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公开(公告)号：US5564105A
公开(公告)日：1996-10-08
申请号：US446154
申请日：1995-05-22
CPC分类号： C02F1/76 , C02F1/72 , C02F1/722 , C02F1/78 , C02F2101/006
摘要： A borated aqueous solution from a nuclear reactor coolant system dilute chemical-decontamination process or from an equipment washing process which has been contaminated with radioactive metals or heavy metals including cobalt, nickel, chromium, iron, manganese, lead or mercury and with a chelating agent, detergent or soap is treated with an oxidizing agent to oxidize the chelating agent, detergent or soap and to precipitate the contaminant metals. The contaminant metals are then separated from the solution by centrifugal filtration, micromembrane belt filtration or magnetic separation. Advantageously, a very small volume of precipitate may then be buried and the decontaminated solution may be recycled or further treated and released for other uses.
摘要翻译： 来自核反应堆冷却剂系统的硼酸化水溶液稀释化学去污过程或已经被放射性金属或重金属（包括钴，镍，铬，铁，锰，铅或汞）和螯合剂污染的设备清洗过程 ，用氧化剂处理洗涤剂或肥皂以氧化螯合剂，洗涤剂或肥皂并沉淀污染金属。 然后通过离心过滤，微膜带过滤或磁分离将污染金属与溶液分离。 有利地，可以埋入非常小体积的沉淀物，并且净化的溶液可以再循环或进一步处理并释放用于其它用途。
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2.发明授权Reinforced composites made by electro-phoretically coating graphite or carbon 失效通过电石墨涂覆石墨或碳素制成的增强复合材料
公开(公告)号：US4664768A
公开(公告)日：1987-05-12
申请号：US717046
申请日：1985-03-28
CPC分类号： C09D5/44 , B32B5/28 , C25D13/12 , Y10T428/30 , Y10T442/2951 , Y10T442/2984 , Y10T442/3512
摘要： Disclosed is a method of making a laminate by electrophoretically coating a flat mat made from a material selected from graphite, carbon, and mixtures thereof with an electrophoretable polymer in a non-aqueous system. The polymer is cured and the mat is impregnated with a thermosetable impregnating resin. The impregnating resin is B-staged to form a prepreg and several prepregs are stacked and cured under heat and pressure to form the laminate. Also disclosed is a laminate made by this method.
摘要翻译： 公开了一种通过在非水系统中电泳涂覆由选自石墨，碳及其与电泳聚合物的混合物的材料制成的平垫而制备层压体的方法。 聚合物固化，并且用可热固性浸渍树脂浸渍垫。 浸渍树脂B阶分级以形成预浸料坯，并且在加热和加压下堆叠并固化数个预浸料以形成层压体。 还公开了通过该方法制成的层压体。
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公开(公告)号：US4895673A
公开(公告)日：1990-01-23
申请号：US755135
申请日：1985-07-12
申请人： William M. Alvino , Ram S. Raghava
发明人： William M. Alvino , Ram S. Raghava
IPC分类号： B32B27/04 , C08J3/09 , C09D5/44 , C09D163/00 , D01F11/14
CPC分类号： B32B27/04 , C08J3/09 , C09D5/44 , D01F11/14 , Y10S524/901 , Y10S524/923 , Y10T442/2984 , Y10T442/3569 , Y10T442/3585
摘要： Disclosed is an emulsion having a discontinuous phase which comprises at least two compounds of different structural formula selected from the group consisting of solvent-soluble polymers, oligomers, and monomers dissolved in an organic solvent, and a discontinuous phase which comprises an organic non-solvent for the compounds. A method of coating a conductor with a polymeric alloy is also disclosed. The conductor is immersed in the emulsion and a direct current is applied between the conductor and the emulsion sufficient to cause the discontinuous phase of the emulsion to migrate to the conductor and deposit on it. The conductor is removed from the emulsion and is dried and the deposit is cured.
