery salt with a hydrogen halide to form a ruthenium intermediate, and reacting the ruthenium intermediate with an L-type ligand to form the ruthenium carbene complex precursor. A method for preparing a ruthenium vinylcarbene complex includes converting a ruthenium carbene complex precursor into a ruthenium hydrido halide complex, and reacting the ruthenium hydrido halide complex with a propargyl halide to form the ruthenium vinylcarbene complex. A method for preparing a ruthenium carbene complex includes converting a ruthenium carbene complex precursor into a ruthenium carbene complex having a structure (PR1R2R3)2Cl2Ru═CH—R4, wherein R1, R2, R3, and R4 are alike or different, and wherein covalent bonds may optionally exist between two or more of R1, R2, and R3 and/or two of R1, R2, and R3 taken together may optionally form a ring with phosphorous.

    摘要翻译： 制备钌卡宾络合物前体的方法包括使钌精炼盐与卤化氢反应形成钌中间体，并使钌中间体与L型配体反应以形成钌卡宾复合物前体。 制备钌乙烯基卡巴复合物的方法包括将钌卡宾络合物前体转化为卤化钌卤化物络合物，并使卤化钌卤化物络合物与炔丙基卤反应形成钌乙烯基卡巴复合物。 制备钌卡宾络合物的方法包括将钌卡宾络合物前体转化成具有结构（PR1R2R3）2Cl2Ru=CH-R4的钌卡宾络合物，其中R 1，R 2，R 3和R 4相同或不同，并且其中共价键 可以任选地存在于R 1，R 2和R 3中的两个或多个之间，和/或R 1，R 2和R 3中的两个可以任选地与磷形成环。