公开(公告)号：US07651973B2

公开(公告)日：2010-01-26

申请号：US12217971

申请日：2008-07-10

Applicant: Andreas Schlegel

Inventor： Andreas Schlegel

IPC: B01J23/70 ,  B01J23/74

CPC classification number: B82Y30/00 ,  B01D53/02 ,  B01D2253/10 ,  B01J20/0229 ,  B01J20/06 ,  B01J20/08 ,  B01J20/2803 ,  B01J20/28057 ,  B01J20/3028 ,  C01G49/0036 ,  C01G49/0045 ,  C01G49/02 ,  C01G49/06 ,  C01P2004/10 ,  C01P2004/50 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12 ,  C02F1/281 ,  C02F1/288 ,  C02F2101/20 ,  C02F2201/006

Abstract: The present invention relates to a filtering unit at least partially filled with particles agglomerated from fine-particle iron oxide and/or iron oxyhydroxide by producing an aqueous suspension of fine-particle iron oxides and/or iron oxyhydroxides having a BET surface area of 50 to 500 m2/g, and removing the water and dissolved constituents by a set of washing drying and filtering steps and processes of using the particles.

Abstract translation: 本发明涉及至少部分填充有细颗粒氧化铁和/或羟基氧化铁附聚的颗粒的过滤单元，该过滤单元通过产生具有BET表面积为50的细颗粒氧化铁和/或羟基氧化铁的水性悬浮液， 500m 2 / g，并通过一组洗涤干燥和过滤步骤和使用颗粒的方法除去水和溶解成分。

公开(公告)号：US07531149B2

公开(公告)日：2009-05-12

申请号：US11204766

申请日：2005-08-16

Applicant: Xiaogang Peng ,  Yongfen Chen ,  Nikhil Jana ,  Arun Narayanaswamy

Inventor： Xiaogang Peng ,  Yongfen Chen ,  Nikhil Jana ,  Arun Narayanaswamy

IPC: B23B5/16 ,  C01G5/00 ,  C01G7/00 ,  C01G51/00 ,  C01G55/00

CPC classification number: C01B13/18 ,  B82Y25/00 ,  B82Y30/00 ,  C01G1/02 ,  C01G9/02 ,  C01G15/00 ,  C01G19/00 ,  C01G19/02 ,  C01G37/02 ,  C01G49/02 ,  C01G49/08 ,  C01G53/04 ,  C01P2002/72 ,  C01P2002/82 ,  C01P2002/84 ,  C01P2004/04 ,  C01P2004/52 ,  C01P2004/64 ,  H01F1/0054 ,  Y10S977/777 ,  Y10S977/811 ,  Y10T428/2982

Abstract: A general, reproducible, and simple synthetic method that employs readily available chemicals permits control of the size, shape, and size distribution of metal oxide nanocrystals. The synthesis entails reacting a metal fatty acid salt, the corresponding fatty acid, and a hydrocarbon solvent, with the reaction product being pyrolyzed to the metal oxide. Nearly monodisperse oxide nanocrystals of Fe3O4, Cr2O3, MnO, Co3O4, NiO, ZnO, SnO2, and In2O3, in a large size range (3-50 nm), are described. Size and shape control of the nanocrystals is achieved by varying the reactivity and concentration of the precursors.

Abstract translation: 使用容易获得的化学品的一般的，可重现的和简单的合成方法允许控制金属氧化物纳米晶体的尺寸，形状和尺寸分布。 合成需要使金属脂肪酸盐，相应的脂肪酸和烃溶剂反应，反应产物被热解成金属氧化物。 描述了大尺寸范围（3-50nm）中的Fe 3 O 4，Cr 2 O 3，MnO，Co 3 O 4，NiO，ZnO，SnO 2和In 2 O 3的近似单分散氧化物纳米晶体。 通过改变前体的反应性和浓度来实现纳米晶体的尺寸和形状控制。

公开(公告)号：US20080267806A1

公开(公告)日：2008-10-30

申请号：US11880518

申请日：2007-07-23

Applicant: Tomohiro Suetsuna ,  Seiichi Suenaga ,  Kouichi Harada ,  Maki Yonetsu