摘要翻译： 公开了具有不连续相的乳液，其包含至少两种不同结构式的化合物，其选自溶剂可溶性聚合物，低聚物和溶解在有机溶剂中的单体，以及包含有机非溶剂的不连续相 化合物。 还公开了一种用聚合物合金涂覆导体的方法。 导体浸入乳液中，并且在导体和乳液之间施加直流电流，足以使乳液的不连续相迁移到导体并沉积在其上。 将导体从乳液中取出并干燥，沉积物固化。
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4.发明授权
公开(公告)号：US4781986A
公开(公告)日：1988-11-01
申请号：US79075
申请日：1987-07-29
申请人： William M. Alvino
发明人： William M. Alvino
CPC分类号： C08G18/721 , C08G18/3221 , C08G18/4277 , C09J175/04 , Y10T428/31565
摘要： Disclosed is a method of making an adhesive comprising forming a first composition of a polyesterether glycol having the general formula ##STR1## where R.sub.1 and R.sub.2 are each independently selected from alkylidene from C.sub.1 to C.sub.10, and n is about 1 to about 5 about 0.01 to about 1% by weight (based on the weight of the polyesterether glycol) of a catalyst, and sufficient solvent for said adhesive to have at least 50% solids, forming a second composition of about 0.85 to about 0.95 mole % of a diisocyanate and about 0.15 to about 0.05 mole % of a polyisocyanate, and mixing the first and second compositions together. The adhesive is applied to a first substrate, the solvent is evaporated, and a second substrate is pressed against the adhesive on the first substrate to form a flexible laminate.
摘要翻译： 公开了一种制备粘合剂的方法，包括形成具有通式“IMAGE”的聚异戊二醇的第一组合物，其中R 1和R 2各自独立地选自C 1至C 10的亚烷基，n为约1至约5约0.01至 约1重量％（基于聚醚醚二醇的重量）的催化剂，以及足够的用于所述粘合剂的溶剂具有至少50％的固体，形成第二组合物约0.85至约0.95摩尔％的二异氰酸酯和约 0.15至约0.05摩尔％的多异氰酸酯，并将第一和第二组合物混合在一起。 将粘合剂施加到第一基底上，蒸发溶剂，并且将第二基底压在第一基底上的粘合剂上以形成柔性层压体。
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5.发明授权Moisture resistant laminates impregnated with an impregnating composition comprising epoxy resin and a dicyandiamide derivative 失效用含有环氧树脂和双氰胺衍生物的浸渍组合物浸渍的耐湿层压材料
公开(公告)号：US4327143A
公开(公告)日：1982-04-27
申请号：US228016
申请日：1981-01-23
CPC分类号： C08J5/24 , B32B27/04 , C08G59/4021 , H05K1/0326 , H05K1/036 , C08J2363/00 , H05K1/0366 , H05K2201/0284 , H05K2201/0293 , Y10S428/901 , Y10T442/2992 , Y10T442/3415 , Y10T442/3431
摘要： A resin impregnated, B-staged sheet material free of crystal formations, useful for metal clad and unclad laminate production, is made by impregnating a sheet containing a resin comprising epoxy resin and an amount of curing agent effective to cure the epoxy resin to the C-stage, where the curing agent consists essentially of the reaction product of dicyandiamide and an aminophylic reagent selected from the group consisting of aldehydes, alkyl monoglycidyl ethers having the formula: ##STR1## where R=an alkyl group having from 1 to 4 carbon atoms, styrene oxide, ethylene oxide, propylene oxide, acetic anhydride, benzoyl chloride, acetyl chloride, and mixtures thereof, and then heating the impregnated sheet until the resin is in the B-stage.
