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公开(公告)号：US5695617A
公开(公告)日：1997-12-09
申请号：US561771
申请日：1995-11-22
CPC分类号： H01L33/346
摘要： A web-like nanoparticle silicon is produced by laser vaporization of silicon metal in an oxygen-free atmosphere in a diffusion cloud chamber where it aggregates into novel web-like microstructures. The aggregates are porous, and bright yellow to orange photoluminescence from the web-like nanoparticle silicon is observed upon irradiation with ultraviolet light.
摘要翻译： 通过在扩散云室中的无氧气氛中通过硅金属的激光蒸发来生产网状纳米颗粒硅，其中它聚集成新的网状微结构。 聚集体是多孔的，并且在用紫外线照射时观察到来自网状纳米颗粒硅的明亮的黄色至橙色的光致发光。
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公开(公告)号：US6136156A
公开(公告)日：2000-10-24
申请号：US813626
申请日：1997-07-14
CPC分类号： B01J37/349 , B01J37/0238 , B01J35/0013
摘要： Nanoparticles of silicon oxide alloys (i.e., oxides of SiMo, SiPt, and SiAl) are produced by laser vaporization of a silicon target and a target of a metal (i.e., Mo, Pt, or Al), in an oxygen containing atmosphere in a diffusion cloud chamber, where the target metal vapors aggregate into novel three-dimensional porous web structures. The structures have a homogeneous composition with a uniform ratio of silicon to the metal.
摘要翻译： 氧化硅合金（即，SiMo，SiPt和SiAl的氧化物）的纳米颗粒是通过在含氧气氛中的硅靶和金属靶（即Mo，Pt或Al）的激光蒸发产生的 扩散云室，其中目标金属蒸气聚集成新颖的三维多孔网状结构。 该结构具有均匀的硅与金属比例的组成。
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公开(公告)号：US5891548A
公开(公告)日：1999-04-06
申请号：US725044
申请日：1996-10-03
申请人： Daniel Graiver , Udo C. Pernisz
发明人： Daniel Graiver , Udo C. Pernisz
IPC分类号： B32B5/16 , B32B5/18 , C08K9/06 , C08K9/08 , C08L83/07 , C09C1/30 , C09D183/07 , C09K11/00 , C09K11/08 , C09K11/59 , B32B5/00 , C08L83/00
CPC分类号： B82Y30/00 , C08K9/06 , C08K9/08 , C09C1/3081 , C01P2002/82 , C01P2002/84 , C01P2004/03 , C01P2004/04 , C01P2004/30 , C01P2004/50 , C01P2004/64 , C01P2006/12 , Y10T428/24 , Y10T428/2998
摘要： A curable silicone is used to encapsulate porous, photoluminescing silica nanoparticles having three-dimensional, web-like structures. The encapsulation protects the silica nanoparticles, preserves their photoluminescent effect, and can be used as a coating. The composition is used to prepare articles of manufacture by casting it on a substrate such as glass or a silicon wafer and curing it. Special effects can be obtained by using a mask on the substrate prior to deposit of nanoparticles and curing the silicone matrix.
摘要翻译： 使用可固化的硅氧烷封装具有三维网状结构的多孔，光致发光的二氧化硅纳米颗粒。 封装保护二氧化硅纳米颗粒，保持其光致发光效果，并可用作涂层。 该组合物用于通过将其浇铸在诸如玻璃或硅晶片的基材上并固化来制备制品。 在沉积纳米颗粒并固化硅树脂基质之前，在基材上使用掩模可以获得特殊的效果。
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公开(公告)号：US5580655A
公开(公告)日：1996-12-03
申请号：US398268
申请日：1995-03-03
CPC分类号： C01B33/12 , Y10T428/2982
摘要： A web-like nanoparticle silica is produced by laser vaporization of silicon metal in a helium/oxygen atmosphere in a diffusion cloud chamber where it aggregates into novel web-like microstructures. The aggregates are porous and have a surface area greater than 300 m.sup.2 /g. Bright blue photoluminescence from the web-like nanoparticle silica is observed upon irradiation with ultraviolet light.
