公开(公告)号：US09925126B2

公开(公告)日：2018-03-27

申请号：US15486579

申请日：2017-04-13

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Brant U. Kolb ,  Bryan C. Feisel ,  Martin Goetzinger ,  Philip S. Hall ,  Holger Hauptmann ,  Mark J. Hendrickson ,  Kathleen M. Humpal ,  John W. Longabach ,  James P. Mathers ,  Roberta R. Naujok ,  Paul D. Pennington ,  Gallus Schechner

IPC: A61K6/02 ,  C04B35/64 ,  C04B35/488 ,  C01G25/02 ,  A61K6/00 ,  A61C13/08 ,  C08J9/28 ,  A61C7/28 ,  A61C13/00 ,  A61C8/00 ,  C04B35/624 ,  A61K6/083 ,  C01G25/00 ,  C04B35/486 ,  B82Y30/00 ,  C08J9/00 ,  A61C5/77 ,  A61C5/20

CPC classification number: A61K6/024 ,  A61C5/20 ,  A61C5/77 ,  A61C7/282 ,  A61C8/0001 ,  A61C8/0012 ,  A61C8/0048 ,  A61C13/0006 ,  A61C13/0022 ,  A61C13/082 ,  A61K6/0002 ,  A61K6/0008 ,  A61K6/025 ,  A61K6/0255 ,  A61K6/083 ,  B82Y30/00 ,  C01G25/00 ,  C01G25/006 ,  C01G25/02 ,  C01P2002/50 ,  C01P2002/52 ,  C01P2002/60 ,  C01P2002/84 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/10 ,  C04B35/486 ,  C04B35/488 ,  C04B35/624 ,  C04B35/64 ,  C04B38/00 ,  C04B38/0045 ,  C04B2111/00836 ,  C04B2235/3217 ,  C04B2235/3225 ,  C04B2235/3227 ,  C04B2235/3244 ,  C04B2235/549 ,  C04B2235/6562 ,  C04B2235/6565 ,  C04B2235/6567 ,  C04B2235/661 ,  C04B2235/77 ,  C04B2235/781 ,  C04B2235/785 ,  C04B2235/80 ,  C04B2235/96 ,  C04B2235/9646 ,  C04B2235/9661 ,  C08J9/008 ,  C08J9/28 ,  C08J2201/038 ,  C08J2201/04 ,  C08J2201/0502 ,  C08J2203/08 ,  C08J2205/026 ,  C08J2205/042 ,  C08J2207/10 ,  C08J2333/02 ,  C08J2333/10 ,  C08J2333/14 ,  Y02P20/544 ,  C04B38/0054 ,  C04B38/0058 ,  C04B38/0074

Abstract: Aerogel, calcined articles, and crystalline articles comprising ZrO2. Exemplary uses of the crystalline metal oxide articles include dental articles (e.g., restoratives, replacements, inlays, onlays, veneers, full and partial crowns, bridges, implants, implant abutments, copings, anterior fillings, posterior fillings, and cavity liner, and bridge frameworks) and orthodontic appliances (e.g., brackets, buccal tubes, cleats, and buttons).

公开(公告)号：US09878954B2

公开(公告)日：2018-01-30

申请号：US14025958

申请日：2013-09-13

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Margaret M. Vogel-Martin ,  Martin B. Wolk ,  Michael Benton Free ,  Olester Benson, Jr. ,  Evan L. Schwartz ,  Robert F. Kamrath ,  Brant U. Kolb ,  Kathleen M. Humpal ,  Mark J. Hendrickson

IPC: E06B3/66 ,  C04B35/486 ,  E06B3/663 ,  C04B35/00

CPC classification number: C04B35/486 ,  C04B35/00 ,  C04B2235/3217 ,  C04B2235/3225 ,  C04B2235/3227 ,  E06B3/6612 ,  E06B3/66304 ,  Y02A30/25 ,  Y02B80/24 ,  Y10T428/24479 ,  Y10T428/24612 ,  Y10T428/252

Abstract: Vacuum insulated glass units having layered pillars. The glass units include two glass panes and an edge seal between the glass panes with a substantial vacuum gap between them. A plurality of pillars are located between the glass panes as spacers to maintain the vacuum gap. The pillars have a sintered ceramic, alpha alumina, or zirconia body with a tapered sidewall and a functional layer on a surface of the body.

