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    Emulsion polymers
    11.
    发明授权
    Emulsion polymers 失效
    乳液聚合物

    公开(公告)号：US4904727A

    公开(公告)日：1990-02-27

    申请号：US318045

    申请日：1989-03-02

    Applicant: Joachim Probst ,  Wolfgang Henning ,  Heinz Baumgen ,  Joachim Konig

    Inventor： Joachim Probst ,  Wolfgang Henning ,  Heinz Baumgen ,  Joachim Konig

    IPC: B01F17/52 ,  C08F2/28 ,  D21H17/28 ,  D21H17/35 ,  D21H17/37 ,  D21H17/57

    CPC classification number: D21H17/57 ,  C08F2/28 ,  D21H17/28 ,  D21H17/35 ,  D21H17/37

    Abstract: Emulsion polymers obtained by emulsifying a monomer mixture of(A) 5-95% by weight of acrylonitrile, methacrylonitrile and/or substituted or unsubstituted styrene and(B) 5-95% by weight of acrylic and/or methacrylic acid esters containing 1-12 carbon atoms in the alcohol group,the sum of components (A)+(B) amounting to 100% by weight, in the presence of an aqueous solution or dispersion of a water soluble or water dispersible, cationically modified polyurethane, and subjecting the resulting emulsion to a radically initiated polymerization. The emulsion polymers are preferably used as paper sizes or in paper sizes together with conventional additives.

    Abstract translation: 通过将（A）5-95重量％的丙烯腈，甲基丙烯腈和/或取代或未取代的苯乙烯和（B）5-95重量％的丙烯酸和/或甲基丙烯酸酯的单体混合物乳化而得到的乳液聚合物， 醇基中的12个碳原子，在水溶液或水分散性阳离子改性聚氨酯的水溶液或分散体的存在下，组分（A）+（B）的总和为100重量％，并对 所得乳液进行自由基引发的聚合。 乳液聚合物优选与纸张尺寸或纸张尺寸一起用于常规添加剂。

    Process for the production of new polyisocyanate compositions and their use for the production of plastics by the isocyanate polyaddition process
    12.
    发明授权
    Process for the production of new polyisocyanate compositions and their use for the production of plastics by the isocyanate polyaddition process 失效
    用于生产新型多异氰酸酯组合物的方法及其通过异氰酸酯加聚方法生产塑料的用途

    公开(公告)号：US4732960A

    公开(公告)日：1988-03-22

    申请号：US818926

    申请日：1986-01-15

    Applicant: Werner Rasshofer ,  Reiner Paul ,  Joachim Probst

    Inventor： Werner Rasshofer ,  Reiner Paul ,  Joachim Probst

    IPC: C08G18/00 ,  C08G18/10 ,  C08G18/12 ,  C08G18/62 ,  C08G18/67

    CPC classification number: C08G18/6254 ,  C08G18/10 ,  C08G18/12 ,  C08G18/6229 ,  C08G2101/0008 ,  C08G2101/0016 ,  C08G2101/0025 ,  C08G2101/0033 ,  C08G2101/0066 ,  C08G2120/00

    Abstract: The present invention relates to a process for the production of polyisocyanate compositions containing urethane groups and having an isocyanate content of about 0.5 to 45% by weight by the reaction of(a) an organic polyisocyanate or mixtures thereof having an isocyanate content of about 30 to 50% by weight with(b) organic polyhydroxyl compounds using an equivalent ratio of isocyanate groups to hydroxyl groups of at least 1.8:1, characterized in that the polyhydroxyl compounds (b) are based on(b1) polyhydroxypolyacrylates having an average molecular weight, determined by vapor pressure osmometry, of 232 to about 100,000 which optionally contain urethane or ester groups in side chains, and a statistical average of at least one alcoholic hydroxyl group per molecule(b2) optionally in admixture with up to about 250% by weight, based on (b1), of other polyhydroxyl compounds in the molecular weight range of 62 to about 12,000.The invention also relates to the polyisocyanate compositions obtainable by this process and their use as components for the production of polyurethanes or polyurethane ureas.

