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    Methods for producing low oxygen biomass-derived pyrolysis oils
    83.
    发明授权
    Methods for producing low oxygen biomass-derived pyrolysis oils 有权
    生产低氧生物质的裂解油的方法

    公开(公告)号：US09222044B2

    公开(公告)日：2015-12-29

    申请号：US12843649

    申请日：2010-07-26

    Applicant: Thomas Traynor ,  Timothy A. Brandvold

    Inventor： Thomas Traynor ,  Timothy A. Brandvold

    IPC: C10L1/10 ,  C10L1/18 ,  C10L1/02

    CPC classification number: C10L1/02 ,  Y02P30/20

    Abstract: Methods for producing low oxygen biomass-derived pyrolysis oil are provided. Starting biomass-derived pyrolysis oil is deoxygenated by exposing the biomass-derived oil to a first catalyst in the presence of hydrogen-containing gas at first hydroprocessing conditions to produce a partially deoxygenated biomass-derived pyrolysis oil. The first catalyst has a neutral catalyst support. The partially deoxygenated biomass-derived pyrolysis oil is exposed to a second catalyst in the presence of additional hydrogen-containing gas at second hydroprocessing conditions to produce a hydrocarbon product. The biomass-derived pyrolysis oil may be esterified prior to deoxygenation. A portion of the low oxygen biomass-derived pyrolysis oil is recycled.

    Abstract translation: 提供了生产低氧生物质的热解油的方法。 起始生物质衍生的热解油通过在第一加氢处理条件下在含氢气体存在下将生物质衍生的油暴露于第一催化剂而脱氧，以产生部分脱氧生物质衍生的热解油。 第一种催化剂具有中性催化剂载体。 部分脱氧生物质衍生的热解油在第二加氢处理条件下在另外含氢气体存在下暴露于第二催化剂以产生烃产物。 生物质衍生的热解油可以在脱氧前被酯化。 一部分低氧生物质衍生的热解油被再循环。

    PROCESSES FOR PRODUCING CELLULOSIC FRUCTOSE FROM LIGNOCELLULOSIC BIOMASS
    84.
    发明申请
    PROCESSES FOR PRODUCING CELLULOSIC FRUCTOSE FROM LIGNOCELLULOSIC BIOMASS 审中-公开
    从细菌生物量生产细胞纤维的方法

    公开(公告)号：US20150361474A1

    公开(公告)日：2015-12-17

    申请号：US14831827

    申请日：2015-08-20

    Applicant: API Intellectual Property Holdings, LLC

    Inventor： Kimberly NELSON ,  Vesa PYLKKANEN ,  Theodora RETSINA ,  Ryan O'CONNOR

    IPC: C12P19/24 ,  C10L1/02 ,  A23L1/236 ,  C10L5/44 ,  A23L2/60 ,  C12P19/02 ,  C10L1/04

    CPC classification number: C12P19/24 ,  A23L2/60 ,  A23L27/33 ,  C10L1/02 ,  C10L5/44 ,  C10L2200/0469 ,  C10L2290/26 ,  C12P19/02 ,  C12P19/14 ,  C12P2201/00 ,  C12P2203/00 ,  C13K1/02 ,  C13K11/00 ,  Y02E50/10 ,  Y02E50/30

    Abstract: Some variations provide a process for producing cellulosic fructose from biomass, comprising: fractionating a biomass feedstock in the presence of an acid catalyst, a solvent for lignin, and water, to produce a liquor containing cellulose-rich solids, lignin, and dissolved hemicellulose; removing the cellulose-rich solids from the liquor; hydrolyzing the dissolved hemicellulose contained in the liquor, to produce a hydrolyzed liquor comprising hemicellulosic monomers; hydrolyzing the cellulose-rich solids to produce glucose, using cellulase enzymes or an acid or base hydrolysis catalyst; enzymatically isomerizing the glucose to fructose, using glucose isomerase enzymes; and recovering the fructose in purified form or in a fructose-glucose solution. The cellulosic fructose produced by the disclosed processes has many uses.

