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1.发明授权Composite ultrafine particles of nitrides, method for production and sintered article thereof 失效氮化物的复合超微粒子，其制造方法及其烧结体
公开(公告)号：US5549951A
公开(公告)日：1996-08-27
申请号：US301879
申请日：1994-09-07
IPC分类号： B01J19/08 , B22F9/12 , C01B21/06 , C01G55/00 , C04B35/58 , C04B35/581 , C22C32/00 , C30B25/00 , B22F7/00
CPC分类号： C04B35/58042 , B22F9/12 , B82Y30/00 , C01B21/0602 , C04B35/58 , C04B35/581 , C22C32/0068 , C30B25/005 , C30B29/38 , C01P2002/72 , C01P2004/04 , C01P2004/10 , C01P2004/64 , C01P2004/82 , Y10T428/12 , Y10T428/12014 , Y10T428/12056 , Y10T428/12146 , Y10T428/12181
摘要： Ultrafine whiskery or columnar ceramic particles, a method for producing the ultrafine particles, and a sintered article obtained by sintering the ultrafine ceramic particles are disclosed. The ultrafine ceramic particles are produced by thermally melting a matrix alloy of a composition of Al--M.sup.1, wherein M.sup.1 stands for at least one metallic element selected from the group consisting of Cr, Co, and Fe, or Al--M.sup.1 --M.sup.2, wherein M.sup.2 stands for at least one metallic element selected from the group consisting of Au, Cu, Dy, Er, Ga, Ge, Gd, Hf, Ho, Lu, Mn, Mo, Nb, Nd, Ni, Pr, Re, Sb, Sc, Si, Sn, Ta, Tb, Ti, Tm, V, W, Y, Zn, or Zr, in a nitriding atmosphere containing nitrogen and causing the vaporized raw material to react with the nitrogen in the atmosphere. By this method, ultrafine composite particles or a mixture comprising ultrafine whiskery or columnar aluminum nitride particles and ultrafine particles of the metal, the intermetallic compound of the metal with aluminum, and the nitride ceramic of the metal are produced. The ultrafine particles thus obtained find extensive utility as sintering materials and dispersion materials, for example.
摘要翻译： 公开了超细威士忌或柱状陶瓷颗粒，超细颗粒的制造方法和通过烧结超细陶瓷颗粒而获得的烧结体。 超细陶瓷颗粒是通过将Al-M1组成的基体合金热熔而制造的，其中M1代表选自Cr，Co和Fe中的至少一种金属元素或Al-M1-M2，其中 M2代表选自Au，Cu，Dy，Er，Ga，Ge，Gd，Hf，Ho，Lu，Mn，Mo，Nb，Nd，Ni，Pr，Re，Sb中的至少一种金属元素， Sc，Si，Sn，Ta，Tb，Ti，Tm，V，W，Y，Zn或Zr中的至少一种，并且使气化的原料与大气中的氮反应。 通过这种方法，制造超细复合颗粒或包含超细威士忌或柱状氮化铝颗粒和金属超细颗粒，金属与铝的金属间化合物和金属的氮化物陶瓷的混合物。 如此得到的超细颗粒例如可用作烧结材料和分散材料。
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公开(公告)号：US5518522A
公开(公告)日：1996-05-21
申请号：US209148
申请日：1994-03-10
CPC分类号： B22F9/14 , B01J35/026 , B22F1/0007 , F01N2330/08
摘要： A deformed ultra fine grain is comprised of a spherical body and a tail-like projection projecting from the surface of the spherical body. The tail-like projection exhibits a separating effect on the adjacent deformed ultra fine grains and therefore, aggregation of the ultra fine grains is avoided. Bulk quantities of the deformed ultra fine grains are produced by evaporating a metal by a plasma arc in a controlled atmosphere having a gas that combines with the material of the spherical body to form the tail-like projection.
摘要翻译： 变形的超细晶粒由球形体和从球体的表面突出的尾状突起构成。 尾状凸起对相邻的变形超细晶粒呈现分离效果，因此避免了超细晶粒的聚集。 通过在具有与球体的材料结合的气体的受控气氛中通过等离子弧蒸发金属来制造大量的变形的超细晶粒，以形成尾状突起。
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3.发明授权
公开(公告)号：US5800638A
公开(公告)日：1998-09-01
申请号：US313464
申请日：1994-09-27
IPC分类号： B22F9/14 , B01J21/02 , B01J23/656 , B22F1/00 , B22F9/12 , C01B3/22 , C22C1/00 , C22C1/04 , C22C21/00 , C22C45/08
CPC分类号： B22F9/12 , B01J21/02 , C01B3/22 , C22C1/0416 , C22C45/08 , B22F2999/00
摘要： Quasi-crystalline aluminum alloy ultrafine particles are produced by a gas-phase reaction and consist of at least one alloy element from the group of V, Cr, Mn, Fe, Co, Ni, Cu and Pd, for example palladium (Pd) in an amount represented by 20 atomic %.ltoreq.Pd.ltoreq.30 atomic %, and the balance of aluminum. Palladium has a catalyst power, and the ultrafine particles have a large specific surface area, because they have a particle size d.ltoreq.200 nm. Such ultrafine particles have a high catalytic activity in a methanol decomposing reaction and also have a good retention of catalytic activity.
