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    Urethane acrylates and their use in coating compositions
    1.
    发明授权
    Urethane acrylates and their use in coating compositions 有权
    聚氨酯丙烯酸酯及其在涂料组合物中的用途

    公开(公告)号：US06191181B1

    公开(公告)日：2001-02-20

    申请号：US09433854

    申请日：1999-11-04

    申请人： Jan Weikard ,  Wolfgang Fischer ,  Frank Richter ,  Christian Zwiener

    发明人： Jan Weikard ,  Wolfgang Fischer ,  Frank Richter ,  Christian Zwiener

    IPC分类号： C08F246

    CPC分类号： C08G18/792 ,  C08G18/672 ,  C09D175/16

    摘要： The present invention relates to urethane acrylates, which may be cured with high-energy radiation, in which the urethane acrylates are the reaction product of a) a polyisocyanate component containing 20 to 100 mole %, based on the moles of the polyisocyanate component a), of iminooxadiazine dione group-containing polyisocyanate trimers corresponding to formula A  wherein R1, R2and R3 are the same or different and represent linear or branched, C4-C20 (cyclo)alkyl groups and X is the same or different and represents isocyanate groups or isocyanate group-containing radicals that also contain iminooxadiazine dione, isocyanurate, uretdione, urethane, allophanate, biuret or oxadiazine trione groups, wherein R1, R2 and R3 are attached to a nitrogen atom, with b) an alcohol component containing at least one monobasic, hydroxy-functional, linear or branched C1-C12 alkyl ester of (meth)acrylic acid. The present invention further relates to the use of the urethane acrylates as binder components for coating compositions that are curable with high-energy radiation.

    摘要翻译： 本发明涉及聚氨酯丙烯酸酯，其可以用高能量辐射固化，其中聚氨酯丙烯酸酯是基于多异氰酸酯组分a）的摩尔数为20-100摩尔％的多异氰酸酯组分的反应产物， 对应于式A的亚氨基恶二嗪二酮基多异氰酸酯三聚体，其中R 1，R 2和R 3相同或不同，表示直链或支链的C 4 -C 20（环）烷基，X相同或不同，表示异氰酸酯基或异氰酸酯基 还含有亚氨基恶二酮二酮，异氰脲酸酯，脲二酮，氨基甲酸酯，脲基甲酸酯，缩二脲或恶二嗪三酮基团的基团，其中R1，R2和R3连接到氮原子上，b）含有至少一个一元羟基官能 或（甲基）丙烯酸的支链C1-C12烷基酯。本发明还涉及聚氨酯丙烯酸酯作为共聚物的粘合剂成分的用途 可以用高能量辐射固化的组合物。

    Pulverent binders for powder coating compositions containing oligo- and polyurethanes having (meth)acryloyl groups
    2.
    发明授权
    Pulverent binders for powder coating compositions containing oligo- and polyurethanes having (meth)acryloyl groups 失效
    含有（甲基）丙烯酰基的低聚物和聚氨酯的粉末涂料组合物的流平粘合剂

    公开(公告)号：US06555597B1

    公开(公告)日：2003-04-29

    申请号：US09639687

    申请日：2000-08-16

    申请人： Jan Weikard ,  Christian Zwiener ,  Wolfgang Fischer ,  Peter Thometzek

    发明人： Jan Weikard ,  Christian Zwiener ,  Wolfgang Fischer ,  Peter Thometzek

    IPC分类号： C08F246

    CPC分类号： C08G18/672 ,  C08G18/3206 ,  C08G18/724 ,  C08G2150/20

    摘要： The present invention relates to pulverent binders for powder coating compositions which contain oligo- and polyurethanes having (meth)acryloyl groups, are curable by means of high energy radiation and have an organic solvent content of less than 1 wt. %. The present invention also relates to a process for preparing these binders in the absence of an organic solvent and to their use in powder coating compositions for coating wood, metal, plastic, mineral and/or preprimed substrates.

    摘要翻译： 本发明涉及用于粉末涂料组合物的浆料粘合剂，其含有具有（甲基）丙烯酰基的低聚物和聚氨酯，可通过高能量辐射固化并且有机溶剂含量小于1wt。 ％。 本发明还涉及在不存在有机溶剂的情况下制备这些粘合剂的方法，以及它们在用于涂覆木材，金属，塑料，矿物和/或预制基材的粉末涂料组合物中的用途。

    Process for preparing urethanes containing (meth)-acryloyl groups as binders for powder coatings
    3.
    发明授权
    Process for preparing urethanes containing (meth)-acryloyl groups as binders for powder coatings 失效
    制备含有（甲基）丙烯酰基的聚氨酯作为粉末涂料的粘合剂的方法

