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    Porous material composed of layered silica and metal oxide and a process for manufacturing the same
    1.
    发明授权
    Porous material composed of layered silica and metal oxide and a process for manufacturing the same 失效
    由层状二氧化硅和金属氧化物构成的多孔材料及其制造方法

    公开(公告)号：US5508081A

    公开(公告)日：1996-04-16

    申请号：US192933

    申请日：1994-02-07

    申请人： Shinji Inagaki ,  Yoshiaki Fukushima ,  Akane Okata ,  Chuzo Kato ,  Kazuyuki Kuroda

    发明人： Shinji Inagaki ,  Yoshiaki Fukushima ,  Akane Okata ,  Chuzo Kato ,  Kazuyuki Kuroda

    IPC分类号： C01B33/12 ,  B01J20/10 ,  B01J21/08 ,  B01J23/04 ,  B01J29/00 ,  B01J29/04 ,  B01J35/04 ,  C01B33/20 ,  C01B33/32 ,  C01B33/44 ,  B32B3/12

    CPC分类号： B01J20/10 ,  B01J21/08 ,  B01J23/04 ,  B01J29/049 ,  B01J35/04 ,  Y10T428/24149 ,  Y10T428/249969 ,  Y10T428/24997

    摘要： A porous material composed of many SiO.sub.4 tetrahedra sheets having interlayer bridges of SiO.sub.2. It has pores having a diameter of 10 .ANG. or above, and possesses the properties of a solid acid formed by the isomorphous substitution of metal atoms for Si of SiO.sub.4 frameworks. It is made by a process including introducing an organic substance into interlayer space of crystals of layered silicates to expand the spacing between crystal layers, as well as forming bridges of SiO.sub.2 therebetween, bringing the intercalated compounds into contact with a metal salt to link metal atoms to the SiO.sub.4 frameworks, and firing the products. The material can withstand a temperature of 800.degree. C., has a pore diameter larger than that of zeolites, etc., and is useful in making an adsorbent or catalyst for molecules having a high molecular weight, such as a catalyst for the catalytic cracking of petroleum.

    摘要翻译： 由具有SiO 2层间桥的许多SiO 4四面体片组成的多孔材料。 它具有直径为10或更大的孔，并且具有通过金属原子对SiO 4骨架的Si的同晶取代而形成的固体酸的性质。 它是通过包括将有机物质引入到层状硅酸盐晶体的层间空间中以扩大晶体层之间的间距，以及在其间形成二氧化硅之间的过程，使插入的化合物与金属盐接触以连接金属原子 到SiO4框架，并烧制产品。 该材料可以承受800℃的温度，孔径大于沸石等的孔径，并且可用于制备具有高分子量的分子的吸附剂或催化剂，例如用于催化裂化的催化剂 的石油。

    Heat resistant layered porous silica and process for producing the same
    4.
    发明授权
    Heat resistant layered porous silica and process for producing the same 失效
    耐热层状多孔二氧化硅及其制造方法

    公开(公告)号：US5382558A

    公开(公告)日：1995-01-17

    申请号：US087440

    申请日：1993-07-02

    申请人： Shinji Inagaki ,  Yoshiaki Fukushima ,  Akane Okada ,  Kazuhiro Fukumoto ,  Kazuyuki Kuroda

    发明人： Shinji Inagaki ,  Yoshiaki Fukushima ,  Akane Okada ,  Kazuhiro Fukumoto ,  Kazuyuki Kuroda

    IPC分类号： B01J20/10 ,  B01J21/08 ,  B01J23/04 ,  B01J29/04 ,  B01J35/04 ,  B01J20/28

    CPC分类号： B01J35/04 ,  B01J20/10 ,  B01J21/08 ,  B01J23/04 ,  B01J29/049

    摘要： A heat resistant layered porous silica having a honeycomb porous structure comprises a plurality of waved or bent sheet layers of crystalline layered silicate superposed one after another, and the neighboring sheets are partially bonded by siloxane bonding. The spacing between the neighboring sheet layers is narrowed toward the bonded portions and expanded at other portions to thereby form fine pores. The layered porous silica contains alkali metal ions in an amount of 0.2% by weight or less and has a specific surface area of 1,000 m.sup.2 /g or more.The layered porous silica has a large specific surface area, and exhibits an excellent heat resistance and adsorption of organic substances such as fuel.

    摘要翻译： 具有蜂窝状多孔结构的耐热性层状多孔二氧化硅，包括多个叠层的多个波状或弯曲的结晶层状硅酸盐层，相邻的片材通过硅氧烷键部分地结合。 相邻片层之间的间隔朝向接合部变窄，在其他部分膨胀，形成细孔。 层状多孔二氧化硅含有0.2重量％以下的碱金属离子，比表面积为1000m 2 / g以上。 层状多孔二氧化硅具有大的比表面积，并表现出优异的耐热性和有机物质如燃料的吸附。

    Cluster-included material
    7.
    发明授权
    Cluster-included material 失效
    集群包含的材料

    公开(公告)号：US6107243A

    公开(公告)日：2000-08-22

    申请号：US925769

    申请日：1997-09-09

    申请人： Shinji Inagaki ,  Noriaki Sugimoto ,  Tatsumi Hioki ,  Yoshiaki Fukushima ,  Masaru Ichikawa

