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    Zirconium basic carbonate and methods of making the same
    36.
    发明授权
    Zirconium basic carbonate and methods of making the same 有权
    碱式碳酸锆及其制备方法

    公开(公告)号：US07101519B2

    公开(公告)日：2006-09-05

    申请号：US10914954

    申请日：2004-08-10

    Applicant: Raymond J. Wong

    Inventor： Raymond J. Wong

    IPC: C01G25/00 ,  C01B31/24 ,  C01B25/37

    CPC classification number: B01J20/043 ,  A61M1/1696 ,  B01J20/0211 ,  B01J20/0277 ,  B01J20/0292 ,  B01J20/08 ,  B01J20/20 ,  B01J20/28052 ,  B01J20/3234 ,  B01J2220/42 ,  B01J2220/62 ,  C01G25/00 ,  C01G25/006 ,  C01P2004/61 ,  C01P2006/82

    Abstract: Methods of making zirconium basic carbonate are further described which involve titrating an aqueous slurry of sodium zirconium carbonate to a pH of from about 3.5 to about 4.0 with an acidic agent wherein the sodium zirconium carbonate has a moisture content of from about 15% to about 25% LOD in solid form. The process further involves washing the aqueous slurry containing the formed zirconium basic carbonate with water. A novel zirconium basic carbonate is further disclosed which has a minimum adsorption capacity of from about 30 to about 35 mg/PO4-P/gm SCZ; a minimum HCO3- content of from about 2 to about 4 mEq HCO3-gm/SCZ; a leachable Na+ content of from about 1.5 to about 2.0 mEq Na+/gm SCZ; and/or a pH range of titrated sodium zirconium carbonate of from about 6 to about 7.

    Abstract translation: 进一步描述了制备碱式碳酸锆的方法，其中包括用酸性试剂滴定碳酸锆钠水溶液至约3.5至约4.0的pH，其中碳酸锆钠的水分含量为约15％至约25 ％LOD为固体形式。 该方法还包括用水洗涤含有形成的碳酸碱式碳酸锆的含水浆料。 进一步公开了一种新型的碱式碳酸锆，其具有约30至约35mg / PO 4 -P / g SCZ的最小吸附容量; 约2至约4mEq HCO 3 -gm / SCZ的最小HCO 3 - 含量; 约1.5至约2.0mEq Na + + / gm SCZ的可浸出的Na + +含量; 和/或滴定的碳酸锆碳酸钙的pH范围为约6至约7。

    Chemical formulations for the removal of mercury and other pollutants present in fluid streams
    37.
    发明授权
    Chemical formulations for the removal of mercury and other pollutants present in fluid streams 失效
    用于去除存在于流体流中的汞和其他污染物的化学配方

    公开(公告)号：US07081434B2

    公开(公告)日：2006-07-25

    申请号：US10292078

    申请日：2002-11-12

    Applicant: Rabindra K. Sinha

    Inventor： Rabindra K. Sinha

    IPC: B01J20/00

    CPC classification number: B01D53/02 ,  B01D53/64 ,  B01D2253/104 ,  B01D2253/106 ,  B01D2253/11 ,  B01D2257/602 ,  B01J20/02 ,  B01J20/0233 ,  B01J20/0237 ,  B01J20/0244 ,  B01J20/0251 ,  B01J20/0259 ,  B01J20/0277 ,  B01J20/0281 ,  B01J20/0288 ,  B01J20/0296 ,  B01J20/045 ,  B01J20/046 ,  B01J20/06 ,  B01J20/08 ,  B01J20/103 ,  B01J20/12 ,  B01J20/24 ,  B01J20/262 ,  B01J2220/46 ,  B01J2220/4825

    Abstract: The invention provides compositions to remove mercury and other pollutants from a fluid stream,, particularly flue gases containing them. The composition is a mixture consisting of (a) polyhydroxy compound selected essentially from the group consisting of mono, di, poly saccharides and mixture thereof; (b) a catalyst selected essentially from the group of ammonium compounds, sulfuric acid, phosphoric acid and salts, zinc chloride, and mixture thereof; and (c) specificity producing compound selected from the group of elemental sulfur, sullides and polysulfides of ammonia and alkalies, compounds and metals of copper, silver, tin, gold, and mixture thereof. The polyhydroxy compound in (a) above, either alone or in conjunction with the third group (c), above is also shown effective to remove mercury and other pollutants from fluid streams. The composition can be liquid or dry powder. Methods are provided for applying the formulation.

    Abstract translation: 本发明提供了从流体流，特别是含有它们的烟道气中除去汞和其它污染物的组合物。 组合物是由（a）多羟基化合物组成的混合物，其基本上由单糖，二糖，多糖及其混合物组成; （b）主要由铵化合物，硫酸，磷酸和盐，氯化锌及其混合物组选择的催化剂; 和（c）特异性产生化合物，其选自氨和碱的元素硫，硫化物和多硫化物，铜，银，锡，金及其混合物的化合物和金属。 上文（a）中单独或与上述第三组（c）结合的多羟基化合物也被证明有效地从流体流中除去汞和其它污染物。 组合物可以是液体或干粉。 提供了用于施用制剂的方法。

    Sodium zirconium carbonate and zirconium basic carbonate and methods of making the same
    39.
    发明申请
    Sodium zirconium carbonate and zirconium basic carbonate and methods of making the same 有权
    碳酸锆锆和碱式碳酸锆及其制备方法