摘要翻译： 通过将含有环氧树脂的树脂和一定量的有效固化环氧树脂的固化剂的片浸渍到C中来制备可用于金属包覆和未包覆层压板生产的不含结晶形成的树脂浸渍的B阶片材 阶段，其中固化剂基本上由双氰胺和选自以下的氨基酚试剂的反应产物组成：醛，具有下式的烷基单缩水甘油醚：其中R =具有1至4个碳原子的烷基 ，氧化苯乙烯，环氧乙烷，环氧丙烷，乙酸酐，苯甲酰氯，乙酰氯及其混合物，然后加热浸渍的片材直到树脂处于B阶段。
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公开(公告)号：US4221840A
公开(公告)日：1980-09-09
申请号：US876818
申请日：1978-02-10
申请人： William M. Alvino
发明人： William M. Alvino
IPC分类号： C08F283/00 , C08G18/69 , C09J175/14 , H05K3/38 , C08L75/00
CPC分类号： C08G18/69 , C08F283/00 , C09J175/14 , H05K3/386 , H05K2201/0133 , H05K2201/0355 , Y10S525/92 , Y10T428/31562 , Y10T428/31721
摘要： An adhesive composition free of free-radical catalysts is disclosed comprising hydroxy terminated 1,2-polybutadiene, a diisocyanate, and either styrene, vinyl toluene, or a mixture thereof. The adhesive composition is A-staged whence a free-radical catalyst is added. A material such as a film or fibrous reinforcement is coated with the composition and the composition is B-staged. The coated material can be cured during lamination with copper in a heated nip roll.
摘要翻译： 公开了一种不含游离基催化剂的粘合剂组合物，其包含羟基封端的1,2-聚丁二烯，二异氰酸酯和苯乙烯，乙烯基甲苯或其混合物。 粘合剂组合物是A级，其中加入自由基催化剂。 用该组合物涂覆诸如薄膜或纤维增强材料的材料，组合物为B阶段。 涂覆的材料可以在加热夹辊中与铜层压期间固化。
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公开(公告)号：US4425467A
公开(公告)日：1984-01-10
申请号：US342029
申请日：1982-01-21
CPC分类号： C09D5/4461 , C08J3/09 , C09D5/4419 , Y10S524/901
摘要： Disclosed is a method of making a non-aqueous emulsion from which a polymer can be electrodeposited. A mixture is prepared of about 50 to about 150 parts by weight of a non-aqueous organic, non-electrolizable, non-solvent for the polymer with about 0.8 to about 1.2 parts by weight of a nitrogen-containing base which can be a tertiary amine, an imidazole, or mixture of a tertiary amine and an imidazole. To the mixture is added a solution of 1 part by weight of the polymer which can be a polyamic acid, a polyamide imide, a polyimide, a polyparabanic acid, a polysulfone, or a mixture of these polymers. The polymer is in a non-aqueous, organic, non-electrolizable aprotic solvent such as N-methyl-2-pyrrolidone.
摘要翻译： 公开了一种制备非水乳液的方法，由该聚合物可电沉积。 制备约50至约150重量份的聚合物的非水有机非电解非溶剂，其中约0.8至约1.2重量份的含氮碱可以是叔 胺，咪唑或叔胺和咪唑的混合物。 向混合物中加入1重量份可以是聚酰胺酸，聚酰胺酰亚胺，聚酰亚胺，聚对苯二甲酸，聚砜或这些聚合物的混合物的聚合物的溶液。 该聚合物是非水，有机，不可电解的非质子溶剂如N-甲基-2-吡咯烷酮。
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8.发明授权Flame-resistant aqueous epoxy impregnating compositions containing nonionic surface active agents 失效含有非离子表面活性剂的耐火水性环氧树脂浸渍组合物
公开(公告)号：US4421877A
公开(公告)日：1983-12-20
申请号：US415096
申请日：1982-09-07
申请人： William M. Alvino
发明人： William M. Alvino
CPC分类号： C08J3/03 , C08G59/4021 , C08G59/621 , H05K1/0326 , H05K1/0373 , C08J2363/00 , H05K2201/012 , H05K2203/122 , Y10S428/901
摘要： Aqueous emulsions of epoxy resins, which can be used to treat glass cloth used in the preparation of printed circuit board laminates, are produced by combining an epoxy resin and a flame retardant phenol, such as tetrabromobisphenol A, with a selected nonionic surface active agent, such as an alkylaryl polyether alcohol, monomethylol dicyandiamide curing agent and, if needed, a catalyst.
