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    2-Fluoro-2-cyanoethenyl cyclopropane carboxylates as pesticides
    8.
    发明授权
    2-Fluoro-2-cyanoethenyl cyclopropane carboxylates as pesticides 失效
    2-氟-2-氰基乙烯基环丙烷羧酸酯作为农药

    公开(公告)号：US4565822A

    公开(公告)日：1986-01-21

    申请号：US637106

    申请日：1984-08-02

    申请人： Jean Tessier ,  Andre Teche ,  Pierre Girault

    发明人： Jean Tessier ,  Andre Teche ,  Pierre Girault

    IPC分类号： C07D233/70 ,  A01N43/40 ,  A01N53/00 ,  A01N53/02 ,  A01N53/04 ,  A01N53/08 ,  A01P7/04 ,  A23K1/16 ,  A61K31/275 ,  C07C67/00 ,  C07C253/00 ,  C07C253/30 ,  C07C255/31 ,  C07C255/39 ,  C07C255/53 ,  C07D213/57 ,  C07D213/64 ,  C07D213/647 ,  C07D233/72 ,  C07D233/74 ,  C07D307/45 ,  C07F3/10 ,  C07F3/12 ,  C07D213/65 ,  C07C121/48

    CPC分类号： C07D213/647 ,  A01N53/00 ,  C07C255/00 ,  C07D233/72 ,  C07F3/10 ,  C07F3/12

    摘要： Novel cyclopropanecarboxylates in all possible isomeric forms or mixtures thereof of the formula ##STR1## with a 1R,cis or 1R,trans structure and wherein X is a halogen, R is selected from the group consisting of (A) optionally unsaturated alkyl of 2 to 12 carbon atoms, (B) optionally unsaturated cycloalkyl of 3 to 12 carbon atoms, (c) ##STR2## Z is selected from the group consisting of --C.tbd.CH, --CH.sub.3 and --CN and Ar is selected from the group consisting of --C.sub.6 H.sub.5, --C.sub.6 F.sub.5, ##STR3## B is hydrogen or fluorine and X is fluorine, chlorine or bromine ##STR4## Y.sub.2 is selected from the group consisting of hydrogen, fluorine, chlorine bromine, --C.tbd.N and --C.tbd.CH, Y.sub.3, Y.sub.4, and Y.sub.5 are individually selected from the group consisting of hydrogen, fluorine, chlorine, bromine alkyl of 1 to 8 carbon atoms and cycloalkyl of 3 to 8 carbon atoms optionally substituted by one or more functional groups, alkenyl of 2 to 8 carbon atoms and alkynyl of 2 to 8 carbon atoms, and two of Y.sub.3, Y.sub.4 and Y.sub.5 can form rings between them with the proviso that if X is bromine and R is ##STR5## and Z is cyano or ethynyl and A.sub.r is ##STR6## the carbon carrying Z is in the (S) configuration and the double bond in the 3-side chain may have E or Z structure useful in combatting pests such as insects, nematodes acarids.

    摘要翻译： 新型环丙烷羧酸酯，其具有1R，顺式或1R，反式结构的所有可能的异构形式或其混合物，其中X为卤素，R选自（A）任选不饱和的2位烷基 至12个碳原子，（B）任选的3至12个碳原子的不饱和环烷基，（c）Z选自-C 3 CH 2，-CH 3和-CN，Ar选自 （D）图像（E）和图像（F），其中，C 6 H 5，-C 6 F 5， Y2选自氢，氟，氯溴，-C 3位N和-C 3位CH，Y 3，Y 4和Y 5分别选自氢，氟，氯，溴烷基1至 8个碳原子和3至8个碳原子的环烷基，任选被一个或多个官能团取代，2至8个碳原子的烯基和2个炔基的炔基 至8个碳原子，并且Y 3，Y 4和Y 5中的两个可以在它们之间形成环，条件是如果X是溴且R是“Z”，Z是氰基或乙炔基，Ar是“ 3侧链中的（S）构型和双键可以具有用于对抗昆虫，线虫螨等害虫的E或Z结构。

    Process for producing 6-phenoxypicolinic aldehydes
    10.
    发明授权
    Process for producing 6-phenoxypicolinic aldehydes 失效
    6-苯氧基吡啶醛的制备方法

    公开(公告)号：US4393213A

    公开(公告)日：1983-07-12

    申请号：US315228

    申请日：1981-10-26

    申请人： Kiyomi Ozawa ,  Shigeru Ishii

    发明人： Kiyomi Ozawa ,  Shigeru Ishii

    IPC分类号： A01N43/40 ,  A01N53/00 ,  C07D213/64 ,  C07D213/643 ,  C07D213/647

    CPC分类号： C07D213/643 ,  A01N43/40 ,  A01N53/00 ,  C07D213/647

    摘要： A process for producing 6-phenoxypicolinic aldehydes, which comprises reacting a 2-halogeno-6-phenoxypyridine represented by the general formula I: ##STR1## where X is a halogen atom, Y is independently an alkyl group of 1 to 4 carbon atoms, an alkoxy group of 1 to 4 carbon atoms, an alkoxy group of 1 to 4 carbon atoms substituted by a halogen atom, an alkylthio group of 1 to 4 carbon atoms, a trifluoromethyl group, a fluorine atom or a chlorine atom, Z is a hydrogen atom or a fluorine atom, and n is an integer of 0 to 2, with magnesium metal, and then with a formylating reagent. These compounds are used as intermediates for the synthesis of insecticides.

    摘要翻译： 一种生产6-苯氧基吡啶甲醛的方法，其包括使通式I表示的2-卤代-6-苯氧基吡啶与其中X为卤素原子的Y反应，Y独立地为1至4个碳原子的烷基 ，1〜4个碳原子的烷氧基，1〜4个碳原子被卤素原子取代的烷氧基，1〜4个碳原子的烷硫基，三氟甲基，氟原子或氯原子，Z为 氢原子或氟原子，n为0〜2的整数，与金属镁反应，然后与甲酰化试剂反应。 这些化合物用作合成杀虫剂的中间体。