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公开(公告)号：US20050027067A1
公开(公告)日：2005-02-03
申请号：US10897683
申请日：2004-07-22
申请人： Hartmut Nefzger , Erika Bauer , Erhard Michels
发明人： Hartmut Nefzger , Erika Bauer , Erhard Michels
IPC分类号： C08F2/38 , C08F2/06 , C08F283/00 , C08F283/02 , C08F283/06 , C08G18/10 , C08G18/40 , C08G18/46 , C08G18/63 , C08G63/688 , C08G64/08 , C08K3/00 , C08K3/20
CPC分类号： C08G18/631 , C08F2/06 , C08F283/00 , C08F283/02 , C08F283/06 , C08G18/10 , C08G18/4072 , C08G63/688 , C08G64/081 , C08G2101/0066 , C08G2410/00 , C08G18/40
摘要： The present invention relates to polymer dispersions in polyester polyols, a process for producing them and their use for the production of polyurethanes, in particular microcellular polyurethanes. These polyester polyols have sulfur atoms and are free of olefinically unsaturated groups.
摘要翻译： 本发明涉及聚酯多元醇中的聚合物分散体，其制备方法及其用于生产聚氨酯，特别是微孔聚氨酯的用途。 这些聚酯多元醇具有硫原子并且不含烯属不饱和基团。
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公开(公告)号：US06541411B2
公开(公告)日：2003-04-01
申请号：US09995332
申请日：2001-11-27
申请人： Andreas Hoffmann , Hartmut Nefzger , Erika Bauer
发明人： Andreas Hoffmann , Hartmut Nefzger , Erika Bauer
IPC分类号： B01J3138
CPC分类号： B01J31/1658 , B01J31/223 , B01J31/38 , B01J2231/14 , B01J2231/49 , B01J2531/46 , B01J2531/48 , C08G18/4241 , C08G63/85 , C08G2101/00
摘要： The invention relates to novel titanium/zirconium catalysts, and to a process for the preparation of these titanium/zirconium catalysts. The process comprises reacting orthoesters or condensed orthoesters of titanium and/or zirconium, with one or more polyalcohols. Suitable polyalcohols comprise those compounds having at least two hydroxyl groups and a number average molecular weight of at least 180 g/mol. The invention also relates to a process for preparing (poly)esters from these novel catalysts, which exhibit little discoloration and are suitable to be used as a reaction component in the preparation of polyurethane (PUR) foams.
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23.发明授权Process for the preparation of polyricinoleic acid ester polyols having primary hydroxyl end groups 有权制备具有伯羟基端基的聚亚油酸酯多元醇的方法公开(公告)号：US09328196B2
公开(公告)日：2016-05-03
申请号：US13988606
申请日：2011-11-18
申请人： Hartmut Nefzger , Jörg Hofmann , Erika Bauer , Bert Klesczewski , Klaus Lorenz
发明人： Hartmut Nefzger , Jörg Hofmann , Erika Bauer , Bert Klesczewski , Klaus Lorenz
IPC分类号： C08G63/91 , C08G63/06 , C08G63/664 , C08G63/87 , C08G18/42 , C08G18/36 , C08G63/82 , C08G18/40 , C08G18/48 , C08G18/66 , C08G18/76 , C08G18/08 , C08G101/00
CPC分类号： C08G63/912 , C08G18/14 , C08G18/36 , C08G18/4018 , C08G18/4283 , C08G18/4288 , C08G18/4804 , C08G18/4841 , C08G18/4891 , C08G18/6696 , C08G18/7664 , C08G63/06 , C08G63/664 , C08G63/82 , C08G63/87 , C08G2101/0008 , C08G2101/0058 , C08G2101/0083
摘要： The present invention relates to a process for the preparation of polyricinoleic acid ester polyols having primary hydroxyl end groups. It furthermore relates to polyricinoleic acid ester polyols obtainable according to the invention and polyurethane polymers prepared using these polyols. The process comprises the steps: a) polycondensation of ricinoleic acid until a hydroxyl number of >0 mg of KOH/g to 80% by weight to
摘要翻译： 本发明涉及一种制备具有伯羟基端基的聚亚油酸酯多元醇的方法。 此外，它还涉及根据本发明获得的聚亚油酸酯多元醇和使用这些多元醇制备的聚氨酯聚合物。 该方法包括以下步骤：a）蓖麻油酸的缩聚直到羟基数> KOH / g至<60mg KOH / g为止; 和b）将步骤a）中获得的产物或包含羧基的步骤a）中获得的产物的次要产物与通式（I）的环氧化物反应，其中R 1表示氢，烷基或芳基 基团，基于所使用的环氧化物（I）的总量，> 80重量％至<100重量％是环氧乙烷，并且在作为催化剂的胺存在下进行反应。
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24.发明授权Process for the preparation of a polyurethane polymer with secondary hydroxyl end groups comprising polyester polyols 有权用于制备具有包含聚酯多元醇的仲羟基端基的聚氨酯聚合物的方法公开(公告)号：US09139685B2
公开(公告)日：2015-09-22
申请号：US13381139
申请日：2010-06-29
申请人： Hartmut Nefzger , Jörg Hofmann , Bert Klesczewski , Erika Bauer , Klaus Lorenz
发明人： Hartmut Nefzger , Jörg Hofmann , Bert Klesczewski , Erika Bauer , Klaus Lorenz
CPC分类号： C08G18/4291 , C08G18/4241 , C08G18/4261 , C08G18/4263 , C08G18/7621 , C08G63/916 , C08G77/46 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： The invention relates to a process for the preparation of a polyurethane polymer, comprising the step of reaction ofA) polyester polyols with secondary hydroxyl end groups, which are obtainable from the reaction of a polyester comprising carboxyl end groups with an epoxide of the general formula (1): wherein R1 represents an alkyl radical or an aryl radical and wherein the polyester comprising carboxyl end groups has an acid number of from ≧25 mg of KOH/g to ≦400 mg of KOH/g and a hydroxyl number of ≦5 mg of KOH/g, with B) polyisocyanates which are chosen from the group comprising toluoylene-diisocyanate, diphenylmethane-diisocyanate, polymeric diphenylmethane-diisocyanate, xylylene-diisocyanate, naphthylene-diisocyanate, hexamethylene-diisocyanate, diisocyanatodicyclohexylmethane and/or isophorone-diisocyanate. The invention furthermore relates to polyurethane polymers prepared by such a process.
