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    Templated native silk smectic gel
    3.
    发明专利
    Templated native silk smectic gel 有权
    模塑原丝绸SMECTIC GEL

    公开(公告)号：JP2011202170A

    公开(公告)日：2011-10-13

    申请号：JP2011106360

    申请日：2011-05-11

    申请人： Trustees Of Tufts College ,  トラスティーズ オブ タフツ カレッジTrustees Of Tufts College

    发明人： VALLUZZI REGINA ,  JIN HYOUNG-JOON ,  PARK JAEHYUNG

    IPC分类号： C08H1/00 ,  A61K38/17 ,  C07K20060101 ,  C07K14/435 ,  C07K14/78

    CPC分类号： A61K47/42 ,  C07K14/43586 ,  Y10T436/25375

    摘要： PROBLEM TO BE SOLVED: To provide a method of preparing a fibrous protein smectic hydrogel by way of a solvent templating process.SOLUTION: The method includes the steps of: pouring a fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; and collecting the resulting fibrous protein smectic hydrogel and allowing it to dry. A method of obtaining predominantly one enantiomer from a racemic mixture includes, in addition to the above steps up to allowing the container to age, steps of: allowing the enantiomers of racemic mixture to diffuse selectively into the smectic hydrogel in solution; removing the smectic hydrogel from the solution; rinsing the predominantly one enantiomer from the surface of the smectic hydrogel; and extracting the predominantly one enantiomer from the interior of the smectic hydrogel.

    摘要翻译： 要解决的问题：提供通过溶剂模板法制备纤维状蛋白质近水晶凝胶的方法。方法：该方法包括以下步骤：将纤维蛋白溶液倒入容器中，该容器包含不与水混溶的溶剂 ; 密封容器并使其在约室温下老化; 并收集所得到的纤维蛋白质近晶凝胶并使其干燥。 从外消旋混合物主要获得一种对映异构体的方法除了上述步骤以至允许容器老化之外，还包括以下步骤：使外消旋混合物的对映异构体选择性扩散到溶液中的近晶水凝胶中; 从溶液中除去近晶凝胶; 从近晶水凝胶的表面漂洗主要是一种对映异构体; 并从近晶水凝胶的内部提取主要的一种对映异构体。