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    COPOLYMER, RUBBER COMPOSITION, CROSS-LINKED RUBBER, CROSS-LINKED FOAM, AND USES THEREOF
    1.
    发明申请
    COPOLYMER, RUBBER COMPOSITION, CROSS-LINKED RUBBER, CROSS-LINKED FOAM, AND USES THEREOF 有权
    共聚物，橡胶组合物，交联橡胶，交联泡沫及其用途

    公开(公告)号：US20110233448A1

    公开(公告)日：2011-09-29

    申请号：US13130746

    申请日：2009-11-26

    申请人： Hiroki Ebata ,  Akinori Takehara ,  Mitsunao Arino ,  Masao Kunizane ,  Yoshiharu Kikuchi ,  Takayuki Kajihara

    发明人： Hiroki Ebata ,  Akinori Takehara ,  Mitsunao Arino ,  Masao Kunizane ,  Yoshiharu Kikuchi ,  Takayuki Kajihara

    IPC分类号： C08F4/6592 ,  C08L9/00 ,  C08J9/00 ,  E04B1/74

    CPC分类号： C08L23/16 ,  C08F4/65908 ,  C08F4/6592 ,  C08F210/18 ,  C08F232/08 ,  C08F2420/02 ,  C08J9/04 ,  C08J2201/026 ,  C08J2323/16 ,  C08L2203/14 ,  C08L2312/00 ,  C08L2314/06 ,  C08L2666/08 ,  C08F210/06 ,  C08F236/20

    摘要： The present invention provides a rubber composition having adequate foamability, uses thereof, a copolymer contained in the rubber composition, a rubber composition capable of providing a cross-linked foam, which has a low specific gravity and an excellent shape-retaining property even when the usage of a nonconjugated polyene is reduced, and a cross-linked rubber and a cross-linked foam, which are produced from the rubber composition. A copolymer (A) according to the present invention is a copolymer including structural units derived from ethylene [A], an α-olefin [B], a nonconjugated polyene [C-1], in which one carbon-carbon double bond (C═C) polymerizable with a metallocene catalyst is present in one molecule, and a nonconjugated polyene [C-2], in which two bonds of C═C polymerizable with the metallocene catalyst are present in one molecule, and being synthesized with the metallocene catalyst, wherein (1) the units derived from the component [B] constitute 10 to 50 percent by mole, (2) the total of the units derived from the component [C-1] and the units derived from the component [C-2] is 1.0 to 6.0 percent by mole, (3) the molar ratio of the units derived from the component [C-1] to the units derived from the component [C-2] is 75/25 to 99.5/0.5, (4) [ML (1+4) 100° C.] is 10 to 200, and (5) 50>activation energy of fluidization (kJ/mol)>35 is satisfied.

    摘要翻译： 本发明提供一种橡胶组合物，其具有足够的发泡性，其用途，包含在橡胶组合物中的共聚物，能够提供交联泡沫的橡胶组合物，即使在 降低了非共轭多烯的使用，以及由橡胶组合物制备的交联橡胶和交联泡沫。 根据本发明的共聚物（A）是包含衍生自乙烯[A]，α-烯烃[B]，非共轭多烯[C-1]的结构单元的共聚物，其中一个碳 - 碳双键 可用金属茂催化剂聚合的≡C）存在于一个分子中，并且在一分子中存在可与金属茂催化剂聚合的C = C的两个键的非共轭多烯[C-2]，并与茂金属催化剂合成 其中（1）衍生自组分[B]的单元构成10至50摩尔％，（2）衍生自组分[C-1]的单元和衍生自组分[C-2 ]为1.0〜6.0摩尔％，（3）[C-1]成分的单元与来自成分[C-2]的单元的摩尔比为75/25〜99.5 / 0.5，（4） ）[ML（1 + 4）100℃]为10〜200，（5）50>流化活化能（kJ / mol）> 35。

    Copolymer, rubber composition, cross-linked rubber, cross-linked foam, and uses thereof
    2.
    发明授权
    Copolymer, rubber composition, cross-linked rubber, cross-linked foam, and uses thereof 有权
    共聚物，橡胶组合物，交联橡胶，交联泡沫及其用途

    公开(公告)号：US09193856B2

    公开(公告)日：2015-11-24

    申请号：US13130746

    申请日：2009-11-26

    申请人： Hiroki Ebata ,  Akinori Takehara ,  Mitsunao Arino ,  Masao Kunizane ,  Yoshiharu Kikuchi ,  Takayuki Kajihara

    发明人： Hiroki Ebata ,  Akinori Takehara ,  Mitsunao Arino ,  Masao Kunizane ,  Yoshiharu Kikuchi ,  Takayuki Kajihara

