公开(公告)号：US20170037688A1

公开(公告)日：2017-02-09

申请号：US15297882

申请日：2016-10-19

Applicant: Baker Hughes Incorporated

Inventor： Valery N. Khabashesku ,  Vladimir P. Filonenko

IPC: E21B10/567 ,  B24D3/06 ,  B24D18/00

CPC classification number: E21B10/567 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/0685 ,  B24D3/06 ,  B24D18/0009

Abstract: A polycrystalline compact includes diamond, cubic boron nitride, and at least one hard material, which may be aluminum nitride, gallium nitride, silicon nitride, titanium nitride, silicon carbide, titanium carbide, titanium boride, titanium diboride, and/or aluminum boride. The diamond, the cubic boron nitride, and the hard material are intermixed and interbonded to form a polycrystalline material. An earth-boring tool includes a bit body and a polycrystalline diamond compact secured to the bit body. Methods of fabricating polycrystalline compacts include forming a mixture comprising diamond, non-cubic boron nitride, and a metal or semimetal; encapsulating the mixture in a container; and subjecting the encapsulated mixture to high-pressure and high-temperature conditions to form a polycrystalline material.

Abstract translation: 多晶结构体包括金刚石，立方氮化硼和至少一种硬质材料，其可以是氮化铝，氮化镓，氮化硅，氮化钛，碳化硅，碳化钛，硼化钛，二硼化钛和/或硼化铝。 将金刚石，立方氮化硼和硬质材料混合并键合以形成多晶材料。 钻孔工具包括固定在钻头体上的钻头体和多晶金刚石块。 制造多晶压块的方法包括形成包含金刚石，非立方氮化硼和金属或半金属的混合物; 将混合物包封在容器中; 并将包封的混合物经受高压和高温条件以形成多晶材料。

公开(公告)号：US09487446B2

公开(公告)日：2016-11-08

申请号：US14650173

申请日：2013-12-05

Applicant: Sumitomo Electric Industries, Ltd.

Inventor： Takeshi Sato ,  Katsuko Yamamoto ,  Kazuhiro Ikeda ,  Hitoshi Sumiya

IPC: C01B31/06 ,  C04B35/52 ,  B21C3/02 ,  C23C14/34 ,  C23C14/06 ,  C04B35/626 ,  B01J3/06 ,  C04B35/645

CPC classification number: C04B35/52 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068 ,  B01J2203/0685 ,  B21C3/025 ,  B22F2005/002 ,  C01B32/25 ,  C04B35/6261 ,  C04B35/6281 ,  C04B35/62826 ,  C04B35/62831 ,  C04B35/62842 ,  C04B35/62884 ,  C04B35/645 ,  C04B2235/3201 ,  C04B2235/3213 ,  C04B2235/3272 ,  C04B2235/3281 ,  C04B2235/3291 ,  C04B2235/40 ,  C04B2235/401 ,  C04B2235/405 ,  C04B2235/407 ,  C04B2235/408 ,  C04B2235/425 ,  C04B2235/427 ,  C04B2235/444 ,  C04B2235/446 ,  C04B2235/5445 ,  C04B2235/725 ,  C04B2235/785 ,  C22C1/053 ,  C22C26/00 ,  C23C14/0611 ,  C23C14/34

Abstract: Provided are a diamond polycrystalline body having a longer life than conventional diamond polycrystalline bodies when it is slid, a method for manufacturing the same, and a tool. In a diamond polycrystalline body, at least one element whose sulfide or chloride has a melting point of less than or equal to 1000° C. is added thereto, and crystal grains have an average grain size of less than or equal to 500 nm. Thereby, wear of diamond can be suppressed, and the diamond polycrystalline body can have a longer life when it is slid.

Abstract translation: 提供一种金刚石多晶体，其在滑动时具有比常规金刚石多晶体更长的寿命，其制造方法和工具。 在金刚石多晶体中，向其中加入硫化物或氯化物的熔点小于或等于1000℃的至少一种元素，晶粒的平均粒径小于或等于500nm。 因此，可以抑制金刚石的磨损，并且金刚石多晶体在滑动时具有更长的寿命。

公开(公告)号：US20160264422A1

公开(公告)日：2016-09-15

申请号：US15163298

申请日：2016-05-24

Applicant: Sumitomo Electric Industries, Ltd.

