公开(公告)号：US08629222B2

公开(公告)日：2014-01-14

申请号：US12935116

申请日：2009-03-27

申请人： Kenichi Takizawa ,  Yoshiaki Koyashiki ,  Hiroshi Kobayashi ,  Masahito Shinbara ,  Hanako Kato ,  Mari Abe ,  Masanori Yamazaki ,  Yutaka Mori

发明人： Kenichi Takizawa ,  Yoshiaki Koyashiki ,  Hiroshi Kobayashi ,  Masahito Shinbara ,  Hanako Kato ,  Mari Abe ,  Masanori Yamazaki ,  Yutaka Mori

IPC分类号： C08G77/12 ,  C08F283/12

CPC分类号： C08L83/04 ,  C08G77/12 ,  C08G77/16 ,  C08G77/18 ,  C08G77/20 ,  C08L83/06 ,  H01L23/296 ,  H01L2224/45144 ,  H01L2224/48091 ,  H01L2224/48227 ,  H01L2224/48247 ,  H01L2224/48257 ,  H01L2224/49107 ,  H01L2224/73265 ,  H01L2924/12044 ,  H01L2924/181 ,  H01L2924/3025 ,  H01L2924/00014 ,  H01L2924/00 ,  H01L2924/00012

摘要： The present invention provides a curable polysiloxane composition which is excellent in light resistance (particularly ultraviolet resistance) and adhesion and has a sufficient heat resistance/hydrothermal resistance and film-forming property and which generates little foaming at curing and does not generate cracks, peeling, coloring, and foaming even when used for a long period of time. A curable polysiloxane composition which comprises a specific hydrosilyl group-containing polysiloxane compound, a specific polysiloxane compound comprising two or more silanol groups in one molecule, and a dehydrogenative condensation reaction catalyst.

摘要翻译： 本发明提供耐光性（特别是耐紫外线性）和粘合性优异且具有充分的耐热/耐热水性和成膜性的固化型聚硅氧烷组合物，其固化发泡少，不产生裂纹，剥离， 着色和发泡，即使长时间使用也是如此。 一种可固化聚硅氧烷组合物，其包含特定含氢硅烷基的聚硅氧烷化合物，在一个分子中包含两个或更多个硅烷醇基团的特定聚硅氧烷化合物和脱氢缩合反应催化剂。

公开(公告)号：US5733644A

公开(公告)日：1998-03-31

申请号：US722140

申请日：1997-01-07

申请人： Seiichiro Tanaka ,  Hanako Kato ,  Takeshi Sawai ,  Nobuyuki Matsuzoe ,  Kenji Oba ,  Yukio Kajiwara ,  Hozumi Endo

发明人： Seiichiro Tanaka ,  Hanako Kato ,  Takeshi Sawai ,  Nobuyuki Matsuzoe ,  Kenji Oba ,  Yukio Kajiwara ,  Hozumi Endo

IPC分类号： C08L83/02 ,  C08L83/16 ,  C09D183/02 ,  C09D183/10 ,  C09D183/16 ,  B32B7/02

CPC分类号： C09D183/02 ,  C08L83/02 ,  C08L83/16 ,  C09D183/10 ,  C09D183/16 ,  Y10T428/24967

摘要： A curable composition comprising an aged mixture of tetramethoxysilane with water added in excess of the theoretical amount sufficient for the hydrolysis and condensation of 100% of the silane and a reactive organic compound having at least two functional groups capable of condensing with the product of hydrolysis and condensation of the silane in the above mixture.

摘要翻译： PCT No.PCT / JP95 / 00746 Sec。 371日期1997年1月7日 102（e）日期1997年1月7日PCT 1995年4月15日PCT PCT。 公开号WO95 / 28445 日期1995年10月26日一种可固化组合物，其包含四甲氧基硅烷的老化混合物和超过足以使100％硅烷水解和缩合的理论量的水与具有至少两个能够与 在上述混合物中硅烷的水解和缩合产物。

公开(公告)号：US07859006B2

公开(公告)日：2010-12-28

申请号：US11816640

申请日：2006-02-23

申请人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

发明人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

IPC分类号： H01L33/00

CPC分类号： H01L33/56 ,  C08G77/04 ,  H01L2224/45144 ,  H01L2224/48091 ,  H01L2224/49107 ,  H01L2924/00014 ,  H01L2924/00

摘要： A semiconductor light-emitting device member excellent in transparency, light resistance, and heat resistance and capable of sealing a semiconductor light-emitting device without causing cracks and peeling even after a long-time use is provided wherein the semiconductor light-emitting device member contains (A) in a solid Si-nuclear magnetic resonance spectrum, at least one peak selected from (a) peaks whose peak top position is in an area of a chemical shift of −40 ppm to 0 ppm inclusive, and whose full width at half maximum is 0.3 ppm to 3.0 ppm inclusive, and (b) peaks whose peak top position is in an area of the chemical shift of −80 ppm or more and less than −40 ppm, and whose full width at half maximum is 0.3 ppm to 5.0 ppm inclusive, wherein (B) silicon content is 20 weight % or more and (C) silanol content is 0.1 weight % to 10 weight % inclusive.