    Abstract translation: 本发明涉及通过（a）有机多异氰酸酯或其混合物与异氰酸酯含量为约30的反应制备含有氨基甲酸酯基团并具有约0.5至45重量％的异氰酸酯含量的多异氰酸酯组合物的方法， 50重量％与（b）异氰酸酯基与羟基的当量比至少为1.8:1的有机多羟基化合物，其特征在于多羟基化合物（b）基于（b1）具有平均分子量的聚羟基聚丙烯酸酯， 通过蒸汽压力渗透压测定，为232至约100,000，其任选地在侧链中含有氨基甲酸酯或酯基，以及每分子至少一个醇羟基（b2）的统计平均值，任选地与至多约250重量％ 基于（b1）的分子量范围为62至约12,000的其它多羟基化合物。 本发明还涉及通过该方法获得的多异氰酸酯组合物及其作为生产聚氨酯或聚氨酯脲的组分的用途。

    Polyquaternary ammonium compounds, their preparation, their use in the production of paper and paper treatment agents containing them
    13.
    发明授权
    Polyquaternary ammonium compounds, their preparation, their use in the production of paper and paper treatment agents containing them 失效
    聚季铵化合物，其制备方法，用于生产包含它们的纸张和纸张处理剂

    公开(公告)号：US4423194A

    公开(公告)日：1983-12-27

    申请号：US410744

    申请日：1982-08-23

    Applicant: Wilfried Lobach ,  Peter Haas ,  Gunter Kolb ,  Guter Sackmann ,  Joachim Probst

    Inventor： Wilfried Lobach ,  Peter Haas ,  Gunter Kolb ,  Guter Sackmann ,  Joachim Probst

    IPC: C08F8/00 ,  C08F8/02 ,  C08F8/18 ,  C08F8/32 ,  C08F8/34 ,  C08F8/44 ,  D21H17/37

    CPC classification number: C08F8/44

    Abstract: The present invention relates to new water-soluble polyquaternary compounds which are obtained by imidation of (A) specific alternating copolymers of maleic anhydride and olefines with (B) specific amines and (C) subsequent alkylation of the reaction product AB, the components (A) and (B) having the meaning given in the text of the Application. The invention furthermore relates to a process for the preparation of these water-soluble polyammonium compounds and their use as agents for improving the wet and dry tear strength of paper. The invention also relates to new intermediate products for the preparation of the compounds according to the invention.

    Abstract translation: 本发明涉及通过（A）马来酸酐和烯烃与（B）特定胺的特定交替共聚物的酰亚胺化和（C）随后的反应产物AB，组分（A）的烷基化而得到的新的水溶性聚季铵化合物 ）和（B）具有本申请文本中给出的含义。 本发明还涉及一种制备这些水溶性多铵化合物的方法及其用作改善纸的湿和干撕裂强度的试剂。 本发明还涉及用于制备本发明化合物的新的中间产物。

    Cationic sizing agents for paper
    14.
    发明授权
    Cationic sizing agents for paper 失效
    阳离子上胶剂纸

    公开(公告)号：US4418175A

    公开(公告)日：1983-11-29

    申请号：US329721

    申请日：1981-12-11

    Applicant: Joachim Probst ,  Gunter Kolb ,  Friedhelm Muller ,  Heinz Baumgen

    Inventor： Joachim Probst ,  Gunter Kolb ,  Friedhelm Muller ,  Heinz Baumgen

    IPC: D21H19/20 ,  C08F8/44 ,  D21H17/35 ,  D21H17/37 ,  D21H17/45 ,  C08F220/46

    CPC classification number: D21H17/455 ,  C08F8/44 ,  D21H17/35 ,  D21H17/37

    Abstract: The aqueous solution of a statistical terpolymer containing quaternized amino groups and having a regular chemical structure of(a) from 8 to 20%, by weight, of N,N-dimethylaminoethyl acrylate and/or N,N-dimethylaminoethyl methacrylate;(b) from 45 to 80%, by weight, of styrene; and(c) from 8 to 35%, by weight, of acrylonitrile;the sum of (a) to (c) being 100%, by weight, and at least 10% of the dimethylamino groups of the terpolymer being quaternized and the remainder protonated is suitable as cationic paper sizing agent.