    IPC分类号： C08F210/18 ,  C08F4/6592 ,  C08L23/16 ,  C08F232/08

    CPC分类号： C08L23/16 ,  C08F4/65908 ,  C08F4/6592 ,  C08F210/18 ,  C08F232/08 ,  C08F2420/02 ,  C08J9/04 ,  C08J2201/026 ,  C08J2323/16 ,  C08L2203/14 ,  C08L2312/00 ,  C08L2314/06 ,  C08L2666/08 ,  C08F210/06 ,  C08F236/20

    摘要： The present invention provides a rubber composition having adequate foamability, uses thereof, a copolymer contained in the rubber composition, a rubber composition capable of providing a cross-linked foam, which has a low specific gravity and an excellent shape-retaining property even when the usage of a nonconjugated polyene is reduced, and a cross-linked rubber and a cross-linked foam, which are produced from the rubber composition. A copolymer (A) according to the present invention is a copolymer including structural units derived from ethylene [A], an α-olefin [B], a nonconjugated polyene [C-1], in which one carbon-carbon double bond (C═C) polymerizable with a metallocene catalyst is present in one molecule, and a nonconjugated polyene [C-2], in which two bonds of C═C polymerizable with the metallocene catalyst are present in one molecule, and being synthesized with the metallocene catalyst, wherein (1) the units derived from the component [B] constitute 10 to 50 percent by mole, (2) the total of the units derived from the component [C-1] and the units derived from the component [C-2] is 1.0 to 6.0 percent by mole, (3) the molar ratio of the units derived from the component [C-1] to the units derived from the component [C-2] is 75/25 to 99.5/0.5, (4) [ML (1+4) 100° C.] is 10 to 200, and (5) 50>activation energy of fluidization (kJ/mol)>35 is satisfied.

    摘要翻译： 本发明提供一种橡胶组合物，其具有足够的发泡性，其用途，包含在橡胶组合物中的共聚物，能够提供交联泡沫的橡胶组合物，即使在 降低了非共轭多烯的使用，以及由橡胶组合物制备的交联橡胶和交联泡沫。 根据本发明的共聚物（A）是包含衍生自乙烯[A]，α-烯烃[B]，非共轭多烯[C-1]的结构单元的共聚物，其中一个碳 - 碳双键 可用金属茂催化剂聚合的≡C）存在于一个分子中，并且在一分子中存在可与金属茂催化剂聚合的C = C的两个键的非共轭多烯[C-2]，并与茂金属催化剂合成 其中（1）衍生自组分[B]的单元构成10至50摩尔％，（2）衍生自组分[C-1]的单元和衍生自组分[C-2 ]为1.0〜6.0摩尔％，（3）[C-1]成分的单元与来自成分[C-2]的单元的摩尔比为75/25〜99.5 / 0.5，（4） ）[ML（1 + 4）100℃]为10〜200，（5）50>流化活化能（kJ / mol）> 35。

    Crosslinkable rubber compositions and uses thereof
    3.
    发明授权
    Crosslinkable rubber compositions and uses thereof 有权
    可交联橡胶组合物及其用途

    公开(公告)号：US06743862B2

    公开(公告)日：2004-06-01

    申请号：US10049888

    申请日：2002-02-19

    申请人： Takashi Hakuta ,  Mitsunao Arino ,  Yoshiharu Kikuchi ,  Masaaki Kawasaki

    发明人： Takashi Hakuta ,  Mitsunao Arino ,  Yoshiharu Kikuchi ,  Masaaki Kawasaki

    IPC分类号： C08F800

    CPC分类号： C08L23/16 ,  C08L83/04 ,  C08L83/00

    摘要： The crosslinkable rubber composition is crosslinkable at room temperature, has a gelation time at room temperature of 30 days or less, and can prepare a crosslinked rubber sheet by crosslinking the composition at room temperature, wherein the crosslinked rubber sheet has a tensile elongation of 20% or more, and is free of cracks after treatment at 40° C. in a 50 pphm ozone concentration for 96 hr. Specifically, it comprises an ethylene/&agr;-olefin/non-conjugated polyene random copolymer rubber comprising a norbornene compound having a specific vinyl end group, an SiH group-containing compound, which has at least two SiH groups in one molecule, and optionally a platinum catalyst, a reaction inhibitor and/or a silane-coupling agent. The sealing, potting and coating materials and adhesives of the present invention comprise the above rubber composition.