    Abstract translation: 一些变体提供了用于从生物质生产纤维素果糖的方法，包括：在酸催化剂，木质素和水的溶剂存在下分解生物质原料，以产生含有富含纤维素的固体，木质素和溶解的半纤维素的液体; 从液体中除去富含纤维素的固体; 水解包含在液体中的溶解的半纤维素，以产生包含半纤维素单体的水解液; 使用纤维素酶或酸或碱水解催化剂水解富含纤维素的固体以产生葡萄糖; 使用葡萄糖异构酶酶将葡萄糖酶促异构化成果糖; 并回收纯化形式的果糖或果糖 - 葡萄糖溶液。 由所公开的方法生产的纤维素果糖具有许多用途。

    Process for converting bio-oil
    88.
    发明授权
    Process for converting bio-oil 有权
    转化生物油的方法

    公开(公告)号：US09187444B2

    公开(公告)日：2015-11-17

    申请号：US14202372

    申请日：2014-03-10

    Applicant: UPM-Kymmene Corporation

    Inventor： Janne Asikkala ,  Andrea Gutierrez

    IPC: C07C67/00 ,  C07D307/42 ,  C07C27/00 ,  C10L1/02

    CPC classification number: C07D307/42 ,  B01D3/36 ,  C07C27/00 ,  C10L1/02

    Abstract: Disclosed is a process for converting bio-oil, wherein the process includes the steps, where a feedstock including bio-oil selected from bio-oils, any fractions of bio-oils and any combinations thereof is subjected to azeotropic distillation with at least one alcohol to yield a liquid component, and subjecting the liquid component to alcoholysis whereby converted bio-oil is obtained. The invention also relates to the use of converted bio-oil, obtainable by the process, as heating oil, as starting material in processes for producing fuels, fuel components, fine chemicals, chemical building-blocks, and solvents.

    Abstract translation: 公开了一种转化生物油的方法，其中该方法包括以下步骤：其中将包含生物油，生物油的任何馏分及其任何组合的生物油的原料与至少一种醇进行共沸蒸馏 得到液体成分，使液体成分进行醇解，得到转化后的生物油。 本发明还涉及在生产燃料，燃料组分，精细化学品，化学结构单元和溶剂的方法中作为加热油作为起始原料的方法可获得的转化生物油的用途。

    Torrefaction reduction of coke formation on catalysts used in esterification and cracking of biofuels from pyrolysed lignocellulosic feedstocks
    89.
    发明授权
    Torrefaction reduction of coke formation on catalysts used in esterification and cracking of biofuels from pyrolysed lignocellulosic feedstocks 有权
    在热解木质纤维素原料的生物燃料的酯化和裂化中使用的催化剂上焦炭形成的脱蜡减少

    公开(公告)号：US09175235B2

    公开(公告)日：2015-11-03

    申请号：US14080153

    申请日：2013-11-14

    Applicant: University of Georgia Research Foundation, Inc.

    Inventor： James R. Kastner ,  Sudhagar Mani ,  Roger Hilten ,  Keshav C. Das

    IPC: C10L1/02 ,  C10G1/00

    CPC classification number: C10L1/02 ,  C10G1/002

    Abstract: A bio-oil production process involving torrefaction pretreatment, catalytic esterification, pyrolysis, and secondary catalytic processing significantly reduces yields of reactor char, catalyst coke, and catalyst tar relative to the best-case conditions using non-torrefied feedstock. The reduction in coke as a result of torrefaction was 28.5% relative to the respective control for slow pyrolysis bio-oil upgrading. In fast pyrolysis bio-oil processing, the greatest reduction in coke was 34.9%. Torrefaction at 275° C. reduced levels of acid products including acetic acid and formic acid in the bio-oil, which reduced catalyst coking and increased catalyst effectiveness and aromatic hydrocarbon yields in the upgraded oils. The process of bio-oil generation further comprises a catalytic esterification of acids and aldehydes to generate such as ethyl levulinate from lignified biomass feedstock.