Inventor： Kazuhiro Ikeda ,  Keiko Arimoto ,  Katsuko Yamamoto ,  Hitoshi Sumiya ,  Takeshi Sato

IPC: C01B31/06

CPC classification number: C04B35/52 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/0655 ,  C01B32/25 ,  C04B2235/42 ,  C04B2235/427 ,  Y10T428/2982

Abstract: Nano polycrystalline diamond is composed of carbon, an element of different type which is an element other than carbon and is added to be dispersed in carbon at an atomic level, and an inevitable impurity. The polycrystalline diamond has a crystal grain size not greater than 500 nm. The polycrystalline diamond can be fabricated by subjecting graphite in which the element of different type which is an element other than carbon has been added to be dispersed in carbon at an atomic level to heat treatment within high-pressure press equipment.

Abstract translation: 纳米多晶金刚石由碳，作为除碳以外的元素的不同类型的元素组成，并且以碳原子级加入并且不可避免的杂质。 多晶金刚石的晶粒尺寸不大于500nm。 多晶金刚石可以通过将其中已经加入作为碳以外的元素的不同类型的元素以原子级分散在碳中的石墨制成，以在高压压制设备中进行热处理。

公开(公告)号：US20160159693A1

公开(公告)日：2016-06-09

申请号：US15017992

申请日：2016-02-08

Applicant: John Hewitt LIVERSAGE ,  Iain Patrick GOUDEMOND ,  Danny Eugene SCOTT

Inventor： John Hewitt LIVERSAGE ,  Iain Patrick GOUDEMOND ,  Danny Eugene SCOTT

IPC: C04B35/528 ,  B32B18/00

CPC classification number: C04B35/528 ,  B01J3/065 ,  B01J2203/0655 ,  B22F7/062 ,  B32B18/00 ,  C04B35/52 ,  C04B35/573 ,  C04B35/645 ,  C04B37/021 ,  C04B37/026 ,  C04B2235/427 ,  C04B2237/083 ,  C04B2237/122 ,  C04B2237/123 ,  C04B2237/16 ,  C04B2237/363 ,  C04B2237/365 ,  C04B2237/704 ,  C22C26/00 ,  C22C2204/00 ,  Y10T156/10 ,  Y10T428/30

Abstract: A polycrystalline diamond (PCD) compact and method for making the compact are provided. The method includes bringing a first PCD wafer and a second PCD wafer together at an interface in the presence of a bonding agent to form an unbonded assembly and bonding the wafers together at the interface at a pressure and temperature at which diamond is thermodynamically stable. The first PCD wafer is more thermally stable than the second PCD wafer.

Abstract translation: 提供了一种多晶金刚石（PCD）紧凑型及其制造方法。 该方法包括在存在粘合剂的情况下将界面处的第一PCD晶片和第二PCD晶片组合在一起以形成未结合的组件，并且在金刚石在热力学稳定的压力和温度下在界面处将晶片粘合在一起。 第一PCD晶片比第二PCD晶片更热稳定。

公开(公告)号：US20160136785A1

公开(公告)日：2016-05-19

申请号：US15005765

申请日：2016-01-25

Applicant: US SYNTHETIC CORPORATION

Inventor： Debkumar Mukhopadhyay ,  Jair J. Gonzalez

IPC: B24D3/06 ,  B24D18/00 ,  E21B10/56

CPC classification number: B24D3/06 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D18/0009 ,  B24D99/005 ,  C04B35/528 ,  E21B10/46 ,  E21B10/56

Abstract: Embodiments relate to polycrystalline diamond compacts (“PDCs”) and methods of manufacturing such PDCs in which an at least partially leached polycrystalline diamond (“PCD”) table is infiltrated with a low viscosity cobalt-based alloy infiltrant. In an embodiment, a method includes forming a PCD table in the presence of a metal-solvent catalyst in a first high-pressure/high-temperature (“HPHT”) process. The method includes at least partially leaching the PCD table to remove at least a portion of the metal-solvent catalyst therefrom to form an at least partially leached PCD table. The method includes subjecting the at least partially leached PCD table and a substrate to a second HPHT process effective to at least partially infiltrate the at least partially leached PCD table with a cobalt-based alloy infiltrant having a composition at or near a eutectic composition of the cobalt-based alloy infiltrant.