公开(公告)号：US09592105B2

公开(公告)日：2017-03-14

申请号：US14418973

申请日：2013-08-01

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Holger Hauptmann ,  Sybille Schmittner ,  Gallus Schechner ,  Brant U. Kolb ,  Andreas Herrmann

IPC: A61C13/00 ,  C04B35/486 ,  C04B35/626 ,  C04B35/632 ,  C04B35/634 ,  C04B35/638 ,  C04B38/00 ,  B82Y30/00 ,  A61C5/10 ,  A61C7/00 ,  A61C8/00 ,  A61C13/01 ,  A61C13/08 ,  C04B35/48 ,  C04B111/00

CPC classification number: A61C13/0022 ,  A61C5/77 ,  A61C7/00 ,  A61C8/0001 ,  A61C8/005 ,  A61C13/0006 ,  A61C13/01 ,  A61C13/08 ,  B82Y30/00 ,  C04B35/48 ,  C04B35/486 ,  C04B35/6263 ,  C04B35/6269 ,  C04B35/632 ,  C04B35/63424 ,  C04B35/63488 ,  C04B35/638 ,  C04B38/0045 ,  C04B2111/00836 ,  C04B2235/3217 ,  C04B2235/3225 ,  C04B2235/3227 ,  C04B2235/3248 ,  C04B2235/449 ,  C04B2235/5409 ,  C04B2235/5454 ,  C04B2235/6023 ,  C04B2235/612 ,  C04B2235/6562 ,  C04B2235/6565 ,  C04B2235/6567 ,  C04B2235/781 ,  C04B2235/945 ,  C04B2235/95 ,  C04B2235/96 ,  F04C2270/041 ,  Y10T428/21 ,  Y10T428/24479 ,  Y10T428/2457

Abstract: The invention relates to a dental mill blank comprising a pre-sintered porous zirconia material, the porous pre-sintered zirconia material showing a N2 adsorption of isotherm type IV according to IUPAC classification, the porous pre-sintered zirconia material having a Vickers hardness from about 25 to about 150, the dental mill blank comprising means for reversible attaching it to a machining device. The invention also relates to a process of producing a zirconia dental article comprising the steps of providing a dental mill blank comprising a porous pre-sintered zirconia material, placing the dental mill blank in a machining device, machining the porous zirconia material and to a dental article obtained by such a process.

Abstract translation: 本发明涉及一种包括预烧结多孔氧化锆材料的多孔预烧结氧化锆材料的多孔预烧结氧化锆材料，根据IUPAC分类显示等温线型IV的N 2吸附，多孔预烧结氧化锆材料的维氏硬度约为 25至约150，牙科磨机坯料包括用于可逆地将其附接到加工装置的装置。 本发明还涉及一种生产氧化锆牙科制品的方法，其包括以下步骤：提供包括多孔预烧结氧化锆材料的牙科磨料坯料，将牙科磨料坯料放置在加工装置中，加工多孔氧化锆材料和牙科 通过这样一个过程获得的文章。

公开(公告)号：US09464179B2

公开(公告)日：2016-10-11

申请号：US14324313

申请日：2014-07-07

Applicant: 3M Innovative Properties Company

Inventor： William B. Kolb ,  Encai Hao ,  Brant U. Kolb ,  David L. Phillips

IPC: C08J9/36 ,  C08J9/28 ,  C08J9/00

CPC classification number: C08J9/286 ,  C08J9/0004 ,  C08J2201/0502 ,  C08J2205/042

Abstract: A process and apparatus for producing a nanovoided article, a nanovoided coating, and a low refractive index coating is described. The process includes providing a first solution of a polymerizable material in a solvent; at least partially polymerizing the polymerizable material to form a composition that includes an insoluble polymer matrix and a second solution, wherein the insoluble polymer matrix includes a plurality of nanovoids that are filled with the second solution; and removing a major portion of the solvent from the second solution. An apparatus for the process is also described, and includes a webline, a coating section, a partial polymerization section, and a solvent removal section.

