Abstract:
Provided is a method for producing a high-purity tungsten powder having a phosphorus content of less than 1 wtppm; wherein an ammonium tungstate solution containing 1 wtppm or more of phosphorus as an impurity in terms of the inclusion in tungsten is used as a starting material, this solution is neutralized with hydrochloric acid at a temperature of 50° C. or less to adjust the pH at 4 or more and less than 7 so as to precipitate ammonium paratungstate undecahydrate crystals, the resulting solution is heated to 70 to 90° C. and filtered in a high-temperature state so as to obtain ammonium paratungstate pentahydrate crystals, the obtained crystals are calcined so as to form a tungsten oxide, and the tungsten oxide is subject to hydrogen reduction so as to obtain a high-purity tungsten powder. Additionally provided is a method for producing a high-purity tungsten powder having a phosphorus content of 0.4 wtppm or less; wherein the ammonium tungstate solution is neutralized with hydrochloric acid to adjust the pH at 4 or more and 6 or less, and this solution is subject to the same procedure as described above so as to obtain a high-purity tungsten powder. Consequently, the phosphorus content can be efficiently reduced.
Abstract:
The present invention relates to a process for producing magnetic metal particles for magnetic recording, comprising:heat-treating goethite particles having an aluminum content of 4 to 50 atom % in terms of Al based on whole Fe to obtain hematite particles; andheat-reducing the hematite particles at a temperature of 200 to 600° C.,the goethite particles being obtained by adding a peroxodisulfate to a reaction solution comprising:a ferrous salt aqueous solution anda mixed alkali aqueous solution comprising:an alkali hydrogen carbonate aqueous solution or alkali carbonate aqueous solution andan alkali hydroxide aqueous solution before initiation of an oxidation reaction of the reaction solution, and then conducting the oxidation reaction.
Abstract:
A Raney-type metal porous material of which at least the inner surface of the pores constituting the porous structure is an alloy of the skeletal metal constituting it and a metal differing from the skeletal metal. The invention has made it possible to alloy a Raney-type metal with a porous structure, to realize a novel method of enabling remarkable enhancement of the function and the activity of the alloy based on the porous structure thereof, and to use the alloy as catalysts, etc.
Abstract:
A method for producing a sintered body includes: a) molding a composition containing a powder primarily made of an inorganic material and a binder including an aliphatic carbonic acid ester based resin in a predetermined shape so as to obtain a compact; b) exposing the compact to a first atmosphere containing an alkaline gas and thus decomposing and removing the aliphatic carbonic acid ester based resin from the compact so as to obtain a degreased body; and c) sintering the degreased body so as to obtain a sintered body.
Abstract:
A chromium-iron alloy comprises in weight %, 1 to 3% C, 1 to 3% Si, up to 3% Ni, 25 to 35% Cr, 1.5 to 3% Mo, up to 2% W, 2.0 to 4.0% Nb, up to 3.0% V, up to 3.0% Ta, up to 1.2% B, up to 1% Mn and 43 to 64% Fe. In a preferred embodiment, the chromium-iron alloy comprises in weight %, 1.5 to 2.3% C, 1.6 to 2.3% Si, 0.2 to 2.2% Ni, 27 to 34% Cr, 1.7 to 2.5% Mo, 0.04 to 2% W, 2.2 to 3.6% Nb, up to 1% V, up to 3.0% Ta, up to 0.7% B, 0.1 to 0.6% Mn and 43 to 64% Fe. The chromium-iron alloy is useful for valve seat inserts for internal combustion engines such as diesel or natural gas engines.
Abstract:
The invention relates to a drill bit containing tungsten carbide powder having powder particles which have a core of cast tungsten carbide and a shell of tungsten monocarbide.
Abstract:
A fuel cell having an excellent life property is achieved. A supported catalyst for a fuel cell includes a catalytic particle made of an alloy of platinum and gold, and a conductive carrier supporting the catalytic particle. 50% or more of gold forms a solid solution with platinum.
Abstract:
The present invention provides a method of manufacturing a porous metal electrode for a molten carbonate fuel cell using a dry process. According to the method of manufacturing a porous metal electrode of the present invention, in the press process for controlling the thickness of dry-cast metal powder and rearranging the dry-cast metal powder, the microstructure of the porous metal electrode can be controlled, and the uniformity of the thickness of the porous metal electrode can also be controlled. Therefore, the method of manufacturing a porous metal electrode according to the present invention can be used to manufacture both an anode and a cathode.
Abstract:
An RE-containing alloy, which is represented by a compositional formula of RrTtAa (wherein R represents at least one rare earth element selected from among La, Ce, Pr, Nd, Sm, Eu, Tb, Dy, Ho, Tm, Yb, Gd, and Lu; T collectively represents transition metal elements containing at least Fe atoms, a portion of the Fe atoms being optionally substituted by at least one species selected from among Co, Ni, Mn, Pt, and Pd; A represents at least one element selected from among Al, As, Si, Ga, Ge, Mn, Sn, and Sb; and r, t, and a have the following relationships: 5.0 at. %≦r≦6.8 at. %, 73.8 at. %≦t≦88.7 at. %, and 4.6 at. %≦a≦19.4 at. %) and having an alloy microstructure containing an NaZn13-type crystal structure in an amount of at least 85 mass % and α-Fe in an amount of 5-15 mass % inclusive.
Abstract:
One provides (101) disperse ultra-nanocrystalline diamond powder material that comprises a plurality of substantially ordered crystallites that are each sized no larger than about 10 nanometers. One then reacts (102) these crystallites with a metallic component. The resultant nanowire is then able to exhibit a desired increase with respect to its ability to conduct electricity while also substantially preserving the thermal conductivity behavior of the disperse ultra-nanocrystalline diamond powder material. The reaction process can comprise combining (201) the crystallites with one or more metal salts in an aqueous solution and then heating (203) that aqueous solution to remove the water. This heating can occur in a reducing atmosphere (comprising, for example, hydrogen and/or methane) to also reduce the salt to metal.