摘要翻译： 可用于处理用于制备印刷电路板层压体的玻璃布的环氧树脂的水性乳液通过将环氧树脂和诸如四溴双酚A的阻燃酚与选择的非离子表面活性剂组合而制备， 例如烷基芳基聚醚醇，单羟甲基双氰胺固化剂和如果需要的催化剂。
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公开(公告)号：US4214071A
公开(公告)日：1980-07-22
申请号：US567220
申请日：1975-04-11
IPC分类号： C08G73/14
CPC分类号： C08G73/14
摘要： Amide-imide polymers formable in deep section and prepared by the condensation reaction of at least one of a diacid halide or a polyanhydride or equivalent, and a diamine containing at least one imide linkage. Soluble amide-imide polymers having the general formula: ##STR1## where n is an integer greater than 10 and preferably greater than 20. A novel amine having the general structural formula: ##STR2## wherein: A is selected from the group consisting of --R'-- and ##STR3## R is a trivalent organic radical in which the two valences included in the imide ring are attached to adjacent carbon atoms and the third valence is attached to a different carbon atom,R' is a divalent organic radical,R" is a tetravalent organic radical in which the bonds are attached to two pairs of adjacent carbon atoms, so that five or six membered imide rings are formed,a, b, c, and d are integers from 0 to 6, the sum of a, b, c, and d is an integer from 1 to 6, at least one R or R" group is included in the molecule, and the bracketed groups are in any order.Although one or more of the R, R', or R" radicals may contain one or more additional amino groups or other compatible linkages, preferably said amine contains only said terminal amino groups.
摘要翻译： 酰胺酰亚胺聚合物可以在深部分形成并通过二酸卤化物或聚酐或等同物中的至少一种与包含至少一个酰亚胺键的二胺的缩合反应制备。 （A）的影响的酰胺 - 酰亚胺聚合物，其中n是大于10，优选大于20的整数。具有 一般结构式：其中：A选自-R'-和
，R是三价有机基团，其中两价包括在 酰亚胺环与相邻碳原子连接，第三价键连接到不同的碳原子上，R'是二价有机基团，R“是四价有机基团，其中键连接到两对相邻的碳原子上， 使得形成五或六元酰亚胺环，a，b，c和d为0至6的整数，a，b，c和d之和为1至6的整数，至少一个R或 R“基团包含在分子中，并且括号中的基团按任何顺序排列。 虽然R，R'或R“基团中的一个或多个可以含有一个或多个另外的氨基或其它相容的键，但优选所述胺仅含有所述末端氨基。 -
公开(公告)号：USRE29134E
公开(公告)日：1977-02-08
申请号：US573285
申请日：1975-04-30
CPC分类号： C08G73/1007 , C08G18/346 , C08G73/1035 , Y10T428/31681 , Y10T428/31721
摘要： A composition is disclosed of a dianhydride and a tetracarboxylic acid in the proportions of about 50 to about 70 mole % dianhydride to about 30 to about 50 mole % tetracarboxylic acid, a stoichiometric amount of an aromatic diisocyanate, and a solvent for the dianhydride, the tetracarboxylic acid, and the diisocyanate. A polyimide precursor is prepared by heating the composition at about 30.degree. to 70.degree. C until the evolution of carbon dioxide substantially ceases, and then at about 30.degree. to about 100.degree. C until its viscosity is about Q to about Z6 on the Gardner-Holdt viscosity scale at 18% solids. The polyimide precursor can be spread on a substrate and cured to produce a polyimide film or coated on a wire and cured to produce a polyimide wire enamel.
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