摘要翻译： 提供透明性，耐光性和耐热性优异的半导体发光元件，即使长时间使用也能够密封半导体发光元件而不引起裂纹和剥离的半导体发光元件，其中半导体发光元件 （A）在固体Si核磁共振谱中，至少一个峰选自（a）峰顶位置在-40ppm至0ppm的化学位移范围内的峰，并且其全宽为一半 最大值为0.3ppm〜3.0ppm，（b）峰顶位置在-80ppm以上且小于-40ppm的化学位移范围内，峰值全宽度为0.3ppm〜 5.0ppm，其中（B）硅含量为20重量％以上，（C）硅烷醇含量为0.1重量％〜10重量％。

公开(公告)号：US06838068B2

公开(公告)日：2005-01-04

申请号：US09891412

申请日：2001-06-27

申请人： Yoshio Katsuro ,  Takashi Yamaguchi ,  Takayuki Yoshimori ,  Hanako Kato

发明人： Yoshio Katsuro ,  Takashi Yamaguchi ,  Takayuki Yoshimori ,  Hanako Kato

IPC分类号： C01B33/16 ,  C01B33/12

CPC分类号： C01B33/163

摘要： A method of producing a silica gel by hydrolyzing a silicon alkoxide and subjecting the resulting hydrogel to a hydrothermal treatment substantially without aging it is described. Also described in a silica gel produced by such a method and a silica gel which has the following characteristics: (a) the pore volume is from 0.6 to 1.6 ml/g, (b) the specific surface area is from 300 to 900 m2/g, (c) the mode diameter (Dmax) of pores is less than 20 nm, (d) the volume of pores having diameters within ±20% of Dmax is at least 50% of the total pore volume, (e) it is amorphous, and (f) the content of metal impurities is at most 500 ppm.

摘要翻译： 描述了通过水解硅醇盐并使所得水凝胶基本上不老化而进行水热处理来生产硅胶的方法。 还描述在通过这种方法制备的硅胶和具有以下特征的硅胶中：（a）孔体积为0.6至1.6ml / g，（b）比表面积为300至900μm， （c）孔的模式直径（Dmax）小于20nm，（d）直径在±20％以内的孔的体积为总孔体积的至少50％，（e ）为非晶态，（f）金属杂质含量为500ppm以下。

公开(公告)号：US06258969B1

公开(公告)日：2001-07-10

申请号：US08726301

申请日：1996-10-02

申请人： Takeshi Sawai ,  Hanako Kato ,  Seiichiro Tanaka ,  Akihiro Takazawa ,  Haruo Katsumata ,  Hozumi Endo

发明人： Takeshi Sawai ,  Hanako Kato ,  Seiichiro Tanaka ,  Akihiro Takazawa ,  Haruo Katsumata ,  Hozumi Endo

IPC分类号： C07F708

CPC分类号： C08G77/42 ,  C08G77/02 ,  C08G77/22 ,  C09D183/02

摘要： A polyalkoxysiloxane of the following rational formula: SiOa(OR)b(OH)c wherein R is a C1-4 alkyl group, a=0.86 to 1.30, b=2.18 to 1.30, and c≦0.10.

摘要翻译： 一种以下合理式的聚烷氧基硅氧烷：其中R为C 1-4烷基，a = 0.86至1.30，b = 2.18至1.30，c <0.10。

公开(公告)号：US08759840B2

公开(公告)日：2014-06-24

申请号：US12950128

申请日：2010-11-19

申请人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

发明人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

IPC分类号： H01L27/15

CPC分类号： H01L33/56 ,  C08G77/04 ,  H01L2224/45144 ,  H01L2224/48091 ,  H01L2224/49107 ,  H01L2924/00014 ,  H01L2924/00

摘要： A semiconductor light-emitting device member excellent in transparency, light resistance, and heat resistance and capable of sealing a semiconductor light-emitting device without causing cracks and peeling even after a long-time use is provided wherein the semiconductor light-emitting device member contains (A) in a solid state Si-nuclear magnetic resonance spectrum, at least one peak selected from (a) peaks whose peak top position is in an area of a chemical shift of −40 ppm to 0 ppm inclusive, and whose full width at half maximum is 0.3 ppm to 3.0 ppm inclusive, and (b) peaks whose peak top position is in an area of the chemical shift of −80 ppm or more and less than −40 ppm, and whose full width at half maximum is 0.3 ppm to 5.0 ppm inclusive, wherein (B) silicon content is 20 weight % or more and (C) silanol content is 0.1 weight % to 10 weight % inclusive.

