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    Solid state extension method
    5.
    发明授权
    Solid state extension method 失效
    固态扩展方法

    公开(公告)号：US6017682A

    公开(公告)日：2000-01-25

    申请号：US979382

    申请日：1997-11-26

    申请人： Marie Angelopoulos ,  Claudius Feger ,  Jeffrey Donald Gelorme ,  Jane Margaret Shaw

    发明人： Marie Angelopoulos ,  Claudius Feger ,  Jeffrey Donald Gelorme ,  Jane Margaret Shaw

    IPC分类号： G03F7/004 ,  G03F7/038 ,  G03F7/40

    CPC分类号： G03F7/0387 ,  G03F7/0045 ,  Y10S430/143 ,  Y10S430/167

    摘要： A solid state chain extension method provides for the formation of a solid state film comprised of a high molecular weight polymer by chain extending a deblocked Lewis base with Lewis acid oligomers while the reactants are in a solid state form. In one embodiment, a negative resist is prepared by selectively exposing regions of the solid state film. The Lewis base is deblocked at the exposed regions by a suitable deblocking means. The Lewis acid oligomers and the deblocked Lewis base chain extend at the exposed regions. Development of the film removes the non-polymerized reactants. Optionally, the Lewis acid oligomers, when radiation-cross-linking, are cross-linked with one another prior to deblocking the Lewis base to form a negative resist. The cross-linked oligomers polymerize with the subsequently deblocked base to provide a high molecular weight polymer film. In an alternative embodiment, a positive resist is used by degrading and removing photo-sensitive Lewis acid oligomers using selective exposure lithography techniques and, subsequently, deblocking the Lewis base and chain extending the remaining oligomers with the deblocked Lewis base at the unexposed regions.

    摘要翻译： 固态链延伸方法提供了通过将路易斯酸低聚物链路延伸解链路易斯碱同时反应物呈固态形式形成由高分子量聚合物构成的固态膜。 在一个实施方案中，通过选择性地暴露固态膜的区域来制备负性抗蚀剂。 路易斯碱通过合适的去块装置在暴露区域解封。 路易斯酸低聚物和解封的路易斯碱基链在暴露的区域延伸。 膜的开发除去未聚合的反应物。 任选地，当辐射交联时，路易斯酸低聚物在将路易斯碱解封以形成负性抗蚀剂之前彼此交联。 交联的低聚物与随后的解封底物聚合以提供高分子量聚合物膜。 在替代实施方案中，通过使用选择性曝光光刻技术降解和除去光敏路易斯酸低聚物，然后使路易斯碱和链在未曝光区域上与解封的路易斯碱扩展剩余的低聚物链，使用正性抗蚀剂。

    Vibrational methods of deaggregation of electrically conductive polymers and precursors thereof
    7.
    发明授权
    Vibrational methods of deaggregation of electrically conductive polymers and precursors thereof 有权
    导电聚合物及其前体解聚的振动方法

    公开(公告)号：US6099756A

    公开(公告)日：2000-08-08

    申请号：US43623

    申请日：1998-10-02

    申请人： Marie Angelopoulos ,  Richard Anthony DiPietro ,  Jane Margaret Shaw

    发明人： Marie Angelopoulos ,  Richard Anthony DiPietro ,  Jane Margaret Shaw

    IPC分类号： C08G61/12 ,  C08G73/02 ,  H01B1/12

    CPC分类号： C08G61/12 ,  C08G61/122 ,  C08G73/0266 ,  H01B1/128

    摘要： The instant invention is drawn vibrational methods of deaggregating electrically conductive polymers. Said methods include the steps of:I) providing an intrinsically conductive polymer comprising a specific morphology;II) determining by experimental or theoretical means a desired degree of aggregation for said intrinsically conductive polymer;III) agitating said intrinsically conductive polymer by a method selected from the group consisting of ultrasound, vibration, shear mixing and cavitation, said agitation being performed at a rate sufficient to achieve the determined degree of aggregation.

    摘要翻译： PCT No.PCT / US97 / 13377 Sec。 371日期：1998年10月2日 102（e）1998年10月2日PCT PCT 1997年7月24日PCT公布。 公开号WO98 / 05043 日期1998年2月5日本发明是拉伸导电聚合物解聚的振动方法。 所述方法包括以下步骤：I）提供包含特定形态的固有导电聚合物; II）通过实验或理论手段确定所述固有导电聚合物所需的聚集度; III）通过选自超声，振动，剪切混合和空化的方法搅拌所述固有导电聚合物，所述搅拌以足以达到确定的聚集度的速率进行。

    Vibrational methods of deaggregation of electrically conductive polymers and precursors thereof
    9.
    发明授权
    Vibrational methods of deaggregation of electrically conductive polymers and precursors thereof 有权
    导电聚合物及其前体解聚的振动方法

    公开(公告)号：US6139778A

    公开(公告)日：2000-10-31

    申请号：US521481

    申请日：2000-03-09

    申请人： Marie Angelopoulos ,  Richard Anthony DiPietro ,  Jane Margaret Shaw

    发明人： Marie Angelopoulos ,  Richard Anthony DiPietro ,  Jane Margaret Shaw

    IPC分类号： C08G61/12 ,  C08G73/02 ,  H01B1/12

    CPC分类号： C08G61/12 ,  C08G61/122 ,  C08G73/0266 ,  H01B1/128

    摘要： The present invention is directed to vibrational methods of fabricating electrically conducting polymers and precursors thereof in which the polymer chains are deaggregated. Such deaggregated conducting polymers and precursors thereof exhibit better solution processability and higher electrical conductivity than do the corresponding aggregated polymers. The polymers in the non-doped precursor form or in the conducting form in solution or during the polymerization process are exposed to ultrasound and shear mixing. Due to this treatment, the chains become deaggregated. Furthermore, ultrasound and shear mixing is used during the doping of the precursor polymers. This treatment allows more uniform doping, enhanced solubility, and higher electrical conductivity. The solutions treated with ultrasound/shear mixing are subsequently processed into a structural part, a film, or a fiber.

    摘要翻译： 本发明涉及制造其中聚合物链解聚的导电聚合物及其前体的振动方法。 这种解聚集的导电聚合物及其前体与相应的聚合聚合物相比表现出更好的溶液加工性能和更高的电导率。 在溶液中或在聚合过程中，非掺杂前体形式或导电形式的聚合物暴露于超声和剪切混合。 由于这种处理，链变得解聚。 此外，在掺杂前体聚合物期间使用超声和剪切混合。 该处理允许更均匀的掺杂，增强的溶解度和更高的导电性。 用超声/剪切混合处理的溶液随后加工成结构部分，薄膜或纤维。