Inventor： Tomohiro Suetsuna ,  Seiichi Suenaga ,  Kouichi Harada ,  Maki Yonetsu

IPC: B22F1/02 ,  H01F1/00 ,  B32B38/00 ,  B05D5/00

CPC classification number: H01F10/3231 ,  B22F9/22 ,  B22F2998/00 ,  B82Y25/00 ,  B82Y30/00 ,  C01G45/02 ,  C01G49/02 ,  C01G51/04 ,  C01P2002/22 ,  C01P2004/32 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2004/80 ,  C01P2006/42 ,  C22C1/051 ,  C22C32/0026 ,  H01F1/24 ,  H01F41/16 ,  H01Q17/004 ,  B22F1/0018

Abstract: A precursor particle having a particle size of 10 nm or more and 1 μm or less, and comprising a first compound selected from an alkoxide, a hydroxide, a sulfate, a nitrate, a carbonate, or a carboxylate of magnetic metal containing at least one metal of Fe and Co, and a second compound selected from an alkoxide or a hydroxide, a sulfate, a nitrate, a carbonate, or a carboxylate of a metal element for forming an oxide, is prepared. Then the precursor particle is heated in a reducing atmosphere to form an insulating particle made of an oxide of the metal element by decomposing the second compound, and to precipitate a particle of the magnetic metal in the insulating particle at a particle size of 1 nm or more and 100 nm or less, thereby manufacturing a high frequency magnetic material.

Abstract translation: 具有10nm以上且1μm以下的粒径的前体粒子，并且含有选自含有至少一个以上的金属的磁性金属的醇盐，氢氧化物，硫酸盐，硝酸盐，碳酸盐或羧酸盐的第一化合物 Fe和Co的金属，以及选自用于形成氧化物的金属元素的醇盐或氢氧化物，硫酸盐，硝酸盐，碳酸盐或羧酸盐的第二种化合物。 然后在还原气氛中加热前体颗粒，通过分解第二化合物形成由金属元素的氧化物制成的绝缘颗粒，并使粒子中的磁性金属颗粒沉淀在1nm的粒径或 大于或等于100nm，由此制造高频磁性材料。

公开(公告)号：US07442362B2

公开(公告)日：2008-10-28

申请号：US10836304

申请日：2004-04-30

Applicant: Esterino Conca ,  Carlo Rubini ,  Guido Petrini

Inventor： Esterino Conca ,  Carlo Rubini ,  Guido Petrini

IPC: C01G49/02 ,  C01G49/06

CPC classification number: B41F1/08 ,  B01J23/745 ,  B01J35/10 ,  B01J35/1014 ,  B01J35/1019 ,  B01J37/086 ,  B01J37/12 ,  B41F1/50 ,  C01G49/02 ,  C01G49/06 ,  C01P2006/12 ,  C01P2006/13 ,  C09C1/24

Abstract: Highly pure iron oxides are prepared by reaction of metallic iron, in the form of microspheroidal particles or of scraps or cuttings, with an agitated aqueous solution of a mono- or polycarboxylic acid with a pKa of 0.5 to 6 relative to the first carboxyl and capable of decomposing, by heating in air at 200 to 350 ° C., to carbon dioxide and water, using 0.03 to 1.5 moles of acid per g-atoms of iron, a water/iron weight ration of 1 to 20, and by oxidation of the ferrous carboxilate to ferric salt, with an agent selected from oxygen, mixtures containing oxygen, hydrogen peroxide, organic peroxides and hydroperoxides.

Abstract translation: 高纯度的氧化铁是通过以微球形颗粒或废料或切屑的形式的金属铁与搅拌的单羧酸或多元羧酸的水溶液相对于第一羧基和pKa为0.5至6的反应制备的 通过在200-350℃的空气中加热分解成二氧化碳和水，每克原子铁使用0.03至1.5摩尔酸，1至20的水/铁重量比，并通过氧化 碳酸亚铁酸盐与铁盐，与选自氧的试剂，含氧的混合物，过氧化氢，有机过氧化物和氢过氧化物。

公开(公告)号：US20080220531A1

公开(公告)日：2008-09-11

申请号：US11683889

申请日：2007-03-08

Applicant: Patrick S. Stayton ,  Allan S. Hoffman ,  Jr-iuan Lai ,  John Hoffman ,  Mitsuhiro Ebara

Inventor： Patrick S. Stayton ,  Allan S. Hoffman ,  Jr-iuan Lai ,  John Hoffman ,  Mitsuhiro Ebara

IPC: G01N33/20 ,  B01J19/00 ,  H01F1/00 ,  C01G49/02

CPC classification number: G01N33/54326 ,  B82Y25/00 ,  C01G49/02 ,  H01F1/0054

Abstract: Stimuli-responsive magnetic nanoparticles, methods of making the nanoparticles, and methods of using the nanoparticles.