摘要翻译： 提供透明性，耐光性和耐热性优异的半导体发光元件，即使长时间使用也能够密封半导体发光元件而不引起裂纹和剥离的半导体发光元件，其中半导体发光元件 （A）为固态Si核磁共振谱，选自（a）峰顶位于-40ppm〜0ppm的化学位移范围内的峰的至少一个峰，其全宽度 半峰值为0.3ppm〜3.0ppm，（b）峰顶位置在-80ppm以上且小于-40ppm的化学位移范围内，峰值全差为0.3ppm的峰 至5.0ppm，其中（B）硅含量为20重量％以上，（C）硅烷醇含量为0.1重量％〜10重量％。

公开(公告)号：US08502364B2

公开(公告)日：2013-08-06

申请号：US12438283

申请日：2007-08-22

申请人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

发明人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

IPC分类号： H01L35/24 ,  H01L31/0312 ,  H01L23/58 ,  H01L23/02 ,  H01L51/00

CPC分类号： C09K11/7774 ,  C09K11/7721 ,  C09K11/7734 ,  C09K11/7735 ,  C09K11/7738 ,  C09K11/774 ,  C09K11/7775 ,  C09K11/7781 ,  C09K11/7789 ,  C09K11/7794 ,  C09K11/7795 ,  H01L23/24 ,  H01L23/293 ,  H01L24/17 ,  H01L33/507 ,  H01L33/54 ,  H01L33/58 ,  H01L2224/32245 ,  H01L2224/32257 ,  H01L2224/45144 ,  H01L2224/48091 ,  H01L2224/48227 ,  H01L2224/48247 ,  H01L2224/48257 ,  H01L2224/49107 ,  H01L2224/73265 ,  H01L2224/8592 ,  H01L2924/01004 ,  H01L2924/01012 ,  H01L2924/01019 ,  H01L2924/0102 ,  H01L2924/01021 ,  H01L2924/01025 ,  H01L2924/01046 ,  H01L2924/01057 ,  H01L2924/01063 ,  H01L2924/01066 ,  H01L2924/01067 ,  H01L2924/01068 ,  H01L2924/01077 ,  H01L2924/01078 ,  H01L2924/01079 ,  H01L2924/01322 ,  H01L2924/10253 ,  H01L2924/12041 ,  H01L2924/12042 ,  H01L2924/181 ,  H01L2924/19041 ,  H01L2924/00014 ,  H01L2924/00 ,  H01L2924/00012

摘要： To provide a semiconductor device member that is superior in heat resistance, light resistance, film-formation capability and adhesion, and is capable of sealing a semiconductor device and holding a phosphor without causing cracks, peelings and colorings even after used for a long period of time, the weight loss at the time of heating, measured by a predetermined weight-loss at-the-time-of-heating measurement method, is 50 weight % or lower and the ratio of peeling, measured by a predetermined adhesion evaluation method, is 30% or lower, in the semiconductor device member.

摘要翻译： 为了提供耐热性，耐光性，成膜性和粘合性优异的半导体器件部件，并且即使在长时间使用之后也能够密封半导体器件和保持荧光体而不引起裂纹，剥离和着色 时间，通过预定的加热温度测量方法的重量损失测量的加热时的重量损失为50重量％以下，通过预定的粘合性评价方法测定的剥离比例， 在半导体器件部件中为30％以下。

公开(公告)号：US20090309116A1

公开(公告)日：2009-12-17

申请号：US12438283

申请日：2007-08-22

申请人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

发明人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

IPC分类号： H01L33/00 ,  C09K11/02

CPC分类号： C09K11/7774 ,  C09K11/7721 ,  C09K11/7734 ,  C09K11/7735 ,  C09K11/7738 ,  C09K11/774 ,  C09K11/7775 ,  C09K11/7781 ,  C09K11/7789 ,  C09K11/7794 ,  C09K11/7795 ,  H01L23/24 ,  H01L23/293 ,  H01L24/17 ,  H01L33/507 ,  H01L33/54 ,  H01L33/58 ,  H01L2224/32245 ,  H01L2224/32257 ,  H01L2224/45144 ,  H01L2224/48091 ,  H01L2224/48227 ,  H01L2224/48247 ,  H01L2224/48257 ,  H01L2224/49107 ,  H01L2224/73265 ,  H01L2224/8592 ,  H01L2924/01004 ,  H01L2924/01012 ,  H01L2924/01019 ,  H01L2924/0102 ,  H01L2924/01021 ,  H01L2924/01025 ,  H01L2924/01046 ,  H01L2924/01057 ,  H01L2924/01063 ,  H01L2924/01066 ,  H01L2924/01067 ,  H01L2924/01068 ,  H01L2924/01077 ,  H01L2924/01078 ,  H01L2924/01079 ,  H01L2924/01322 ,  H01L2924/10253 ,  H01L2924/12041 ,  H01L2924/12042 ,  H01L2924/181 ,  H01L2924/19041 ,  H01L2924/00014 ,  H01L2924/00 ,  H01L2924/00012