摘要翻译： 准晶体铝合金超细颗粒是通过气相反应生成的，由至少一种由V，Cr，Mn，Fe，Co，Ni，Cu和Pd组成的合金元素组成，例如钯（Pd） 由20原子％
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公开(公告)号：US5578108A
公开(公告)日：1996-11-26
申请号：US313827
申请日：1994-09-28
CPC分类号： B22F9/12 , C22C1/002 , C22C45/02 , C22C45/10 , B22F2999/00
摘要： Ultrafine amorphous metal particles which combine the properties of ultrafine particles with those of an amorphous alloy and a method for the production thereof are disclosed. The ultrafine amorphous metal particles are produced by a method which comprises discharging a plasma arc against a raw metal capable of forming a carbide in a reaction gas using an inert gas as a main component thereof and containing a hydrocarbon gas, and allowing the metal which has been consequently vaporized to contact the reaction gas which has been consequently converted into a plasma, thereby inducing formation of a solid solution of carbon atoms in the vaporized metal and quenching the solid solution in the reaction gas to confer an amorphous structure thereon. As the raw metal, at least one metal selected from the group consisting of Fe, Mo, Nb, Ta, Ti, Zr, Al, Si, and Cr is preferably used. By this method are obtained ultrafine amorphous metal particles which comprise the metal mentioned above, possess at least 50% by volume of an amorphous phase, and have particle diameters of not more than 500 nm.
摘要翻译： 公开了将超细颗粒的性质与非晶合金的特性结合的超细无定形金属颗粒及其制造方法。 超细非晶态金属颗粒通过以下方法制造：使用惰性气体作为主要成分并含有烃气体的反应气体中能够形成碳化物的原料的等离子体电弧放电， 随后蒸发以接触已经转化成等离子体的反应气体，从而在蒸发的金属中引起碳原子的固溶体的形成，并淬灭反应气体中的固溶体以赋予其非晶结构。 作为原料金属，优选使用选自Fe，Mo，Nb，Ta，Ti，Zr，Al，Si和Cr中的至少一种金属。 通过该方法获得了包含上述金属的超细无定形金属颗粒，具有至少50体积％的非晶相，并且具有不大于500nm的粒径。
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5.发明授权Composite ultrafine particles of aluminum nitride and rare earth nitride, method for production and sintered article thereof 失效氮化铝和稀土氮化物的复合超细颗粒，其生产方法及其烧结制品
公开(公告)号：US5468697A
公开(公告)日：1995-11-21
申请号：US212864
申请日：1994-03-15
IPC分类号： C01B21/06 , C01B21/072 , C04B35/581 , C30B11/00
CPC分类号： B82Y30/00 , C01B21/0602 , C01B21/0724 , C04B35/581 , C30B11/00 , C30B29/38 , C01P2002/72 , C01P2004/04 , C01P2004/10 , C01P2004/11 , C01P2004/20 , C01P2004/50 , C01P2004/54 , C01P2004/64
摘要： Ultrafine particles of aluminum nitride having a morphologically anisotropic structure of columns, plates, or whiskers such that the ratio of thickness or width to length or the ratio of thickness to width or length of particle is not less than 1 are produced by thermally melting a binary alloy of metallic aluminum and a rare earth element in a nitriding atmosphere containing nitrogen. By this method are produced composite ultrafine particles which substantially comprise ultrafine particles of aluminum nitride having the morphologically anisotropic structure and ultrafine particles of the rare earth nitride which functions as a sintering auxiliary therefor. The composite ultrafine particles or an aggregate thereof are usable as a raw material for the production of a sintered article, a reinforcing material for various metal-based composite materials, a blast powder, and the like.