    公开(公告)号：US06569944B2

    公开(公告)日：2003-05-27

    申请号：US09810989

    申请日：2001-03-16

    申请人： Jan Weikard ,  Christian Zwiener ,  Wolfgang Fischer ,  Peter Thometzek

    发明人： Jan Weikard ,  Christian Zwiener ,  Wolfgang Fischer ,  Peter Thometzek

    IPC分类号： C08L7514

    CPC分类号： C08G18/8175 ,  C08G18/672 ,  C08G2150/20 ,  Y10T428/31551 ,  Y10T428/31591 ,  Y10T428/31605

    摘要： The present invention relates to a process for preparing urethanes containing (meth)acryloyl groups that are suitable as binders for powder coatings by reacting a polyisocyanate component with a hydroxyl group-containing component that contains at least one compound additionally containing (meth)acryloyl groups in a melt of compounds containing (meth)acryloyl groups, which are crystalline in the solid state and have a melting point of 30 to 100° C. and a dynamic viscosity at 111° C. of less than 10 Pa·s, at elevated temperature until the NCO content has dropped below 0.5 wt. %. The present invention also relates to the use of these urethanes as binders for powder coating compositions for coating substrates made of wood, metal, plastics or mineral substances, which may have been primed.

    摘要翻译： 本发明涉及一种制备含有（甲基）丙烯酰基的聚氨酯的方法，所述聚氨酯通过使多异氰酸酯组分与含有至少一种另外含有（甲基）丙烯酰基的化合物的含羟基的组分反应，适合作为粉末涂料的粘合剂 含有（甲基）丙烯酰基的化合物的熔体，其在固态下为结晶，熔点为30-100℃，在111℃下的动态粘度小于10Pa.s，在高温下 直到NCO含量低于0.5wt。 ％。 本发明还涉及这些氨基甲酸酯作为用于涂覆由木材，金属，塑料或矿物质制成的基材的粉末涂料组合物作为粘合剂的用途，所述基材可能已被引发。

    Aminoacrylates and a process for their preparation
    4.
    发明授权
    Aminoacrylates and a process for their preparation 失效
    氨基丙烯酸酯及其制备方法

    公开(公告)号：US5482649A

    公开(公告)日：1996-01-09

    申请号：US95886

    申请日：1993-07-22

    申请人： Jurgen Meixner ,  Wolfgang Fischer ,  Christian Zwiener

    发明人： Jurgen Meixner ,  Wolfgang Fischer ,  Christian Zwiener

    IPC分类号： C08F20/36 ,  C07C69/54 ,  C07C217/50 ,  C07C219/08 ,  C07C227/06 ,  C07C229/12 ,  C07C229/14 ,  C07C229/16 ,  C08F20/34 ,  C08F220/36 ,  C08F299/02 ,  C08G65/332 ,  C09D4/00 ,  C09D4/02 ,  C09J4/02 ,  C09K3/00

    CPC分类号： C08G65/3322 ,  C07C227/06 ,  C07C229/12 ,  C07C229/14 ,  C07C69/54 ,  C08F299/024 ,  C09D4/00

    摘要： The present invention relates to aminoacrylates which have a viscosity of 200 to 3000 mPa.s at 23.degree. C. and 100% solids, a content of olefinic double bonds (calculated as C=C, molecular weight=24) of 8 to 20% by weight and a nitrogen content of 0.4 to 2.0% by weight, and which are prepared by an addition reaction by reacting at a molar ratio of primary amino groups from component a) to olefinic double bonds from component b) of 0.05:1 to 0.25:1a) mono- or diamines having a molecular weight of 31 to 300 and having aliphatically bound amino groups withb) acrylic esters of polyhydric alcohols which have been prepared at a COOH/OH equivalent ratio of 0.8:1 to 1:1 fromb1) acrylic acid andb2) ether-alcohols which have 3 or 4 hydroxyl groups and a molecular weight of 136 to 1000, possess at least one ethylene oxide unit --CH.sub.2 --CH.sub.2 --O-- as part of the ether structure and do not contain propylene oxide units --CH.sub.2 --CH(CH.sub.3)--O--.The present invention also relates to a process for the preparation these aminoacrylates.

