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    Methods of making an antistatic agent
    2.
    发明申请
    Methods of making an antistatic agent 有权
    制造抗静电剂的方法

    公开(公告)号：US20050228194A1

    公开(公告)日：2005-10-13

    申请号：US10966774

    申请日：2004-10-15

    申请人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    发明人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    IPC分类号： C07C303/32 ,  C07C309/06 ,  C07F9/54 ,  C07C39/02 ,  C07F9/02

    CPC分类号： C07C303/32 ,  C08K5/50 ,  Y10S524/912 ,  C07C309/06

    摘要： A method for making the phosphonium sulfonate salt of generic formula (1): wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is not zero then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms, the method comprising combining in an aqueous medium a compound of generic formula (2): wherein M is Li or Na, and X, q, p, and r are as defined above, with a stoichiometric excess of a compound of the generic formula (3): (R)4P-Z  (3) wherein Z is a halogen and R is as defined above; and separating the product of formula (1) from the medium.

    摘要翻译： 制备通式（1）的鏻磺酸盐的方法：其中每个X独立地为卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p不为零，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基，该方法包括在水性介质中混合通式（2）的化合物：其中M是Li或Na，X，q，p和 r如上所定义，化学计量过量的通式（3）的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”→（R） PZ（3）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上定义; 和将式（1）的产物与介质分离。

    METHOD OF MAKING A THERMOPLASTIC COMPOSITION CONTAINING AN ANTISTATIC AGENT
    3.
    发明申请
    METHOD OF MAKING A THERMOPLASTIC COMPOSITION CONTAINING AN ANTISTATIC AGENT 有权
    制备含有抗静电剂的热塑性组合物的方法

    公开(公告)号：US20080081857A1

    公开(公告)日：2008-04-03

    申请号：US11869338

    申请日：2007-10-09

    申请人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    发明人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    IPC分类号： C08G64/00 ,  C08K5/51

    CPC分类号： C07C303/32 ,  C08K5/50 ,  Y10S524/912 ,  C07C309/06

    摘要： A method for preparing a thermoplastic composition containing an antistatic agent is described. The antistatic agent is a phosphonium sulfonate salt of generic formula (1) wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is not zero then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms. The phosphonium sulfonate salt is prepared by a method that includes combining in an aqueous medium sodium hydroxide and/or lithium hydroxide, a compound of the generic formula (4) wherein X, q, p, and r are as defined above, and a compound of the generic formula (3) (R)4P-Z  (3) wherein Z is a halogen and R is as defined above; and separating the phosphonium sulfonate of formula (1) from the aqueous medium. The phosphonium sulfonate salt is then combined with a thermoplastic resin.

    摘要翻译： 描述了制备含有抗静电剂的热塑性组合物的方法。 抗静电剂是通式（1）的鏻磺酸盐，其中每个X独立地是卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p不为零，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基。 鏻磺酸盐通过包括在水性介质氢氧化钠和/或氢氧化锂中组合其中X，q，p和r如上定义的通式（4）的化合物和化合物 通用公式（3）<？in-line-formula description =“In-line Formulas”end =“lead”？>（R）（3） formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上定义; 并将式（1）的磺酸鏻与水性介质分离。 然后将鏻磺酸盐与热塑性树脂组合。

    Methods of making an antistatic agent
    7.
    发明申请
    Methods of making an antistatic agent 审中-公开
    制造抗静电剂的方法

    公开(公告)号：US20060100327A1

    公开(公告)日：2006-05-11

    申请号：US10983878

    申请日：2004-11-08

    申请人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    发明人： Theodorus Hoeks ,  Chiel Leenders ,  Robert van de Grampel

    IPC分类号： C08K5/49

    CPC分类号： C07C303/32 ,  C07F9/5407 ,  C07C309/06 ,  C07C309/10

    摘要： Disclosed are methods for making the phosphonium sulfonate salt of generic formula (1): wherein each X is independently a halogen or hydrogen, provided that the molar ratio of halogen to hydrogen is greater than about 0.90; p is 0 or 1 and q and r are integers of 0 to about 7 provided that q+r is less than 8 and that if p is 1 then r is greater than zero; and each R is the same or different hydrocarbon radical containing 1 to about 18 carbon atoms, the method comprising the steps of combining in an aqueous medium, a compound of the generic formula (2): wherein M is K, and X, q, p, and r are as defined above, with a compound of the generic formula (3): (R)4P-Z  (3) wherein Z is a halogen and R is as defined above; and separating the phosphonium sulfonate of formula (1) from the aqueous medium. Also disclosed is an antistatic composition comprising phosphonium sulfonate (1), and articles prepared therefrom.

    摘要翻译： 公开了制备通式（1）的鏻磺酸盐的方法：其中每个X独立地是卤素或氢，条件是卤素与氢的摩尔比大于约0.90; p为0或1，q和r为0至约7的整数，条件是q + r小于8，如果p为1，则r大于零; 并且每个R是含有1至约18个碳原子的相同或不同的烃基，该方法包括以下步骤：在水性介质中混合通式（2）的化合物：其中M是K，X，q， p和r如上所定义，与通式（3）的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？（R） PZ（3）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中Z是卤素，R如上所定义; 并将式（1）的磺酸鏻与水性介质分离。 还公开了包含磺酸鏻（1）和由其制备的制品的抗静电组合物。