Abstract translation: 实施例涉及多晶金刚石压块（“PDC”）以及制造这样的PDC的方法，其中至少部分浸出的多晶金刚石（“PCD”）工作台用低粘度钴基合金渗透剂渗透。 在一个实施方案中，一种方法包括在第一高压/高温（“HPHT”）方法中在金属溶剂催化剂存在下形成PCD表。 该方法包括至少部分浸出PCD表以从其中除去至少一部分金属 - 溶剂催化剂以形成至少部分浸出的PCD台。 该方法包括使至少部分浸出的PCD台和基板经受有效的至少部分浸渗的PCD台的第二HPHT方法，所述第二HPHT工艺具有钴基合金浸渗剂，所述钴基合金浸渗剂具有或接近共晶组成 钴基合金浸润剂。

公开(公告)号：US09302236B2

公开(公告)日：2016-04-05

申请号：US13622530

申请日：2012-09-19

Applicant: Baker Hughes Incorporated

Inventor： Anthony A. DiGiovanni ,  Danny E. Scott

IPC: B01J3/06 ,  B24D3/14 ,  B24D18/00 ,  B24D99/00 ,  E21B10/567

CPC classification number: B24D18/0009 ,  B01J3/062 ,  B01J3/067 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D3/14 ,  B24D99/005 ,  E21B10/55 ,  E21B10/567

Abstract: Methods for forming cutting elements comprising polycrystalline materials, methods for forming polycrystalline compacts for cutting elements of a drilling tool, methods for forming polycrystalline diamond compacts, and resulting polycrystalline compacts and cutting elements are disclosed. Grains of a hard material are introduced to a press and subjected to a high-pressure, high-temperature (HPHT) process to sinter the grains. The system conditions (i.e., temperature and pressure) are then adjusted past a phase or state change point, after which, at least one of the system conditions is held during an anneal stage before the system conditions are adjusted to final levels. The resulting compacts and cutting elements may therefore include inter-granularly bonded hard material grains with a more stable microstructure (e.g., less stressed microstructure) than a polycrystalline compact and cutting element formed without an anneal stage during the HPHT process.

Abstract translation: 公开了用于形成包括多晶材料的切割元件的方法，用于形成用于切割钻孔工具的元件的多晶压块的方法，用于形成多晶金刚石压块的方法，以及所得到的多晶压块和切割元件。 将硬质材料的颗粒引入压机中并进行高压高温（HPHT）工艺以烧结晶粒。 然后将系统条件（即，温度和压力）调整到相位或状态变化点之后，在将系统条件调整到最终水平之前，在退火阶段期间保持至少一个系统条件。 因此，所形成的压块和切割元件可以包括与在HPHT处理期间不具有退火阶段形成的多晶压块和切割元件相比，具有更稳定的微结构（例如，较不受应力的微结构）的颗粒间结合的硬质材料颗粒。

公开(公告)号：US09249054B2

公开(公告)日：2016-02-02

申请号：US14009453

申请日：2012-04-05

Applicant: Mark Gregory Munday ,  Charles Stephan Montross

Inventor： Mark Gregory Munday ,  Charles Stephan Montross

IPC: C04B33/00 ,  C04B33/13 ,  B01J3/06 ,  B30B11/00 ,  C04B33/04 ,  C04B35/185 ,  C04B35/20 ,  C04B35/63 ,  C04B35/645

CPC classification number: C04B33/13 ,  B01J3/065 ,  B01J3/067 ,  B01J2203/0655 ,  B01J2203/066 ,  B30B11/004 ,  C04B33/04 ,  C04B35/185 ,  C04B35/20 ,  C04B35/6303 ,  C04B35/6316 ,  C04B35/645 ,  C04B2235/3418 ,  C04B2235/3463 ,  C04B2235/349 ,  C04B2235/36 ,  C04B2235/604 ,  C04B2235/80

Abstract: A containment element for a pressure containment assembly, comprising mullite or a polymorph of mullite.