    发明人： Shinji Inagaki ,  Noriaki Sugimoto ,  Tatsumi Hioki ,  Yoshiaki Fukushima ,  Masaru Ichikawa

    IPC分类号： B01J20/28 ,  B01J20/10

    CPC分类号： B01J20/28083 ,  B01J20/28004 ,  B01J20/28009 ,  B01J20/2803 ,  B01J20/28069 ,  B01J20/28097 ,  Y10T428/24149

    摘要： The present cluster-included material characterized by utilizing a porous host material for clusters having a pore larger in size than that of zeolite. The cluster-included material is obtained by forming a cluster in a pore of a mesoporous material having a pore size of 1.3 to 10 nm. When the mesoporous material is particularly a mesoporous material having a pore volume of not less than 60% of a total pore volume within a pore size range of -40 to +40% of a pore size which shows a maximum peak in a pore size distribution curve, a granular cluster having a uniform particle size or a fine-linear cluster having a uniform diameter is obtained. The cluster-included material performs the various quantum effects.

    摘要翻译： 本发明的包含簇的材料的特征在于利用多孔主体材料用于具有比沸石尺寸更大的孔的簇。 通过在孔径为1.3〜10nm的介孔材料的孔中形成簇而获得含有簇的材料。 当介孔材料特别是孔体积为孔体积的孔体积的最大峰值在孔径的-40〜+ 40％的孔径范围内的孔体积的60％以上的中孔材料时， 得到具有均匀粒径的粒状团簇或具有均匀直径的微细线粒团。 包含簇的材料执行各种量子效应。

    Solid electrolyte
    8.
    发明授权
    Solid electrolyte 有权
    固体电解质

    公开(公告)号：US07488559B2

    公开(公告)日：2009-02-10

    申请号：US10415353

    申请日：2001-10-31

    申请人： Shinji Inagaki ,  Shiyou Guan ,  Yoshiaki Fukushima

    发明人： Shinji Inagaki ,  Shiyou Guan ,  Yoshiaki Fukushima

    IPC分类号： H01M10/40 ,  H01M6/18 ,  H01M8/10

    CPC分类号： H01M8/124 ,  H01B1/122 ,  H01M6/18 ,  H01M8/1027 ,  H01M8/1037 ,  H01M8/1044 ,  H01M8/1067 ,  H01M10/05 ,  Y02P70/56

    摘要： The solid electrolyte of the present invention is composed of an organic/inorganic composite material having pores with a mean pore diameter of 1 to 30 nm and having a skeleton comprising a metal atom, an oxygen atom bonded to the metal atom, and an organic group having at least one carbon atom bonded to the metal atom or the oxygen atom, and a functional group having an ion exchange function and bonded to the organic group inside the pores. As a result, even if the relative pressure of the water vapor in the atmosphere is less than 1.0, it is still possible to achieve a solid electrolyte with a sufficiently high ion conductivity at a lower temperature than with a conventional solid electrolyte such as stabilized zirconia.

    摘要翻译： 本发明的固体电解质由平均孔径为1〜30nm，具有金属原子，与金属原子键合的氧原子和有机基团的骨架的有机/无机复合材料构成 具有与金属原子或氧原子键合的至少一个碳原子，和具有离子交换功能的官能团，并与孔内的有机基团结合。 结果，即使气氛中的水蒸气的相对压力小于1.0，仍然可以在比常规固体电解质如稳定的氧化锆更低的温度下获得具有足够高的离子传导性的固体电解质 。

    Organic/inorganic complex porous materials
    9.
    发明授权
    Organic/inorganic complex porous materials 有权
    有机/无机复合多孔材料

    公开(公告)号：US06248686B1

    公开(公告)日：2001-06-19

    申请号：US09347005

    申请日：1999-07-02

    申请人： Shinji Inagaki ,  Shiyou Guan ,  Yoshiaki Fukushima

    发明人： Shinji Inagaki ,  Shiyou Guan ,  Yoshiaki Fukushima

    IPC分类号： B01J2100

    CPC分类号： C08G77/58 ,  B01J20/103 ,  B01J20/262 ,  B01J20/28083 ,  C08G77/22 ,  C08G83/001

    摘要： Organic/inorganic complex porous materials are disclosed having a main skeletal chain containing metal atoms, oxygen atoms, and organic groups. Preferably, the metal atoms, oxygen atoms and organic groups are bound by ionic bonds and/or covalent bonds, and the organic group is bound to at least two metal atoms in the main chain of the skeleton of the porous material. More preferably, 60% or more of the total pore volume in the porous material has a pore diameter in a range of ±40% of the pore diameter, as determined from the maximum peak in a pore size distribution curve. Alternatively, at least one peak is present at a diffraction angle that preferably corresponds to a d value of at least 1 nm in an x-ray diffraction pattern. Method of making such organic/inorganic complex materials are also disclosed.

    摘要翻译： 公开了具有含有金属原子，氧原子和有机基团的主骨架链的有机/无机复合多孔材料。 优选地，金属原子，氧原子和有机基团通过离子键和/或共价键结合，并且有机基团结合到多孔材料的骨架的主链中的至少两个金属原子。 更优选地，多孔材料中的总孔体积的60％以上具有从孔径分布曲线中的最大峰值确定的孔径在±40％范围内的孔径。 或者，在x射线衍射图中优选对应于至少1nm的d值的衍射角处存在至少一个峰。 还公开了制备这种有机/无机复合材料的方法。