    公开(公告)号：US20050031523A1

    公开(公告)日：2005-02-10

    申请号：US10914954

    申请日：2004-08-10

    Applicant: Raymond Wong

    Inventor： Raymond Wong

    IPC: A61M1/14 ,  A61K33/24 ,  A61M1/16 ,  A61M1/28 ,  A61P7/08 ,  B01J20/02 ,  B01J20/04 ,  B01J20/06 ,  B01J20/24 ,  B01J20/28 ,  C01B32/60 ,  C01G25/00 ,  C01B31/30

    CPC classification number: B01J20/043 ,  A61M1/1696 ,  B01J20/0211 ,  B01J20/0277 ,  B01J20/0292 ,  B01J20/08 ,  B01J20/20 ,  B01J20/28052 ,  B01J20/3234 ,  B01J2220/42 ,  B01J2220/62 ,  C01G25/00 ,  C01G25/006 ,  C01P2004/61 ,  C01P2006/82

    Abstract: A method of making sodium zirconium carbonate is described which involves forming a mixture of zirconium oxychloride with soda ash and then heating at a sufficient temperature and for a sufficient time to form the sodium zirconium carbonate. Subsequent washing and filtration steps can further form parts of this process. A novel sodium zirconium carbonate is further described which contains from about 2 wt % to about 5 wt % Na+; from about 44 wt % to about 50 wt % ZrO2; from about 12 wt % to about 18 wt % CO32−; and from about 32 wt % to about 35 wt % H2O. Methods of making zirconium basic carbonate are further described which involve titrating an aqueous slurry of sodium zirconium carbonate to a pH of from about 3.5 to about 4.0 with an acidic agent wherein the sodium zirconium carbonate has a moisture content of from about 15% to about 25% LOD in solid form. The process further involves washing the aqueous slurry containing the formed zirconium basic carbonate with water. A novel zirconium basic carbonate is further disclosed which has a minimum adsorption capacity of from about 30 to about 35 mg/PO4- P/gm SCZ; a minimum HCO3- content of from about 2 to about 4 mEq HCO3-gm/SCZ; a leachable Na+ content of from about 1.5 to about 2.0 in Eq Na+/gm SCZ; and/or a pH range of titrated sodium zirconium carbonate of from about 6 to about 7. A method of making zirconium phosphate is also disclosed which involves treating sodium zirconium carbonate with caustic soda to from an alkaline hydrous zirconium oxide which is subsequently heated and mixed with phosphoric acid to obtain an acid zirconium phosphate which can be titrated with caustic soda to achieve the desired zirconium phosphate. Novel zirconium phosphates are also disclosed as well as uses for the above zirconium containing materials.

    Abstract translation: 描述了制备碳酸锆钠的方法，其涉及形成氯氧化锆与苏打灰的混合物，然后在足够的温度下加热足够的时间以形成碳酸锆钠。 随后的洗涤和过滤步骤可以进一步形成该方法的一部分。 进一步描述了一种新的碳酸锆钠，其含有约2重量％至约5重量％的Na +; 约44重量％至约50重量％的ZrO 2; 约12重量％至约18重量％的CO 3 2-; 和约32重量％至约35重量％的H 2 O. 进一步描述了制备碱式碳酸锆的方法，其中包括用酸性试剂滴定碳酸锆钠水溶液至约3.5至约4.0的pH，其中碳酸锆钠的水分含量为约15％至约25 ％LOD为固体形式。 该方法还包括用水洗涤含有形成的碳酸碱式碳酸锆的含水浆料。 进一步公开了一种新型的碱式碳酸锆，其具有约30至约35mg / PO 4 -P / g SCZ的最小吸附容量; 约2至约4mEq HCO 3 -gm / SCZ的最小HCO 3含量; 在Na + / gm SCZ中可浸出的Na +含量为约1.5至约2.0; 和/或滴定的碳酸锆碳酸钙的pH范围为约6至约7.还公开了制备磷酸锆的方法，其涉及用苛性钠将碳酸锆钠从碱性水合氧化锆处理，随后加热和混合 与磷酸一起获得可用苛性钠滴定的酸式磷酸锆，以达到所需的磷酸锆。 还公开了新的磷酸锆，以及上述含锆材料的用途。

    Copper-containing materials
    40.
    发明授权
    Copper-containing materials 有权
    含铜材料

    公开(公告)号：US06703342B1

    公开(公告)日：2004-03-09

    申请号：US09664556

    申请日：2000-09-18

    Applicant: Cornelis Martinus Lok

    Inventor： Cornelis Martinus Lok

    IPC: B01J2372

    CPC classification number: B01J37/0203 ,  B01J20/0237 ,  B01J20/0277 ,  B01J20/06 ,  B01J20/08 ,  B01J20/223 ,  B01J20/28004 ,  B01J20/28061 ,  B01J20/28073 ,  B01J20/28083 ,  B01J20/3007 ,  B01J20/3078 ,  B01J20/3204 ,  B01J20/3236 ,  B01J21/04 ,  B01J23/72 ,  B01J35/0053 ,  B01J37/03

    Abstract: Copper/alumina compositions for uses as e.g. catalysts are made by impregnating a porous transition alumina support with an aqueous solution of a copper ammine carbonate complex, draining off any excess of the impregnating solution, and then heating the impregnated support to a temperature above 80° C. to decompose the complex thereby depositing a basic copper carbonate compound on the surfaces of the pores of transition alumina support. After reduction, the composition has a high copper surface area, expressed per unit weight of copper in the composition.

    Abstract translation: 铜/氧化铝组合物用于例如。 通过用铜氨基甲酸铜络合物的水溶液浸渍多孔转变氧化铝载体，排出任何过量的浸渍溶液，然后将浸渍的载体加热至高于80℃的温度以分解复合物从而沉积 在过渡氧化铝载体的孔表面上的碱性碳酸铜化合物。 还原后，组合物具有高的铜表面积，表示组合物中每单位重量的铜。

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