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    Soot Reduction By Combustor Conditioning
    4.
    发明申请
    Soot Reduction By Combustor Conditioning 有权
    燃烧器调节烟尘减少

    公开(公告)号：US20100186387A1

    公开(公告)日：2010-07-29

    申请号：US12358635

    申请日：2009-01-23

    Applicant: Robert James Perry ,  Patrick Pastecki

    Inventor： Robert James Perry ,  Patrick Pastecki

    IPC: F01N9/00

    CPC classification number: F23K5/10 ,  C10L1/26 ,  C10L1/2608 ,  C10L1/2616 ,  C10L1/2633 ,  C10L1/2641 ,  C10L1/265 ,  C10L10/02

    Abstract: A method of affecting soot particulate size in an internal combustion engine exhaust by selectively providing a phosphorous based additive to the engine during combustion. Soot particulate size can be increased or decreased depending on the particular additive provided. Also disclosed in a conditioning effect experienced by using a phosphorous based additive for a period of time. A conditioned engine can also have its exhaust properties affected during the life of its conditioned state. Manipulating particle size during engine operation can employ an oligomeric phosphorous compound. Engine conditioning can employ a monomeric phosphorous containing compound, an oligomeric phosphorous containing compound, a polymeric phosphorous containing compound, or combinations thereof.

    Abstract translation: 一种通过在燃烧期间选择性地向发动机提供磷基添加剂来影响内燃机排气中烟尘颗粒尺寸的方法。 根据所提供的特定添加剂，烟灰颗粒尺寸可以增加或减少。 还在通过使用基于磷的添加剂经历一段时间的调理效果中也公开。 经调节的发动机在其调节状态的寿命期间也可以具有受其影响的排气性能。 在发动机操作期间操纵粒度可以使用低聚磷化合物。 发动机调节可以使用含单体磷的化合物，含低聚磷的化合物，含聚合磷的化合物或其组合。

    Method of preparing monothiophosphoric acid by sulfurizing a phosphite in the presence of an amide
    9.
    发明授权
    Method of preparing monothiophosphoric acid by sulfurizing a phosphite in the presence of an amide 失效
    在酰胺存在下硫化亚磷酸盐制备单硫代磷酸的方法

    公开(公告)号：US4997968A

    公开(公告)日：1991-03-05

    申请号：US413897

    申请日：1989-09-28

    Applicant: Louis Burjes ,  Alan C. Clark

    Inventor： Louis Burjes ,  Alan C. Clark

    IPC: B01J31/02 ,  C07B61/00 ,  C07F9/17 ,  C10L1/26 ,  C10M137/10 ,  C10M159/12 ,  C10N30/06 ,  C10N40/25

    CPC classification number: C10M159/123 ,  C07F9/17 ,  C10L1/265 ,  C10M137/105 ,  C10M2223/047

    Abstract: A method of preparing an oil-soluble composition is disclosed. The method comprises preparing a dihydrocarbyl monothiophosphoric acid characterized by the formula ##STR1## wherein R.sub.1 and R.sub.2 are each independently hydrocarbyl groups of from 1 to about 30 carbon atoms and X is oxygen or sulfur, with the proviso that one X is sulfur comprising reacting(A) a phosphite ester of the structure ##STR2## with (B) a sulfur source, in the presence of(C) a catalytic amount of an amide of the structure R.sub.3 CONR.sub.4 R.sub.5 wherein R.sub.3, R.sub.4 and R.sub.5 are each independently hydrogen or a hydrocarbyl group containing from 1 to about 30 carbon atoms or an ethoxylated amide of the structure ##STR3## wherein the sum of x and y is from 1 to about 50; and isolating the reaction product obtained.

    Abstract translation: 公开了制备油溶性组合物的方法。 该方法包括制备特征为式（I）的二烃基一硫代磷酸，其中R 1和R 2各自独立地为具有1至约30个碳原子的烃基，X为氧或硫，条件是一个X为硫 包括在（C）催化量的结构为R3CONR4R5的酰胺的存在下，使（A）结构为“IMAGE”的亚磷酸酯与（B）硫源反应，其中R 3，R 4和R 5各自独立地为氢或 含有1至约30个碳原子的烃基或结构“IMAGE”的乙氧基化酰胺，其中x和y的总和为1至约50; 并分离得到的反应产物。

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