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    Process and reagent useful for the synthesis of sulphanilide which is perhalogenated on the carbon borne by the sulphur atom of the sulphanilide function
    1.
    发明申请
    Process and reagent useful for the synthesis of sulphanilide which is perhalogenated on the carbon borne by the sulphur atom of the sulphanilide function 有权
    用于合成磺酰苯胺的方法和试剂，其在硫酰胺功能的硫原子上承载的碳上是全卤代的

    公开(公告)号：US20010020113A1

    公开(公告)日：2001-09-06

    申请号：US09859016

    申请日：2001-05-15

    发明人： Jean-Roger Desmurs ,  Andre Millet ,  Virginie Pevere

    IPC分类号： C07C37/02

    CPC分类号： C07B45/00 ,  C07C303/38 ,  C07C311/09

    摘要： The present invention relates to a process and a reagent useful for the synthesis of sulphanilide which is perhalogenated on the carbon borne by the sulphur atom of the sulphanilide function. This persulphonylation process is characterized in that it comprises a step of placing a nucleophile, whose nucleophilic atom is a nitrogen, in contact with a reagent comprising, for successive or simultaneous addition, a heavy halide of sulphonyl, advantageously sulphonyl chloride, and an organic base comprising a trivalent atom from column V whose lone pair is conjugated directly or indirectly to a bond, and in that the organic part of the said sulphonyl is perhalogenated, advantageously perfluorinated, on the carbon borne by the sulphur. Application to the synthesis of intermediates for organic chemistry.

    摘要翻译： 本发明涉及可用于合成磺酰苯胺的方法和试剂，其在由硫化物酰亚胺功能的硫原子承载的碳上过卤化。 该磺酰化方法的特征在于其包括将亲核原子为氮的亲核试剂置于与试剂接触的步骤中，所述试剂包括连续或同时加入磺酰卤的重卤化物，有利地为磺酰氯和有机碱 其包含来自第V列的三价原子，其双对直接或间接结合到键上，并且所述磺酰基的有机部分在由硫承载的碳上被全卤化，有利地全氟化。 应用于有机化学中间体的合成。

    Process and reagent useful for the synthesis of sulphanilide which is perhalogenated on the carbon borne by the sulphur atom of the sulphanilide function
    10.
    发明授权
    Process and reagent useful for the synthesis of sulphanilide which is perhalogenated on the carbon borne by the sulphur atom of the sulphanilide function 有权
    用于合成磺酰苯胺的方法和试剂，其在硫酰胺功能的硫原子上承载的碳上是全卤代的

    公开(公告)号：US06399820B2

    公开(公告)日：2002-06-04

    申请号：US09859016

    申请日：2001-05-15

    申请人： Jean-Roger Desmurs ,  Andr{dot over (e)} Millet ,  Virginie Pevere

    发明人： Jean-Roger Desmurs ,  Andr{dot over (e)} Millet ,  Virginie Pevere

    IPC分类号： C07C30318

    CPC分类号： C07B45/00 ,  C07C303/38 ,  C07C311/09

    摘要： The present invention relates to a process and a reagent useful for the synthesis of sulphanilide which is perhalogenated on the carbon borne by the sulphur atom of the sulphanilide function. This persulphonylation process is characterized in that it comprises a step of placing a nucleophile, whose nucleophilic atom is a nitrogen, in contact with a reagent comprising, for successive or simultaneous addition, a heavy halide of sulphonyl, advantageously sulphonyl chloride, and an organic base comprising a trivalent atom from column V whose lone pair is conjugated directly or indirectly to a bond, and in that the organic part of the said sulphonyl is perhalogenated, advantageously perfluorinated, on the carbon borne by the sulphur. Application to the synthesis of intermediates for organic chemistry.

    摘要翻译： 本发明涉及可用于合成磺酰苯胺的方法和试剂，其在由硫化物酰亚胺功能的硫原子承载的碳上过卤化。 该磺酰化方法的特征在于其包括将亲核原子为氮的亲核试剂置于与试剂接触的步骤中，所述试剂包括连续或同时加入磺酰卤的重卤化物，有利地为磺酰氯和有机碱 其包含来自第V列的三价原子，其双对直接或间接结合到键上，并且所述磺酰基的有机部分在由硫承载的碳上被全卤化，有利地全氟化。 应用于有机化学中间体的合成。