Mesoporous nano-crystalline titania structures for hydrogen sensing
    96.
    发明授权
    Mesoporous nano-crystalline titania structures for hydrogen sensing 失效
    用于氢感测的介孔纳米结晶二氧化钛结构

    公开(公告)号:US07833483B2

    公开(公告)日:2010-11-16

    申请号:US11777305

    申请日:2007-07-13

    IPC分类号: G01N27/00

    摘要: A structure includes a substantially non-conductive frame having an exterior surface. The structure defines a plurality of passages that open to the exterior surface. Mesoporous material is disposed in the plurality of passages and is supported therein by the frame. In a method for making a mesoporous nanocrystalline titania hybrid material, a templating agent, an acid, and a titania precursor is mixed into a template liquid. A frame that defines a plurality of passages is placed into the template liquid. A solvent is evaporated from the template liquid, thereby forming a titania gel encapsulating the templating agent. The gel is heated to remove substantially the templating agent from the non-conductive frame and the titania, thereby leaving a mesoporous titania material.

    摘要翻译: 一种结构包括具有外表面的基本不导电的框架。 该结构限定了多个通向外表面的通道。 介孔材料设置在多个通道中并被框架支撑在其中。 在制备介孔纳米晶二氧化钛混合材料的方法中,将模板剂,酸和二氧化钛前体混合到模板液中。 将限定多个通道的框架放置在模板液体中。 从模板液中蒸发溶剂,从而形成包封模板剂的二氧化钛凝胶。 将凝胶加热以从非导电性框架和二氧化钛基本上除去模板剂,从而留下介孔二氧化钛材料。