    Abstract translation: 包括烘焙预处理，催化酯化，热解和二次催化处理的生物油生产过程相对于使用非烘焙原料的最佳情况，显着降低了反应器焦炭，催化剂焦炭和催化剂焦油的产率。 相对于缓慢裂解生物油升级的相应对照，由于焙烧而导致的焦炭减少量为28.5％。 在快速热解生物油加工中，焦炭最大减少了34.9％。 在275℃烘烤，生物油中酸产物（包括乙酸和甲酸）的水平降低，这降低了催化剂焦化，提高了催化剂的有效性和改性油中的芳烃产率。 生物油生成的过程还包括酸和醛的催化酯化以从木质素生物质原料产生乙酰乙酸乙酯。

    Methods for hydrothermal digestion of cellulosic biomass solids in the presence of a slurry catalyst and a digestible filter aid
    90.
    发明授权
    Methods for hydrothermal digestion of cellulosic biomass solids in the presence of a slurry catalyst and a digestible filter aid 有权
    在浆料催化剂和可消化助滤剂存在下水热消化纤维素生物质固体的方法

    公开(公告)号：US09174898B2

    公开(公告)日：2015-11-03

    申请号：US13928877

    申请日：2013-06-27

    Applicant: SHELL OIL COMPANY

    Inventor： Glenn Charles Komplin ,  Joseph Broun Powell

    IPC: C07C27/00 ,  C07C29/132 ,  C13K1/02 ,  D21C3/22 ,  C10L1/02 ,  C10L9/08 ,  C10G3/00

    CPC classification number: C07C29/132 ,  C10G3/42 ,  C10G3/52 ,  C10G3/56 ,  C10G2300/1011 ,  C10G2300/1014 ,  C10G2400/02 ,  C10L1/02 ,  C10L1/026 ,  C10L9/086 ,  C13K1/02 ,  D21C3/222 ,  Y02E50/10 ,  Y02E50/30 ,  Y02P30/20 ,  Y02T50/678

    Abstract: Digesting cellulosic biomass in the presence of a slurry catalyst may reduce degradation product formation, but catalyst distribution and retention can be problematic. Digestion methods can comprise: providing cellulosic biomass solids and a slurry catalyst capable of activating molecular hydrogen in a digestion unit; providing a digestible filter aid in the digestion unit; distributing the slurry catalyst within the cellulosic biomass solids using fluid flow; retaining at least a portion of the slurry catalyst in a fixed location using the digestible filter aid; heating the cellulosic biomass solids in the presence of the slurry catalyst, a digestion solvent, and molecular hydrogen, thereby forming a liquor phase comprising soluble carbohydrates; and performing a catalytic reduction reaction on the soluble carbohydrates within the digestion unit, thereby at least partially forming a reaction product comprising a triol, a diol, a monohydric alcohol, or any combination thereof in the digestion unit.

    Abstract translation: 在淤浆催化剂存在下消化纤维素生物质可能会降低产物的形成，但催化剂的分布和保留可能是有问题的。 消化方法可以包括：提供纤维素生物质固体和能够在消化单元中活化分子氢的淤浆催化剂; 在消化单元中提供可消化的助滤剂; 使用流体流将浆料催化剂分散在纤维素生物质固体内; 使用可消化助滤剂将至少一部分浆料催化剂保持在固定位置; 在淤浆催化剂，消化溶剂和分子氢的存在下加热纤维素生物质固体，从而形成包含可溶性碳水化合物的液相; 并对消化单元内的可溶性碳水化合物进行催化还原反应，由此在消化单元中至少部分地形成包含三醇，二醇，一元醇或其任何组合的反应产物。

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