    摘要翻译： 可交联橡胶组合物在室温下可交联，在室温下凝胶化时间为30天以下，并且可以通过在室温下交联组合物来制备交联橡胶片，其中交联橡胶片的拉伸伸长率为20％ 以上，并且在50pphm臭氧浓度下在40℃下处理96小时后没有裂纹。 具体地说，它包括一种乙烯/α-烯烃/非共轭多烯无规共聚物橡胶，其包含具有特定乙烯基端基的降冰片烯化合物，含有SiH基的化合物，其在一个分子中具有至少两个SiH基团， 铂催化剂，反应抑制剂和/或硅烷偶联剂。 本发明的密封，灌封和涂覆材料和粘合剂包括上述橡胶组合物。

    Crosslinkable rubber compositions and use thereof
    5.
    发明授权
    Crosslinkable rubber compositions and use thereof 有权
    可交联橡胶组合物及其用途

    公开(公告)号：US06864315B1

    公开(公告)日：2005-03-08

    申请号：US09673608

    申请日：2000-03-14

    申请人： Takashi Hakuta ,  Masaaki Kawasaki ,  Yoshiharu Kikuchi ,  Hidenari Nakahama ,  Taku Koda ,  Hiroshi Kameda ,  Shuichi Nonaka ,  Mikio Hosoya ,  Yuji Ishii ,  Mitsunao Arino ,  Tsutomu Nakamura ,  Satao Hirabayashi ,  Takeo Yoshida

    发明人： Takashi Hakuta ,  Masaaki Kawasaki ,  Yoshiharu Kikuchi ,  Hidenari Nakahama ,  Taku Koda ,  Hiroshi Kameda ,  Shuichi Nonaka ,  Mikio Hosoya ,  Yuji Ishii ,  Mitsunao Arino ,  Tsutomu Nakamura ,  Satao Hirabayashi ,  Takeo Yoshida

    IPC分类号： C08K5/00 ,  C08L23/16 ,  C08L83/04 ,  C08L47/00

    CPC分类号： C08K5/0025 ,  C08L23/16 ,  C08L83/04 ,  C08L2312/08 ,  C08L2314/02 ,  C08L83/00

    摘要： The crosslinkable rubber composition of the invention is crosslinkable by hot air, and a hot-air crosslinked rubber sheet thereof has no scratch on the surface in a hardness test using a pencil of HB and has a compression set of not more than 70% after a heat treatment at 150° C. for 22 hours. The rubber composition comprises an ethylene/α-olefin/non-conjugated polyene random copolymer rubber comprising a specific vinyl end group-containing norbornene compound, a SiH group-containing compound having at least two SiH groups in one molecule, and if necessary, an addition reaction catalyst comprising a platinum group element and a reaction inhibitor. The automobile weatherstrip, hose, rubber vibration insulator, belt, sealing material, expanded product, covered electric wire, electric wire joint, electric insulating part and household rubber product according to the invention comprise the above-mentioned rubber composition. The rubber composition has a high crosslinking rate and excellent productivity to produce crosslinked rubber molded products, is capable of undergoing hot-air crosslinking such as HAV or UHF and is capable of providing crosslinked rubber molded products having excellent compression set resistance, strength properties, heat resistance, weathering resistance and abrasion resistance.

    摘要翻译： 本发明的交联性橡胶组合物可以通过热风进行交联，在使用HB的铅笔的硬度试验中，热风交联橡胶片在表面没有刮痕，并且在a后的压缩永久变形为70％以上 在150℃下热处理22小时。 该橡胶组合物包含一个乙烯/α-烯烃/非共轭多烯无规共聚物橡胶，其包含特定的含乙烯基端基的降冰片烯化合物，在一个分子中具有至少两个SiH基团的含SiH基化合物，如果需要， 包含铂族元素和反应抑制剂的加成反应催化剂。 根据本发明的汽车密封条，软管，橡胶振动绝缘子，带，密封材料，膨胀产品，包覆电线，电线接头，电绝缘部件和家用橡胶制品包括上述橡胶组合物。 橡胶组合物具有高交联率和优异的生产交联橡胶成型体的生产率，能够进行热风交联如HAV或UHF，并且能够提供具有优异的耐压缩变形性，强度性能，热性能的交联橡胶模制产品 耐电阻，耐候性和耐磨性。

    Pellet comprising ethylene-alpha-olefin-non-conjugated polyene copolymer, method for producing thermoplastic elastomer, and method for producing pellet comprising ethylene-alpha-olefin-non-conjugated polyene copolymer
    7.
    发明申请
    Pellet comprising ethylene-alpha-olefin-non-conjugated polyene copolymer, method for producing thermoplastic elastomer, and method for producing pellet comprising ethylene-alpha-olefin-non-conjugated polyene copolymer 审中-公开
    包含乙烯-α-烯烃 - 非共轭多烯共聚物的颗粒，用于生产热塑性弹性体的方法，以及包含乙烯-α-烯烃 - 非共轭多烯共聚物