摘要翻译： 本发明涉及一种制备聚氨酯聚合物的方法，包括A）聚酯多元醇与仲羟基端基反应的步骤，其可从包含羧基端基的聚酯与通式 （1）表示：其中R1表示烷基或芳基，其中包含羧基端基的聚酯的酸值为≥25mgKOH / g至＆lt; NlE; 400mg KOH / g，羟值为＆ ; B）多异氰酸酯，其选自甲苯二异氰酸酯，二苯基甲烷二异氰酸酯，聚合二苯基甲烷二异氰酸酯，亚二甲苯基二异氰酸酯，亚萘基二异氰酸酯，六亚甲基二异氰酸酯，二异氰酸二环己基甲烷和/或异佛尔酮 - 二异氰酸酯。 本发明还涉及通过这种方法制备的聚氨酯聚合物。
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公开(公告)号：US20100022739A1
公开(公告)日：2010-01-28
申请号：US12515775
申请日：2007-11-23
申请人： Hartmut Nefzger , Erika Bauer , Michael Ludewig , Matthias Schaub , Klaus-Dieter Nehren , Michael Freckmann , Holger Urbas
发明人： Hartmut Nefzger , Erika Bauer , Michael Ludewig , Matthias Schaub , Klaus-Dieter Nehren , Michael Freckmann , Holger Urbas
IPC分类号： C08G77/04
CPC分类号： C08G18/4825 , C08G18/10 , C08G65/33348 , C08G65/336 , C08G18/289
摘要： The present invention relates to impression compounds based on polyether derivatives, a process for their production and their use.
摘要翻译： 本发明涉及基于聚醚衍生物的印模化合物，其制备方法及其用途。
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26.发明申请Aliphatic, sinterable, thermoplastic polyurethane molding compositions with improved blooming behavior 有权脂肪，可烧结，热塑性聚氨酯模塑组合物，具有改善的起霜性能公开(公告)号：US20070265413A1
公开(公告)日：2007-11-15
申请号：US11800117
申请日：2007-05-04
IPC分类号： C08G18/00
CPC分类号： C08G18/4018 , C08G18/3221 , C08G18/6607 , C08G18/73 , C08G2140/00
摘要： Light-stable, sinterable, thermoplastic polyurethanes with improved blooming behavior and good thermal stability as well as good technical processability are produced from an aliphatic diisocyanate using one or more chain extenders corresponding to a specified formula. These polyurethanes are particularly useful in the production of molded articles, particularly molded articles for automotive interiors.
摘要翻译： 具有改善的起泡性能和良好的热稳定性以及良好的技术加工性能的光稳定的可烧结的热塑性聚氨酯由使用一种或多种对应于特定配方的扩链剂的脂族二异氰酸酯制备。 这些聚氨酯特别可用于制造模制品，特别是用于汽车内部的模塑制品。
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27.发明授权公开(公告)号：US09605106B2
公开(公告)日：2017-03-28
申请号：US13322989
申请日：2010-05-18
IPC分类号： C08L75/06 , C08J9/00 , C07C69/82 , C08G18/42 , C08G63/672 , C08G63/85 , C08G101/00
CPC分类号： C08G18/4252 , C08G18/4211 , C08G63/672 , C08G63/85 , C08G2101/0025 , C08G2101/005 , C08G2105/02
摘要： The present invention relates to a method for producing a polyester polyol having a concentration of ether groups in the range from 9.0 mol/kg of polyester polyol to 22 mol/kg polyester polyol, characterized in that (i) in a first step (A) isophthalic acid, optionally in the form of a C1-C4 alkyl ester, and/or terephthalic acid, optionally in the form of a C1-C4 alkyl ester, is reacted with (B) oligoethylene glycol of the formula H—(OCH2CH2)n—OH having a numerical average number of oxyethylene groups n in the range from 3.0 to 9.0, in the presence of at least one catalyst selected from the group made up of tin(II) salts, bismuth(II) salts, and titanium tetraalkoxylates, at a temperature in the range from 160° C. to 240° C., and at a pressure in the range from 1 to 1013 mbar, for a duration in the range from 7 to 100 hours, and (ii) in a second step the reaction mixture resulting from step (i) is reacted with (C) phthalic acid and/or phthalic acid hydride, the polyester polyols obtained according to said method, and to the use thereof for producing PUR/PIR hard foam materials.