Abstract translation: 刺激响应磁性纳米颗粒，制备纳米颗粒的方法和使用纳米颗粒的方法。

公开(公告)号：US20080175740A1

公开(公告)日：2008-07-24

申请号：US11949283

申请日：2007-12-03

Applicant: Michael J. RUTHNER

Inventor： Michael J. RUTHNER

IPC: B22F9/22 ,  C22C33/00

CPC classification number: C22B5/12 ,  C01G49/02 ,  C01G49/06 ,  C01P2006/12 ,  C01P2006/80 ,  C22B1/24 ,  C22B7/00 ,  Y02P10/212

Abstract: A method for manufacturing of iron- respectively micro-alloyed steel powders, starting from fluffy spray roasted iron oxides exhibiting a specific surface area in excess of 2.0 m2/g and residual chloride contents over 440 ppm Cl′, decrease the chloride content in two steps to less than 100 ppm, the specific surface area (BET) of to a pre-selected value of less than 10.0 m2/g, preferably between 0.1 and 2.0 m2/g and reduce the pre-sintered granules exhibiting a bulk density in excess of 1.200 g/dm3.

Abstract translation: 铁 - 微细合金钢粉末的制造方法，从表面积超过2.0m 2 / g的蓬松喷雾焙烧铁氧化物开始，残余氯化物含量超过440ppm Cl' ，将两步的氯化物含量降低到小于100ppm，比表面积（BET）小于10.0m 2 / g，优选0.1-2.0μm的预选值 减少表现出超过1.200g / dm 3的堆积密度的预烧结颗粒。

公开(公告)号：US20080035562A1

公开(公告)日：2008-02-14

申请号：US11658163

申请日：2005-07-15

Applicant: Hiroshi Hata ,  Kenji Haiki ,  Kazuhiko Nishina ,  Masatami Sakata

Inventor： Hiroshi Hata ,  Kenji Haiki ,  Kazuhiko Nishina ,  Masatami Sakata

IPC: C25C7/06 ,  B01J20/02

CPC classification number: B01J20/06 ,  B01D15/00 ,  B01J20/0211 ,  B01J20/0229 ,  B01J20/0244 ,  B01J20/0248 ,  B01J20/0281 ,  B01J20/041 ,  B01J20/045 ,  B01J20/3433 ,  B01J20/3475 ,  B01J2220/42 ,  C01G49/02 ,  C01G49/06 ,  C01G49/08 ,  C01P2004/04 ,  C22B3/24 ,  C25C1/16 ,  Y02P10/234 ,  Y10S210/915

Abstract: In order to remove fluorine from a zinc containing solution before zinc electro-refining in lower cost, fluorine is removed by adsorption from a zinc containing solution (leached solution) utilizing the character of the predetermined iron compound or zinc compound which can adsorb fluorine in an acid solution and desorb fluorine in an alkaline solution. The fluorine adsorbent/desorbent having adsorbed fluorine is treated in an alkaline solution, to desorb the fluorine. This makes it possible to regenerate the fluorine adsorbent/desorbent. Further, an electrolytic solution for zinc electro-refining can be prepared in lower cost, thus total zinc refining costs can be reduced.

Abstract translation: 为了在较低成本的锌精炼之前从含锌溶液中除去氟，利用可以吸附氟的预定铁化合物或锌化合物的特性，从含锌溶液（浸出溶液）中吸附除去氟 酸溶液并在碱性溶液中解吸氟。 吸附了氟的氟吸附剂/解吸剂在碱性溶液中进行处理，以解吸氟。 这使得可以再生氟吸附剂/解吸剂。 此外，可以以更低的成本制备锌电精炼用电解液，从而可以降低锌精炼成本。

公开(公告)号：US07186395B2

公开(公告)日：2007-03-06

申请号：US10473214

申请日：2002-04-03

Applicant: Christian Walsdorff ,  Michael Bajer ,  Reinhard Körner ,  Klaus Harth ,  Gerald Vorberg ,  Wilhelm Ruppel

Inventor： Christian Walsdorff ,  Michael Bajer ,  Reinhard Körner ,  Klaus Harth ,  Gerald Vorberg ,  Wilhelm Ruppel

IPC: B10J23/745 ,  C07C5/32 ,  C01G49/00

CPC classification number: C01G49/06 ,  B01J23/745 ,  B01J23/78 ,  B01J23/881 ,  B01J23/8872 ,  B01J35/023 ,  B01J37/08 ,  B01J37/088 ,  C01G49/02 ,  C01P2004/51 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/16 ,  C01P2006/80 ,  C07C5/3332 ,  C07C2523/745 ,  Y10S423/01 ,  C07C15/46

Abstract: Iron oxides are upgraded by calcining at from 700 to 1200° C.