    公开(公告)号：US20060142437A1

    公开(公告)日：2006-06-29

    申请号：US10543593

    申请日：2004-03-12

    申请人： Takashi Hakuta ,  Yoshiharu Kikuchi ,  Masaaki Kawasaki

    发明人： Takashi Hakuta ,  Yoshiharu Kikuchi ,  Masaaki Kawasaki

    IPC分类号： C08K5/00 ,  C09B67/00

    CPC分类号： C08J3/24 ,  C08J2323/16 ,  C08K3/04 ,  C08K3/06 ,  C08K3/26 ,  C08K5/05 ,  C08K7/26 ,  C08L23/10 ,  C08L23/16 ,  C08L91/00 ,  C08L2312/00 ,  C08L2666/06

    摘要： A pellet comprising 100 parts by weight of an ethylene/α-olefin/non-conjugated polyene copolymer (A) containing a constitutional unit derived from non-conjugated polyene represented by a specific Formula, 1 to 150 parts by weight of a plasticizer (B) relative to 100 parts by weight of the above (A), and 0 to 30 parts by weight of a thermoplastic resin (C) relative to 100 parts by weight of the above (A), is obtained, and a vulcanized rubber or a thermoplastic elastomer which does not cause blocking and has excellent crosslinking reactivity and thus excellent properties can be prepared therefrom. According to a process for preparation of a thermoplastic elastomer using the above-mentioned pellet, a thermoplastic elastomer having excellent compression set or dispersibility can be economically and efficiently prepared. In particular, since it can be prepared continuously using a twin screw extruder, the process is excellent from an industrial viewpoint. According to a process for preparation of a pellet of an ethylene copolymer rubber composition according to the invention, it is possible to obtain a copolymer pellet which has a low degree of crystallinity, does not cause blocking, has excellent crosslinking reactivity and has carbon-carbon double bonds of excellent crosslinking reactivity.

    摘要翻译： 包含100重量份含有由特定式表示的非共轭多烯衍生的结构单元的乙烯/α-烯烃/非共轭多烯共聚物（A），1〜150重量份增塑剂（B ）相对于上述（A）的100重量份，相对于上述（A）相对于100重量份为0〜30重量份的热塑性树脂（C），硫化橡胶或 可以制备不引起阻塞并且具有优异的交联反应性和因此优异性能的热塑性弹性体。 根据使用上述颗粒制备热塑性弹性体的方法，可以经济有效地制备具有优异压缩永久变形或分散性的热塑性弹性体。 特别地，由于可以使用双螺杆挤出机连续制备，从工业的观点来看，该方法是优异的。 根据本发明的乙烯共聚物橡胶组合物的颗粒的制备方法，可以获得结晶度低，不引起粘连，具有优异的交联反应性并具有碳 - 碳的共聚物颗粒 双键具有优异的交联反应性。

    Raw rubber lapping film
    8.
    发明授权
    Raw rubber lapping film 有权
    生橡胶研磨膜

    公开(公告)号：US06391413B1

    公开(公告)日：2002-05-21

    申请号：US09514162

    申请日：2000-02-28

    申请人： Keiji Okada ,  Yoshiharu Kikuchi ,  Takashi Hakuta

    发明人： Keiji Okada ,  Yoshiharu Kikuchi ,  Takashi Hakuta

    IPC分类号： B32B2732

    CPC分类号： C08J3/005 ,  C08J5/18 ,  C08J2323/08 ,  C08J2323/16 ,  C08K3/36 ,  C08K5/20 ,  C08L23/0815 ,  C08L23/16 ,  C08L2203/16 ,  Y10T428/1352 ,  Y10T428/1386 ,  Y10T428/31913

    摘要： The present invention provides a raw rubber lapping film formed of an ethylene·&agr;-olefin random copolymer comprising ethylene unit and an &agr;-olefin unit having 4 to 20 carbon atoms and a raw rubber bale lapped with this film. Since the film is superior in strength and release properties and has good dispersibility in ethylene·&agr;-olefin copolymer rubber, the operation of lapping raw rubber with a film, the operation of stripping a film from a lapped raw rubber bale and the operation of separating each of a plurality of raw rubber bales are carried out easily and yet there is no adverse effect on the subsequent rubber processing step without stripping the film by heating at a temperature higher than the melting point of the film at the time of kneading.

    摘要翻译： 本发明提供一种由包含乙烯单元和碳原子数4〜20的α-烯烃单元的乙烯-α-烯烃无规共聚物形成的生胶橡胶研磨膜，并且与该薄膜一起研磨生橡胶包。 由于膜的强度和剥离性能优异，并且在乙烯-α-烯烃共聚橡胶中具有良好的分散性，使用膜研磨生橡胶的操作，从研磨的生橡胶包剥离膜的操作和分离 多个生橡胶捆中的每一个都容易进行，而对随后的橡胶加工步骤没有不利影响，而不会在捏合时在高于熔点的温度下加热而剥离膜。