    摘要翻译： 本发明涉及在23℃和100％固体粘度为200-3000mPa.s，烯属双键（C = C，分子量= 24计算）的含量为8至20％的氨基丙烯酸酯， 并且氮含量为0.4〜2.0重量％，并且其通过加成反应制备，其通过使组分a）中的伯氨基与组分b）的烯属双键的摩尔比为0.05:1至0.25 ：1a）分子量为31〜300，具有脂族结合氨基的单胺或二胺，b）以0.8:1〜1:1的COOH / OH当量比制备的多元醇丙烯酸酯， b1）丙烯酸和b2）具有3或4个羟基并且分子量为136至1000的醚醇具有至少一个环氧乙烷单元-CH 2 -CH 2 -O-作为醚结构的一部分，并且不含 环氧丙烷单元-CH2-CH（CH3）-O-。 本发明还涉及制备这些氨基丙烯酸酯的方法。

    Process for the production of polyurethane coatings
    9.
    发明授权
    Process for the production of polyurethane coatings 失效
    聚氨酯涂料生产工艺

    公开(公告)号：US5236741A

    公开(公告)日：1993-08-17

    申请号：US877682

    申请日：1992-05-01

    申请人： Christian Zwiener ,  Josef Pedain ,  Lothar Kahl ,  Klaus Nachtkamp

    发明人： Christian Zwiener ,  Josef Pedain ,  Lothar Kahl ,  Klaus Nachtkamp

    IPC分类号： C08G18/38 ,  C08G18/62 ,  C08G18/78 ,  C08G18/79

    CPC分类号： C08G18/3821 ,  C08G18/6229 ,  C08G18/7831 ,  C08G18/792

    摘要： The present invention relates to a process for the preparation of a polyurethane coating by coating a substrate with a coating composition containinga) a polyisocyanate component andb) an isocyanate-reactive component containing at least one compound corresponding to the formula ##STR1## wherein X represents an organic group which has a valency of n and is inert towards isocyanate groups at a temperature of 100.degree. C. or less,R.sup.1 and R.sup.2 may be identical or different and represent organic groups which are inert towards isocyanate groups at a temperature of 100.degree. C. or less,R.sup.3 and R.sup.4 may be identical or different and represent hydrogen or organic groups which are inert towards isocyanate groups at a temperature of 100.degree. C. or less andn represents an integer with a value of at least 2, and curing the coating composition at a temperature of 100.degree. C. or less.

    摘要翻译： 本发明涉及通过用包含a）多异氰酸酯组分的涂料组合物涂布基材来制备聚氨酯涂料的方法，和b）含有至少一种对应于下式的化合物的异氰酸酯反应性组分（I ）其中X表示在100℃或更低的温度下具有n价并且对异氰酸酯基团呈惰性的有机基团，R 1和R 2可以相同或不同，表示在一个或多个基团上对于异氰酸酯基团是惰性的有机基团 温度为100℃以下时，R 3和R 4可以相同或不同，表示在100℃以下的温度下对异氰酸酯基具有惰性的氢或有机基团，n表示至少为 并且在100℃或更低的温度下固化涂料组合物。

    Process for the production of polyurethane coatings
    10.
    发明授权
    Process for the production of polyurethane coatings 失效
    聚氨酯涂料生产工艺

    公开(公告)号：US5126170A

    公开(公告)日：1992-06-30

    申请号：US540536

    申请日：1990-06-19

    申请人： Christian Zwiener ,  Josef Pedain ,  Lothar Kahl ,  Klaus Nachtkamp

    发明人： Christian Zwiener ,  Josef Pedain ,  Lothar Kahl ,  Klaus Nachtkamp

    IPC分类号： B05D7/24 ,  C08G18/30 ,  C08G18/34 ,  C08G18/38 ,  C08G18/62 ,  C08G18/78 ,  C08G18/79 ,  C09D175/00 ,  C09D175/04

    CPC分类号： C08G18/6229 ,  C08G18/3821 ,  C08G18/7831 ,  C08G18/792

    摘要： The present invention relates to a process for the preparation of a polyurethane coating by coating a substrate with a coating composition containinga) a polyisocyanate component andb) an isocyanate-reactive component containing at least one compound corresponding to the formula ##STR1## wherein X represents an organic group which has a valency of n and is inert towards isocyanate groups at a temperature of 100.degree. C. or less,R.sup.1 and R.sup.2 may be identical or different and represent organic groups which are inert towards isocyanate groups at a temperature of 100.degree. C. or less,R.sup.3 and R.sup.4 may be identical or different and represent hydrogen or organic groups which are inert towards isocyanate groups at a temperature of 100.degree. C. or less andn represents an integer with a value of at least 2,and curing the coating composition at a temperature of 100.degree. C. or less.

    摘要翻译： 本发明涉及通过用包含a）多异氰酸酯组分的涂料组合物涂布基材来制备聚氨酯涂料的方法，和b）含有至少一种对应于下式的化合物的异氰酸酯反应性组分（I ）其中X表示在100℃或更低的温度下具有n价并且对异氰酸酯基团呈惰性的有机基团，R 1和R 2可以相同或不同，表示在一个或多个基团上对于异氰酸酯基团是惰性的有机基团 温度为100℃以下时，R 3和R 4可以相同或不同，表示在100℃以下的温度下对异氰酸酯基具有惰性的氢或有机基团，n表示至少为 并且在100℃或更低的温度下固化涂料组合物。