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    Process for the preparation of copolymers of vinylphosphonic acid and (meth) acrylic acid in aqueous solution
    2.
    发明授权
    Process for the preparation of copolymers of vinylphosphonic acid and (meth) acrylic acid in aqueous solution 失效
    乙烯基膦酸和（甲基）丙烯酸在水溶液中的共聚物的制备方法

    公开(公告)号：US4749758A

    公开(公告)日：1988-06-07

    申请号：US858568

    申请日：1986-04-24

    申请人： Walter Dursch ,  Jurgen Grosse ,  Werner Gohla ,  Friedrich Engelhardt ,  Ulrich Riegel

    发明人： Walter Dursch ,  Jurgen Grosse ,  Werner Gohla ,  Friedrich Engelhardt ,  Ulrich Riegel

    IPC分类号： C08F2/00 ,  C08F4/32 ,  C08F30/00 ,  C08F30/02 ,  C08F220/06 ,  C08F230/02 ,  C11D3/37

    CPC分类号： C08F230/02 ,  C11D3/3784

    摘要： Process for the preparation of polymers of vinylphosphonic acid in water with the aid of catalysts which form free radicals, which comprises heating vinylphosphonic acid and (meth)acrylic acid to temperatures of 40.degree. to 120.degree. C. in water in the presence of 1 to 5.5% by weight of aliphatic peroxy esters and/or diacyl peroxides which dissociate by half in one hour at temperatures below 122.degree. C., the total amount of vinylphosphonic acid being taken together with up to 30% by weight, based on the total amount of monomer, of (meth)acrylic acid and the remainder of the (meth)acrylic acid being added in the course of the reaction.The copolymers are suitable for use in detergent and cleaning agents.

    摘要翻译： 借助于形成自由基的催化剂制备乙烯基膦酸在水中的聚合物的方法，该催化剂包括将乙烯基膦酸和（甲基）丙烯酸在40℃至120℃的温度下在1〜 5.5％（重量）脂肪族过氧酯和/或二酰基过氧化物，其在低于122℃的温度下在1小时内解离了一半，乙烯基膦酸的总量基于总量达到30重量％ 的单体，（甲基）丙烯酸，其余的（甲基）丙烯酸是在反应过程中加入的。 该共聚物适用于洗涤剂和清洁剂。

    Hydrophilic hydrogels with a high swelling capacity and method for producing and using them
    8.
    发明授权
    Hydrophilic hydrogels with a high swelling capacity and method for producing and using them 失效
    具有高溶胀能力的亲水性水凝胶及其制造和使用方法

    公开(公告)号：US06602950B1

    公开(公告)日：2003-08-05

    申请号：US09806944

    申请日：2001-04-06

    申请人： Joachim Dentler ,  Rüdiger Funk ,  Norbert Herfert ,  Mariola Wanior ,  Friedrich Engelhardt

    发明人： Joachim Dentler ,  Rüdiger Funk ,  Norbert Herfert ,  Mariola Wanior ,  Friedrich Engelhardt

    IPC分类号： A61L1524

    CPC分类号： C08F283/06 ,  A61L15/60 ,  C08F8/00 ,  C08F251/00 ,  C08F283/02 ,  Y10S524/916 ,  Y10S526/932 ,  Y10S604/904 ,  C08F283/00

    摘要： A hydrophilic, highly swellable hydrogel based on (co)polymerized monomers or based on graft (co)polymers and prepared by a) free-radically (co)polymerizing one-or more hydrophilic monomers or graft (co)polymerizing one or more hydrophilic monomers onto a grafting base, the average degree of neutralization of the acid-functional monomers being from 0 to 40 mol %, b) comminuting the acidic hydrogel, c) neutralizing the acidic hydrogel to an ultimate degree of neutralization of 50-85 mol % by adding a neutralizing agent, d) drying, grinding and sieving the hydrogel particles characterized by a centrifuge retention and a vertical absorption swell height, each having a specified minimum.value, coupled with an extractables content having a specified maximum value or a centrifuge retention and a vertical absorption swell height, each having a specified minimum value and an extractables content having a specified maximum value.

    摘要翻译： 基于（共）聚合单体或基于接枝（共）聚合物的亲水性，高度可溶胀的水凝胶，并通过自由基（共）聚合一种或多种亲水单体或将一种或多种亲水性单体接枝（共）聚合到 接枝碱，酸官能单体的平均中和度为0〜40摩尔％，b）粉碎酸性水凝胶，c）通过加入酸性水凝胶中和酸性水凝胶至50-85摩尔％的最终中和度 中和剂，d）干燥，研磨和筛分水凝胶颗粒，其特征在于离心机保留和垂直吸收膨胀高度，每个具有特定的最小值，加上具有特定最大值的可提取物含量或离心机保留和垂直吸收 每个具有指定的最小值的膨胀高度，以及具有指定的最大值的可提取物内容。

    Hydrophilic swellable graft copolymers, their preparation and use
    10.
    发明授权
    Hydrophilic swellable graft copolymers, their preparation and use 失效
    亲水性可溶胀接枝共聚物，其制备和用途

    公开(公告)号：US5011892A

    公开(公告)日：1991-04-30

    申请号：US498722

    申请日：1990-03-26

    申请人： Friedrich Engelhardt ,  Ulrich Riegel

    发明人： Friedrich Engelhardt ,  Ulrich Riegel

    IPC分类号： A61F13/53 ,  A61F13/49 ,  A61L15/60 ,  C08F283/06 ,  C08F290/06

    CPC分类号： C08F283/06 ,  A61L15/60

    摘要： The present invention relates to hydrophilic, swellable graft copolymers composed, in random distribution, of 0.5 to 20% by weight of radicals of the general formula I ##STR1## 79 to 99% by weight of radicals containing an acidic group, of the general formula II ##STR2## and 0.1 to 2% by weight of crosslinking structures which are derived from monomers having at least two olefinically unsaturated double bonds, where the radicals X, Y, R.sup.1 to R.sup.4 and n have the meanings given in claim 1, and which are used as absorbents for water and aqueous solutions.

    摘要翻译： 本发明涉及亲水性，可溶胀的接枝共聚物，其以随机分布的形式含有0.5-20％（重量）的通式Ⅰ（I）的基团为79-99％（重量）含酸性基团的基团， 衍生自具有至少两个烯属不饱和双键的单体的交联结构的通式II（II）和0.1至2重量％的交联结构，其中基团X，Y，R 1至R 4和n具有给定的含义 在权利要求1中，其用作水和水溶液的吸收剂。