Abstract translation: 描述了用于制备纳米复合制品，纳米复合涂层和低折射率涂层的方法和装置。 该方法包括在溶剂中提供可聚合材料的第一溶液; 至少部分地聚合所述可聚合材料以形成包含不溶性聚合物基质和第二溶液的组合物，其中所述不溶性聚合物基质包括填充有所述第二溶液的多个纳米泡; 并从第二溶液中除去大部分溶剂。 还描述了用于该方法的装置，并且包括纤维网，涂布部分，部分聚合部分和溶剂去除部分。

公开(公告)号：US10420207B2

公开(公告)日：2019-09-17

申请号：US15636264

申请日：2017-06-28

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Matthew H. Frey ,  Ta-Hua Yu ,  Kari A. McGee ,  Hui Luo ,  William B. Kolb ,  Brant U. Kolb ,  Moses M. David ,  Lijun Zu

IPC: B82Y99/00 ,  H05K1/09 ,  H05K1/02 ,  H05K9/00 ,  H05K3/06 ,  H05K3/46 ,  G06F3/041 ,  G02B1/116 ,  G02B27/14 ,  H05K1/03 ,  B82Y20/00 ,  B82Y30/00 ,  H03K17/96

Abstract: The present disclosure provides an article having a substrate having a first nanostructured surface and an opposing second surface; and a conductor micropattern disposed on the first surface of the substrate, the conductor micropattern formed by a plurality of traces. The micropattern may have an open area fraction greater than 80%. The traces of the conductor micropattern may have a specular reflectance in a direction orthogonal to and toward the first surface of the substrate of less than 50%. The nanostructured surface may include nanofeatures having a height from 50 to 750 nanometers, a width from 15 to 200 nanometers, and a lateral spacing from 5 to 500 nanometers. The articles are useful in devices such as displays, in particular, touch screen displays useful for mobile hand held devices, tablets and computers. They also find use in antennas and for EMI shields.

公开(公告)号：US20170233591A1

公开(公告)日：2017-08-17

申请号：US15502679

申请日：2015-08-19

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Naota Sugiyama ,  Kristy A. Gillette ,  Brant U. Kolb ,  Richard J. Pokorny

IPC: C09D7/12 ,  C09D4/00

CPC classification number: C09D7/62 ,  C08K3/36 ,  C08K9/06 ,  C08K2201/005 ,  C08K2201/011 ,  C09D4/00 ,  C09D7/67 ,  C08F230/08

Abstract: Hardcoat comprising a binder, and in a range from 15 to 95 volume % nanoparticles, wherein at least a portion of the nanoparticles are functionalized by free radical reactive silane and cyano group containing silane. Hardcoats described herein are useful, for example, on portable and non-portable information display articles (e.g., illuminated and non-illuminated display articles).

公开(公告)号：US09551816B2

公开(公告)日：2017-01-24

申请号：US15076149

申请日：2016-03-21

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： William D. Coggio ,  John S. Huizinga ,  Michael L. Steiner ,  Robert F. Watkins ,  Encai Hao ,  William B. Kolb ,  Peiwang Zhu ,  Michael Benton Free ,  Brant U. Kolb ,  Kui Chen-Ho ,  Paul E. Humpal ,  Scott M. Tapio ,  Kenneth L. Smith

IPC: G02B5/124 ,  G02B5/02

CPC classification number: G02B5/124 ,  G02B5/0236 ,  G02B5/0242 ,  G02B5/0247

Abstract: Retroreflecting optical constructions are disclosed. A disclosed retroreflecting optical construction includes a retroreflecting layer that has a retroreflecting structured major surface, and an optical film that is disposed on the retroreflecting structured major surface of the retroreflecting layer. The optical film has an optical haze that is not less than about 30%. Substantial portions of each two neighboring major surfaces in the retroreflecting optical construction are in physical contact with each other.