摘要翻译： 通过在扩散云室中的氦/氧气氛中的硅金属的激光蒸发来生产网状纳米颗粒二氧化硅，其中它聚集成新的网状微结构。 聚集体是多孔的并且具有大于300m 2 / g的表面积。 在紫外线照射下观察到来自网状纳米颗粒二氧化硅的明亮蓝色光致发光。
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公开(公告)号：US20150291741A1
公开(公告)日：2015-10-15
申请号：US14567100
申请日：2014-12-11
申请人： Ramani Narayan , Daniel Graiver , Elodie Hablot
发明人： Ramani Narayan , Daniel Graiver , Elodie Hablot
IPC分类号： C08H1/00 , C07K1/107 , C08J9/00 , C07K14/415
CPC分类号： C08H1/00 , C07K1/1077 , C08G18/5039 , C08G18/5045 , C08G71/04 , C08J2389/00 , C08L89/00
摘要： A process of producing multi-hydroxy polyols, the process comprising providing a biomass material and transamidating the biomass material with an amine selected from the group consisting essentially of a diamine and an alkanolamine, to provide low molecular weight derived amino-acids or derived oligomers of proteins. Thereafter, reacting the derived amino-acids or derived oligomers with a carbonate to provide hydroxyl terminated urethane oligomers.
摘要翻译： 一种生产多羟基多元醇的方法，该方法包括提供生物质材料并使选自基本上由二胺和链烷醇胺组成的组中的胺转酰胺化生物质材料，以提供低分子量衍生的氨基酸或衍生的低聚物 蛋白质。 此后，使衍生的氨基酸或衍生的低聚物与碳酸酯反应，得到羟基封端的氨基甲酸酯低聚物。
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公开(公告)号：US20080202020A1
公开(公告)日：2008-08-28
申请号：US12148049
申请日：2008-04-16
IPC分类号： C10L1/18
摘要： Fuel oxygenates comprised of fatty acid or fatty acid ester derivatives which have been reacted with ozone; a base; and a lower alkanol (1 to 8 carbon atoms) are described. The oxygenates comprise ester groups at a point of cleavage by the ozone which provide oxygen in the oxygenate.
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7.发明授权Method of rendering substrates water repellent using hyperbranched polymers containing silicon atoms 失效使用含有硅原子的超支化聚合物使底物防水的方法
公开(公告)号：US6103848A
公开(公告)日：2000-08-15
申请号：US334902
申请日：1999-06-17
IPC分类号： B27K3/15 , C08G77/54 , C08G83/00 , C09D183/14 , C09D201/00 , C08G77/06
CPC分类号： C09D201/005 , C08G77/54 , C08G83/005 , C08L97/02 , C09D183/14 , B27K3/15 , C08K5/3445 , C08L83/04
摘要： Substrates are rendered water repellent by applying to the substrate a hyperbranched polymer containing a silicon atom made by polymerizing a derivatized aminofunctional organosilicon monomer which is the reaction product of an amine functional silane monomer precursor or an amine functional polysiloxane monomer precursor and a derivative of carbonic acid or a cyclic lactone.