Abstract translation: 一种用于压力容纳组件的容纳元件，包括莫来石或莫来石的多晶型物。

公开(公告)号：US09238875B2

公开(公告)日：2016-01-19

申请号：US12929567

申请日：2011-02-01

Applicant: Hexiang Zhu ,  Karl Pearson ,  Joo Ro Kim

Inventor： Hexiang Zhu ,  Karl Pearson ,  Joo Ro Kim

IPC: C30B29/04 ,  B01J3/06

CPC classification number: C30B29/04 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068 ,  Y10T117/10

Abstract: A multi-layer structure in a reaction cell for a diamond growth is provided. The multi-layer structure includes: a diamond seed; a first metal catalyst layer provided on the diamond seed, the first metal catalyst layer containing a first concentration of carbon; a second metal catalyst layer provided on the first metal layer, the second metal catalyst layer containing a second concentration of carbon that is higher than the first concentration; and a carbon source layer provided on the second metal layer.

Abstract translation: 提供了用于金刚石生长的反应池中的多层结构。 多层结构包括：金刚石种子; 设置在所述金刚石晶种上的第一金属催化剂层，所述第一金属催化剂层含有第一浓度的碳; 设置在所述第一金属层上的第二金属催化剂层，所述第二金属催化剂层含有高于所述第一浓度的第二浓度的碳; 以及设置在第二金属层上的碳源层。

公开(公告)号：US09227166B2

公开(公告)日：2016-01-05

申请号：US11988891

申请日：2006-07-21

Applicant: Hitoshi Sumiya

Inventor： Hitoshi Sumiya

IPC: B01J3/06 ,  B82Y30/00 ,  C04B35/52 ,  C04B35/626 ,  C04B35/645

CPC classification number: B01J3/062 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/068 ,  B01J2203/0685 ,  B82Y30/00 ,  C04B35/52 ,  C04B35/6261 ,  C04B35/645 ,  C04B2235/422 ,  C04B2235/425 ,  C04B2235/427 ,  C04B2235/528 ,  C04B2235/5288 ,  C04B2235/5436 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/656 ,  C04B2235/78 ,  C04B2235/781 ,  C04B2235/785 ,  C04B2235/96 ,  Y10T428/2982

Abstract: There are provided sufficiently strong, hard, and heat resistant, dense and homogenous polycrystalline diamond applicable to cutting tools, dressers, dies and other working tools and excavation bits and the like, and a cutting tool having a cutting edge of the polycrystalline diamond. The polycrystalline diamond is formed substantially only of diamond formed using a composition of material containing a non diamond type carbon material, the composition of material being converted directly into diamond and sintered at ultra high pressure and ultra high temperature without aid of a sintering aid or a catalyst, and has a mixed microstructure having a fine crystal grain of diamond having a maximal grain size of at most 100 nm and an average grain size of at most 50 nm and a coarse crystal grain of diamond in the form of one of a platelet and a granule having a grain size of at least 50 nm and at most 10,000 nm.

公开(公告)号：US20150345229A1

公开(公告)日：2015-12-03

申请号：US14291862

申请日：2014-05-30

Applicant: Baker Hughes Incorporated

Inventor： Marc W. Bird

IPC: E21B10/567 ,  B24D99/00 ,  E21B10/55 ,  B24D18/00

CPC classification number: E21B10/567 ,  B01J3/00 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D18/0009 ,  B24D99/005 ,  E21B10/55

Abstract: A method of forming polycrystalline diamond includes encapsulating diamond particles, carbon monoxide, and carbon dioxide in a container. The encapsulated diamond particles, carbon monoxide, and carbon dioxide are subjected to a pressure of at least 4.5 GPa and a temperature of at least 1400° C. to form inter-granular bonds between the diamond particles. A cutting element includes polycrystalline diamond material comprising inter-bonded grains of diamond. The polycrystalline diamond material is substantially free of graphitic carbon and metallic compounds. The polycrystalline diamond material exhibits a density of at least about 3.49 g/cm3 and a modulus of at least about 1000 GPa. An earth-boring tool may include such a cutting element secured to a body.

Abstract translation: 形成多晶金刚石的方法包括将金刚石颗粒，一氧化碳和二氧化碳包封在容器中。 将包封的金刚石颗粒，一氧化碳和二氧化碳经受至少4.5GPa的压力和至少1400℃的温度以在金刚石颗粒之间形成颗粒间结合。 切割元件包括多晶金刚石材料，其包含金刚石的互相结合的颗粒。 多晶金刚石材料基本上不含石墨碳和金属化合物。 多晶金刚石材料表现出至少约3.49g / cm 3的密度和至少约1000GPa的模量。 钻孔工具可以包括固定到主体上的这种切割元件。