摘要翻译： 具有柱，板或晶须的形态各向异性结构的氮化铝的超细颗粒，使得厚度或宽度与长度的比率或者颗粒的厚度与宽度或长度的比率不小于1是通过将二元 金属铝和稀土元素的合金在含氮的氮化气氛中。 通过该方法制造了复合超细颗粒，其基本上包含具有形态各向异性结构的氮化铝的超细颗粒和作为其烧结助剂的稀土氮化物的超细颗粒。 复合超细颗粒或其聚集体可用作生产烧结制品的原料，用于各种金属基复合材料的增强材料，鼓风粉末等。
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公开(公告)号：US5436080A
公开(公告)日：1995-07-25
申请号：US943324
申请日：1992-09-10
CPC分类号： C22C1/10 , B22F1/025 , C22C32/0068 , C30B23/02 , Y10T428/12014 , Y10T428/12181
摘要： A structural member is produced using starting powder consisting of composite particulates each containing AlN grain within its surface covered by an Al layer of a single crystal structure, and Al alloy particulates of a single crystal structure, and then by sintering the Al layers of the composite particulates with the Al alloy particulates. The Al layers and the Al alloy particulates of the single crystal structure have no dislocation fault, crystal grain boundary. etc., produced therein, and for this reason, they have a low chemical activity. Therefore, the Al layers and the like have a characteristic that they are extremely difficult to oxidize. This ensures that the Al layers and the Al alloy particulates can be reliably sintered to achieve the densification of the resulting structural member.
摘要翻译： 使用由在由Al单晶结构覆盖的表面内含有AlN晶粒的复合颗粒和单晶结构的Al合金微粒组成的起始粉末制造结构构件，然后通过烧结复合材料的Al层 颗粒与Al合金微粒。 单晶结构的Al层和Al合金微粒没有位错，晶界。 等等，因此，它们具有低的化学活性。 因此，Al层等具有极难氧化的特性。 这确保了Al层和Al合金颗粒可以可靠地烧结以实现所得结构构件的致密化。
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公开(公告)号：US5405458A
公开(公告)日：1995-04-11
申请号：US120523
申请日：1993-09-14
申请人： Hiroshi Yamagata , Tadashi Yamaguchi , Hideki Takeda , Nobuyuki Nishiyama , Katsutoshi Nozaki , Akihisa Inoue , Tsuyoshi Masumoto
发明人： Hiroshi Yamagata , Tadashi Yamaguchi , Hideki Takeda , Nobuyuki Nishiyama , Katsutoshi Nozaki , Akihisa Inoue , Tsuyoshi Masumoto
IPC分类号： C23C14/00 , C23C14/06 , C23C14/22 , C23C14/24 , C23C14/32 , C23C14/34 , C22C14/00 , C22C1/00 , C22C29/00
CPC分类号： C23C14/0021 , C23C14/0641 , C23C14/0688 , Y10T428/12486 , Y10T428/12576
摘要： Deposition of a hard film of Ti--Si--N composite material on a substrate is carried out by using a source of evaporation possessing a composition of Ti.sub.a Si.sub.b (wherein "a" and "b" stand for atomic percentages respectively falling in the ranges of 75 at %.ltoreq.a.ltoreq.85 at % and 15 at %.ltoreq.b.ltoreq.25 at %, providing a+b=100 at %). Deposition is effected by a sputtering process or ion plating process in an atmosphere of an inert gas containing a nitrogen-containing reaction gas while controlling the feed rate of the reaction gas into a chamber in such a manner that the partial pressure of nitrogen is kept constant or varied continuously or stepwise. By this method, there can be obtained a film having fine TiN crystalline particles uniformly dispersed in the matrix phase of Ti--Si amorphous metal or a film of functionally gradient structure in which the ratio of fine TiN crystalline particles dispersed in the matrix phase increases continuously or stepwise in the direction of thickness of the film.
摘要翻译： 通过使用具有TiaSib组成的蒸发源（其中“a”和“b”表示分别落在75的范围内的原子百分比），将Ti-Si-N复合材料的硬膜沉积在基板上 at％
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公开(公告)号：US5423923A
公开(公告)日：1995-06-13
申请号：US315620
申请日：1994-09-30
申请人： Hiroshi Yamagata , Tadashi Yamaguchi , Hideki Takeda , Nobuyuki Nishiyama , Katsutoshi Nozaki , Akihisa Inoue , Tsuyoshi Masumoto
发明人： Hiroshi Yamagata , Tadashi Yamaguchi , Hideki Takeda , Nobuyuki Nishiyama , Katsutoshi Nozaki , Akihisa Inoue , Tsuyoshi Masumoto
IPC分类号： C23C14/00 , C23C14/06 , C23C14/22 , C23C14/24 , C23C14/32 , C23C14/34 , C22C14/00 , C22C1/00 , C22C29/00
CPC分类号： C23C14/0021 , C23C14/0641 , C23C14/0688 , Y10T428/12486 , Y10T428/12576
摘要： Deposition of a hard film of Ti-Si-N composite material on a substrate is carried out by using a source of evaporation possessing a composition of Ti.sub.a Si.sub.b (wherein "a" and "b" stand for atomic percentages respectively falling in the ranges of 75 at % .ltoreq.a.ltoreq.85 at % and 15 at %.ltoreq.b.ltoreq.25 at %, providing a+b=100 at %). Deposition is effected by a sputtering process or ion plating process in an atmosphere of an inert gas containing a nitrogen-containing reaction gas while controlling the feed rate of the reaction gas into a chamber in such a manner that the partial pressure of nitrogen is kept constant or varied continuously or stepwise. By this method there can be obtained a film having fine TiN crystalline particles uniformly dispersed in the matrix phase of Ti-Si amorphous metal or a film of functionally gradient structure in which the ratio of fine TiN crystalline particles dispersed in the matrix phase increases continuously or stepwise in the direction of thickness of the film.