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公开(公告)号：US08334035B2
公开(公告)日：2012-12-18
申请号：US13263144
申请日：2010-03-27
申请人： Hartmut Nefzger , Erika Bauer , Uwe Kuenzel , Jürgen Schloβmacher , Lutz Brassat
发明人： Hartmut Nefzger , Erika Bauer , Uwe Kuenzel , Jürgen Schloβmacher , Lutz Brassat
CPC分类号： C08G18/4252 , C08G63/672 , C08G63/83 , C08G63/85 , C08G2101/0025 , C08G2101/005 , C08G2105/02 , C08J9/141 , C08J2375/06 , Y10T428/1376 , Y10T428/139
摘要： Polyester polyols are produced by reacting terephthalic acid with a glycol corresponding to the formula H—(OCH2CH2)n—OH and an aliphatic dicarboxylic acid. These polyester polyols are particularly useful for the production of polyurethane) (PUR) and polyurethane/polyisocyanurate (PUR/PIR) foams for use in insulation applications.
摘要翻译： 聚对苯二甲酸与对应于式H-（OCH 2 CH 2）n -OH的二元醇和脂族二羧酸反应制备聚酯多元醇。 这些聚酯多元醇特别可用于生产用于绝缘应用的聚氨酯（PUR）和聚氨酯/聚异氰脲酸酯（PUR / PIR）泡沫。
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29.发明申请METHOD FOR THE PRODUCTION OF POLYETHER POLYOLS COMPRISING TERMINAL PRIMARY HYDROXYL GROUPS 有权生产包含终端主要羟基组合的聚醚多元醇的方法公开(公告)号：US20120196999A1
公开(公告)日：2012-08-02
申请号：US13381130
申请日：2010-06-30
申请人： Hartmut Nefzger , Erika Bauer , Jörg Hofmann , Klaus Lorenz , Norbert Hahn
发明人： Hartmut Nefzger , Erika Bauer , Jörg Hofmann , Klaus Lorenz , Norbert Hahn
CPC分类号： C08G18/4887 , C07C67/08 , C07C69/708 , C07C69/734 , C07C69/757 , C07C69/76 , C07C69/80 , C07C69/82 , C08G18/4866 , C08G65/2615 , C08G65/2663 , C08G65/2669 , C08G65/2672 , C08G65/3324 , C08G65/3326
摘要： The present invention relates to a process for producing polyether polyols having primary hydroxyl end groups, comprising the steps of reacting a starter compound containing active hydrogen atoms with an epoxide under double metal cyanide catalysis, reacting the resulting product with a cyclic carboxylic anhydride and reacting this resulting product with ethylene oxide in the presence of a catalyst containing at least one nitrogen atom per molecule, excluding non-cyclic, identically substituted tertiary amines. The invention further relates to polyether polyols obtainable by this process, compositions containing said polyols and polyurethane polymers based on said polyols.
摘要翻译： 本发明涉及一种制备具有伯羟基端基的聚醚多元醇的方法，包括以下步骤：在双金属氰化物催化下使含有活性氢原子的起始化合物与环氧化物反应，使所得产物与环状羧酸酐反应， 在每分子含有至少一个氮原子的催化剂存在下，得到的产物与环氧乙烷不同，不包括非环状，相同取代的叔胺。 本发明还涉及可通过该方法获得的聚醚多元醇，所述组合物含有所述多元醇和基于所述多元醇的聚氨酯聚合物。
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30.发明申请PROCESS FOR PRODUCING POLYESTER POLYOLS WITH LOW QUANTITIES OF DIOXANE WASTE 审中-公开用于生产低浓度二氧化硫废物的聚酯多元醇的方法公开(公告)号：US20120129966A1
公开(公告)日：2012-05-24
申请号：US13376450
申请日：2010-06-02
CPC分类号： C08G18/4252 , C08G18/4018 , C08G63/181 , C08G2101/0025 , C08G2101/005 , C08K5/0066 , C08L75/06
摘要： The present invention relates to the production and use of polyester polyols produced from at least one aromatic dicarboxylic acid or an alkyl ester of an aromatic dicarboxylic acid or the anhydride of an aromatic dicarboxylic acid and at least one α,ω-diol, wherein the formation of 1,4-dioxane from diethylene glycol is largely suppressed by means of specific reaction management.
摘要翻译： 本发明涉及由至少一种芳族二羧酸或芳族二羧酸的烷基酯或芳族二羧酸的酸酐和至少一种α，ω-二醇制备的聚酯多元醇的制造和使用，其中形成 的二甘醇的1,4-二恶烷通过特定的反应管理被大大抑制。
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