Abstract translation: 铁氧化物通过700至1200℃的煅烧升级。

公开(公告)号：US20050169861A1

公开(公告)日：2005-08-04

申请号：US10510946

申请日：2003-06-03

Applicant: Wolfgang Lortz ,  Christoph Batz-Sohn ,  Steffen Hasenzahl ,  Gabriele Perlet ,  Werner Will

Inventor： Wolfgang Lortz ,  Christoph Batz-Sohn ,  Steffen Hasenzahl ,  Gabriele Perlet ,  Werner Will

IPC: A61K8/19 ,  A61K8/00 ,  A61K8/04 ,  A61K8/24 ,  A61K8/25 ,  A61K8/26 ,  A61K8/29 ,  A61Q17/04 ,  A61Q19/00 ,  C01G1/02 ,  C01G9/02 ,  C01G23/04 ,  C01G23/047 ,  C01G49/02 ,  C09C1/00 ,  C09C1/36 ,  C09D17/00 ,  A61K7/021

CPC classification number: A61K8/044 ,  A61K8/24 ,  A61K8/29 ,  A61Q17/04 ,  A61Q19/00 ,  C01G1/02 ,  C01G9/02 ,  C01G23/047 ,  C01G49/02 ,  C01P2006/22 ,  C09C1/3653 ,  C09D17/007

Abstract: Aqueous dispersion containing pyrogenically produced oxide particles of titanium, zinc, iron or cerium having an average particle size, expressed as a median value, in the dispersion of less than 200 nm, the particle sizes of the oxide particles are not distributed symmetrically in the dispersion, the dispersion contains as dispersing agent at least one (poly)phosphate corresponding to the general formula I and has a pH of 4.5 to 7.5. It is prepared by dispersing a stream of a preliminary dispersion by means of a high-energy mill. It can be used in sunscreen formulations.

Abstract translation: 含有热解产生的氧化物粒子的钛，锌，铁或铈的水分散体，在分散体中的平均粒径（以中值表示）小于200nm，氧化物粒子的粒径在分散体中不对称分布 ，分散体含有至少一种对应于通式I的（聚）磷酸酯作为分散剂，pH为4.5〜7.5。 通过高能磨分散预备分散液流来制备。 它可用于防晒配方。

公开(公告)号：US20050042155A1

公开(公告)日：2005-02-24

申请号：US10647137

申请日：2003-08-21

Applicant: Duane Powell ,  Luke Daly ,  Lee Ciampi

Inventor： Duane Powell ,  Luke Daly ,  Lee Ciampi

IPC: B01F13/10 ,  B01F15/04 ,  B01J4/00 ,  B01J19/18 ,  C01G49/00 ,  C01G49/02 ,  C02F1/72 ,  B01F1/00

CPC classification number: B01J4/008 ,  B01F13/1055 ,  B01F15/0445 ,  B01F15/0479 ,  B01J19/18 ,  B01J2219/00006 ,  B01J2219/00038 ,  B01J2219/00103 ,  B01J2219/00186 ,  C01G49/0081 ,  C01G49/02 ,  C02F1/72

Abstract: Disclosed herein is a device for the synthesis of ferrate, comprising, a plurality of containers 102 to hold starting materials; a measuring unit to measure an amount of said starting materials; a mixer to mix said measured amount of said starting materials; a reaction chamber, wherein said mixed starting materials react to produce ferrate; and a drain through which said ferrate is obtained; wherein said drain is located at a site proximal to the site of use of said ferrate.

Abstract translation: 本文公开了一种用于合成高铁酸盐的装置，其包括多个用于保持起始材料的容器102; 用于测量所述起始材料的量的测量单元; 混合所述测量量的所述起始材料的混合器; 反应室，其中所述混合起始材料反应以产生高铁酸盐; 和通过该漏极获得所述高铁酸盐; 其中所述排水管位于靠近所述高铁酸盐使用部位的位置。