摘要翻译： 通过使用具有TiaSib组成的蒸发源（其中“a”和“b”表示分别落在75的范围内的原子百分比），将Ti-Si-N复合材料的硬膜沉积在基底上 at％
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公开(公告)号：US09318238B2
公开(公告)日：2016-04-19
申请号：US14345053
申请日：2011-10-04
申请人： Tadashi Yamaguchi , Shigehiro Sasai
发明人： Tadashi Yamaguchi , Shigehiro Sasai
CPC分类号： H01B7/04 , H01B11/00 , H01B11/1808 , H01B11/1856 , H01B13/0006
摘要： A hollow core body for signal transmission cable comprises an inner conductor that employs a compressed bunched conductor formed by bunching and compressing plural strands such that a cross-section of the compressed bunched conductor is substantially circular, and a hollow insulating core that includes an inner annular member, rib members, an outer annular member, and hollow members. Accordingly, as almost no recesses are produced on the circumferential surface of the compressed bunched conductor, weakening of the mechanical strength due to presence of recesses on the circumferential surface of the inner conductor can be suppressed.
摘要翻译： 用于信号传输电缆的中空芯体包括内导体，其使用通过聚束和压缩多股而形成的压缩聚束导体，使得压缩的聚束导体的横截面基本上为圆形，以及中空绝缘芯，其包括内环形 构件，肋构件，外环形构件和中空构件。 因此，由于在压缩的聚束导体的圆周表面上几乎没有产生凹陷，因此可以抑制由于在内导体的圆周表面上存在凹陷而导致的机械强度的弱化。
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公开(公告)号：US07875894B2
公开(公告)日：2011-01-25
申请号：US11543196
申请日：2006-10-05
申请人： Tadashi Yamaguchi
发明人： Tadashi Yamaguchi
IPC分类号： H01L23/48
CPC分类号： H01L24/11 , H01L2223/5448 , H01L2224/0401 , H01L2224/05124 , H01L2224/05144 , H01L2224/05147 , H01L2224/05557 , H01L2224/05559 , H01L2224/05571 , H01L2224/05572 , H01L2224/05647 , H01L2224/13006 , H01L2224/13022 , H01L2224/13023 , H01L2224/13099 , H01L2224/16 , H01L2924/0002 , H01L2924/01005 , H01L2924/01006 , H01L2924/01013 , H01L2924/01029 , H01L2924/01033 , H01L2924/01074 , H01L2924/01079 , H01L2924/014 , H01L2924/14 , H01L2924/181 , H01L2224/05552 , H01L2924/00 , H01L2924/00014 , H01L2924/013
摘要： A semiconductor device includes a semiconductor chip having electrode pads, and a rewiring pattern having interconnects which are connected to the electrode pads and extend over an insulation film. The semiconductor device also includes columnar electrodes each of which has a main body section and a protrusion section, and a sealing section which has a top face having a height the same as the top faces of the protrusion sections. The semiconductor device also includes solder balls formed on the protrusion sections. The semiconductor device also has trenches in the sealing section. Each trench has a depth which reaches the boundary between the main body and protrusion of the electrode. The side faces of the protrusion section are exposed face defined by the trenches. Each solder ball is electrically connected to the top face and side faces of the protrusion section of each electrode.
摘要翻译： 半导体器件包括具有电极焊盘的半导体芯片和具有连接到电极焊盘并且在绝缘膜上延伸的互连的重新布线图案。 半导体器件还包括柱状电极，每个柱状电极具有主体部分和突出部分，以及具有与突起部分的顶面相同高度的顶面的密封部分。 半导体器件还包括形成在突出部分上的焊球。 半导体器件还在密封部分中具有沟槽。 每个沟槽的深度达到主体和电极突起之间的边界。 突出部分的侧面是由沟槽限定的露出面。 每个焊球与每个电极的突出部分的顶面和侧面电连接。
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