摘要： To provide a semiconductor device member that is superior in heat resistance, light resistance, film-formation capability and adhesion, and is capable of sealing a semiconductor device and holding a phosphor without causing cracks, peelings and colorings even after used for a long period of time, the weight loss at the time of heating, measured by a predetermined weight-loss at-the-time-of-heating measurement method, is 50 weight % or lower and the ratio of peeling, measured by a predetermined adhesion evaluation method, is 30% or lower, in the semiconductor device member.

摘要翻译： 为了提供耐热性，耐光性，成膜性和粘合性优异的半导体器件部件，并且即使在长时间使用之后也能够密封半导体器件和保持荧光体而不引起裂纹，剥离和着色 时间，通过预定的加热温度测量方法的重量损失测量的加热时的重量损失为50重量％以下，通过预定的粘合性评价方法测定的剥离比例， 在半导体器件部件中为30％以下。

公开(公告)号：US06291697B1

公开(公告)日：2001-09-18

申请号：US09155209

申请日：1998-11-09

申请人： Seiichirou Tanaka ,  Hanako Kato ,  Takeshi Sawai ,  Kenji Oba ,  Hozumi Endo ,  Haruo Katsumata

发明人： Seiichirou Tanaka ,  Hanako Kato ,  Takeshi Sawai ,  Kenji Oba ,  Hozumi Endo ,  Haruo Katsumata

IPC分类号： C07F708

CPC分类号： C08G77/02 ,  C08G77/16 ,  C08G77/18 ,  C09D183/02

摘要： The siloxane compounds represented by the following formula: SiOa(OH)b(OR1)c(OR2)d wherein 1.0≦a≦1.6, 0≦b

摘要翻译： 由下式表示的硅氧烷化合物：其中1.0 <= a <= 1.6,0 <= b <0.3,0.2 <= c <2.0,0 <= d <= 1.4,2a + b + c + d = 4 R1是甲基或乙基，R2是与R1不同的有机基团。

公开(公告)号：US20110121321A1

公开(公告)日：2011-05-26

申请号：US12950128

申请日：2010-11-19

申请人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

发明人： Hanako Kato ,  Yutaka Mori ,  Hiroshi Kobayashi ,  Tsubasa Tomura

IPC分类号： H01L33/52

CPC分类号： H01L33/56 ,  C08G77/04 ,  H01L2224/45144 ,  H01L2224/48091 ,  H01L2224/49107 ,  H01L2924/00014 ,  H01L2924/00

摘要： A semiconductor light-emitting device member excellent in transparency, light resistance, and heat resistance and capable of sealing a semiconductor light-emitting device without causing cracks and peeling even after a long-time use is provided wherein the semiconductor light-emitting device member contains (A) in a solid state Si-nuclear magnetic resonance spectrum, at least one peak selected from (a) peaks whose peak top position is in an area of a chemical shift of −40 ppm to 0 ppm inclusive, and whose full width at half maximum is 0.3 ppm to 3.0 ppm inclusive, and (b) peaks whose peak top position is in an area of the chemical shift of −80 ppm or more and less than −40 ppm, and whose full width at half maximum is 0.3 ppm to 5.0 ppm inclusive, wherein (B) silicon content is 20 weight % or more and (C) silanol content is 0.1 weight % to 10 weight % inclusive.

摘要翻译： 提供透明性，耐光性和耐热性优异的半导体发光元件，即使长时间使用也能够密封半导体发光元件而不引起裂纹和剥离的半导体发光元件，其中半导体发光元件 （A）为固态Si核磁共振谱，选自（a）峰顶位于-40ppm〜0ppm的化学位移范围内的峰的至少一个峰，其全宽度 半峰值为0.3ppm〜3.0ppm，（b）峰顶位置在-80ppm以上且小于-40ppm的化学位移范围内，峰值全差为0.3ppm的峰 至5.0ppm，其中（B）硅含量为20重量％以上，（C）硅烷醇含量为0.1重量％〜10重量％。