摘要翻译： 通过向基材施加含有通过聚合作为胺官能的硅烷单体前体或胺官能的聚硅氧烷单体前体与碳酸的衍生物的反应产物的衍生的氨基官能的有机硅单体而制备的硅原子的超支化聚合物， 或环状内酯。
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公开(公告)号：US5789516A
公开(公告)日：1998-08-04
申请号：US826716
申请日：1997-04-07
IPC分类号： C08L83/10 , C08F4/40 , C08F4/44 , C08F293/00 , C08G77/442 , C08G77/06
CPC分类号： C08G77/442 , C08F4/40
摘要： A method of manufacturing block copolymers containing a polyorganosiloxane segment, by dual polymerization involving (i) polycondensation of a silicone block followed by (ii) the free radical polymerization of a monomer that can be polymerized by free radical polymerization, such as a vinyl containing organic monomer. Initiation of free radical polymerization in step (ii) is carried out with a carbonyl functional group attached to the silicone polymer block. The carbonyl functional silicone polymer, preferably an aldehyde functional silicone polymer, is included as one component of a copper-based Redox initiating system. The method ensures no free homopolymerization, complete reactivity, and various polymer architectures are possible, including for example, polymeric structures such as AB, ABA, (AB).sub.n, brush, and radiant types. The method is fast, effective, convenient, and easier to control than typical ionic polymerization techniques. The silicone-organic block copolymers obtained by the process have utility as polymeric surfactants or as solubility modifiers.
摘要翻译： 通过双重聚合制造含有聚有机硅氧烷链段的嵌段共聚物的方法，包括（i）硅氧烷嵌段的缩聚，随后（ii）可通过自由基聚合反应的单体的自由基聚合，例如含乙烯基的有机物 单体。 在步骤（ii）中开始自由基聚合是用与硅氧烷聚合物嵌段连接的羰基官能团进行的。 羰基官能硅氧烷聚合物，优选醛官能的硅氧烷聚合物，作为铜基氧化还原引发体系的一个组分被包括在内。 该方法确保没有游离的均聚，完全的反应性，并且各种聚合物结构是可能的，包括例如聚合物结构如AB，ABA，（AB）n，刷和辐射型。 该方法比典型的离子聚合技术快速，有效，方便，易于控制。 通过该方法获得的硅氧烷 - 有机嵌段共聚物可用作聚合物表面活性剂或溶解度调节剂。
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公开(公告)号：US5708115A
公开(公告)日：1998-01-13
申请号：US798990
申请日：1997-02-11
CPC分类号： C08G77/38 , C07F7/12 , C07F7/1836 , C08F4/42
摘要： A method in which radical polymerization of a vinyl monomer is initiated by an ozonide group attached to a silane or a siloxane polymer. The method is particularly useful for preparing organic polymers having a silicone chain end, or for preparing wide ranges of silicone/organic polymers and copolymers with varied architecture, i.e., ABA block copolymers, comb polymers, star polymers, and hyper-branched polymers. In one embodiment, the method is carried out by simply heating a vinyl monomer in the presence of a silane containing ozonide functionality. The ozonide silane is obtained by exposing silanes or siloxanes having an alkyl group containing a double bond to ozone. Surprisingly, an ozonide attached to an organosilicon compound was found to be stable, and capable of initiating vinyl polymerization upon heating to moderate temperatures, i.e., about 70.degree. C.
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10.发明授权Method for preparing tubing and hollow fibers from non-crosslinked polyvinyl alcohol hydrogels 失效从非交联聚乙烯醇水凝胶制备管材和中空纤维的方法
公开(公告)号：US5225120A
公开(公告)日：1993-07-06
申请号：US851599
申请日：1992-03-16
申请人： Daniel Graiver , Arnold W. Lomas
发明人： Daniel Graiver , Arnold W. Lomas
摘要： This invention relates to hollow elongate articles such as tubing and fibers formed from non-crosslinked polyvinyl alcohol. The articles are prepared by extruding a solution of polyvinyl alcohol in the shape of the desired article into a coagulating bath concurrently with a stream of a non-solvent for the polymer. The stream occupies the area corresponding to the interior cavity of the article and prevents collapse of the cavity until the article has solidified in the coagulation bath.
摘要翻译： 本发明涉及中空细长制品，例如由非交联聚乙烯醇形成的管材和纤维。 通过将所需制品形状的聚乙烯醇溶液与用于聚合物的非溶剂流同时挤出到凝固浴中来制备制品。 流体占据与制品的内部空腔相对应的区域，并防止腔体塌陷，直到制品在凝固浴中凝固。
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