    Abstract translation: 具有季铵化氨基的统计三元共聚物的水溶液，其具有规则的化学结构（a）8至20重量％的丙烯酸N，N-二甲基氨基乙酯和/或甲基丙烯酸N，N-二甲基氨基乙酯; （b）45〜80重量％的苯乙烯; 和（c）8至35重量％的丙烯腈; （a）至（c）的总和为100重量％，并且至少10％的三元共聚物的二甲基氨基被季铵化，其余被质子化适合作为阳离子纸上胶剂。

    Low molecular weight acrylate resins containing hydroxyl and tertiary amino groups
    15.
    发明授权
    Low molecular weight acrylate resins containing hydroxyl and tertiary amino groups 失效
    含有羟基和叔氨基的低分子量丙烯酸酯树脂

    公开(公告)号：US4293661A

    公开(公告)日：1981-10-06

    申请号：US108349

    申请日：1979-12-31

    Applicant: Joachim Probst ,  Michael Sonntag ,  Gunter Kolb

    Inventor： Joachim Probst ,  Michael Sonntag ,  Gunter Kolb

    IPC: C08F8/00 ,  C08F8/32 ,  C08G18/00 ,  C08G18/62 ,  C08G59/12 ,  C08G59/14 ,  C09D175/04 ,  C08F8/08

    CPC classification number: C08G18/6237 ,  C08F8/32 ,  C08F2800/20

    Abstract: A reaction product of an acrylate resin containing glycidyl groups and secondary mono-amines containing hydroxyl groups, obtained by reacting of said acrylate resin of copolymerized, statistically distributed units of(A) 3 to 30% by weight of the glycidyl ester of (meth)acrylic acid and/or of vinyl glycidyl ether;(B) 0 to 20% by weight of at least a hydroxy C.sub.2 -C.sub.4 alkyl ester of (meth)acrylic acid;(C) 5 to 80% by weight of at least an optionally substituted styrene, methyl methacrylate, (meth)acrylonitrile or any mixture thereof;(D) 5 to 70% by weight of an acrylic acid C.sub.1 -C.sub.12 -alkyl-or of a methacrylic acid C.sub.2 -C.sub.12 -alkyl ester or any mixture thereof; and(E) 0 to 10% by weight of an .alpha.,.beta.-mono-olefinically unsaturated monocarboxylic or dicarboxylic acid containing from 3 to 5 carbon atoms or of a maleic acid C.sub.2 -C.sub.14 -mono ester or any mixture thereof,with at least one secondary mono-amine containing at least one secondary hydroxyl group. The reaction products are useful for crosslinking polyisocyanates.

    Abstract translation: 由（A）3〜30重量％的（甲基）丙烯酸缩水甘油酯的共聚统计分布单位的所述丙烯酸酯树脂与所述含有缩水甘油基的丙烯酸酯树脂和含有羟基的二次一元胺反应， 丙烯酸和/或乙烯基缩水甘油醚; （B）0〜20重量％的（甲基）丙烯酸的至少羟基C 2 -C 4烷基酯; （C）5至80重量％的至少任选取代的苯乙烯，甲基丙烯酸甲酯，（甲基）丙烯腈或其任何混合物; （D）5-70重量％的丙烯酸C 1 -C 12烷基或甲基丙烯酸C 2 -C 12烷基酯或其任何混合物; 和（E）0至10重量％的含有3至5个碳原子的α，β-单烯属不饱和单羧酸或二羧酸或马来酸C2-C14-单酯或其任何混合物，至少具有 一个含有至少一个仲羟基的二次单胺。 反应产物可用于交联多异氰酸酯。

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