Abstract translation: 公开了反射光学结构。 公开的回射光学构造包括具有回射结构主表面的回射层和设置在回射层的回射结构化主表面上的光学膜。 光学膜的光学雾度不小于约30％。 回射光学结构中的每两个相邻主表面的实质部分彼此物理接触。

公开(公告)号：US20150157430A1

公开(公告)日：2015-06-11

申请号：US14418975

申请日：2013-03-08

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Holger Hauptmann ,  Andreas Herrmann ,  Brant U. Kolb

IPC: A61C13/08 ,  A61C5/10 ,  C04B35/48 ,  A61C7/12 ,  A61C13/083 ,  A61C13/00 ,  A61C13/01

CPC classification number: A61C13/082 ,  A61C5/77 ,  A61C7/12 ,  A61C8/0012 ,  A61C13/0003 ,  A61C13/0006 ,  A61C13/0022 ,  A61C13/01 ,  A61C13/083 ,  C04B35/48 ,  C04B35/486 ,  C04B35/624 ,  C04B38/0045 ,  C04B41/009 ,  C04B41/501 ,  C04B41/85 ,  C04B2111/00836 ,  C04B2235/3225 ,  C04B2235/3244 ,  C04B2235/449 ,  C04B2235/616 ,  C04B2235/6562 ,  C04B2235/6565 ,  C04B2235/6567 ,  C04B2235/661 ,  C04B2235/9653 ,  Y10T428/24997 ,  C04B41/4535 ,  C04B2103/0021 ,  C04B2103/0094

Abstract: The invention relates to kit of parts comprising a solution, a porous zirconia article, optionally application equipment, the solution comprising cation(s) of non-colouring agent(s) selected from ions of Y, Gd, La, Yb, Tm, Mg, Ca and mixtures thereof, solvent(s) for the ion(s), optionally complexing agent(s), optionally thickening agent(s), optionally organic marker substance(s), optionally additive(s), the porous zirconia article showing a N2 adsorption and/or desorption of isotherm type IV according to IUPAC classification. The invention also relates to a method for enhancing the translucency of a zirconia article comprising the steps of providing a porous zirconia article and a solution, applying the solution to at least a part of the outer surface of the porous zirconia article, optionally drying the porous zirconia article of the preceding step, sintering the porous zirconia article to obtain a zirconia ceramic article.

Abstract translation: 本发明涉及包含溶液，多孔氧化锆制品，任选应用设备的部件的试剂盒，所述溶液包含选自Y，Gd，La，Yb，Tm，Mg的离子的非着色剂的阳离子 ，Ca及其混合物，用于离子的溶剂，任选的络合剂，任选的增稠剂，任选的有机标记物质，任选的添加剂，所述多孔氧化锆制品显示 根据IUPAC分类，IV型等温线的N 2吸附和/或解吸附。 本发明还涉及一种用于增强氧化锆制品的半透明度的方法，包括以下步骤：提供多孔氧化锆制品和溶液，将溶液施加到多孔氧化锆制品的外表面的至少一部分上，任选地将多孔 氧化锆制品，烧结多孔氧化锆制品以获得氧化锆陶瓷制品。

公开(公告)号：US20150049384A1

公开(公告)日：2015-02-19

申请号：US13970260

申请日：2013-08-19

Applicant: 3M Innovative Properties Company

Inventor： William D. Coggio ,  John S Huizinga ,  Michael L. Steiner ,  Robert F. Watkins ,  Encai Hao ,  William B. Kolb ,  Peiwang Zhu ,  Michael B. Free ,  Brant U. Kolb ,  Kui Chen-Ho ,  Paul E. Humpal ,  Scott M. Tapio

IPC: G02B5/124

CPC classification number: G02B5/124 ,  G02B5/0236 ,  G02B5/0242 ,  G02B5/0247

Abstract: Retroreflecting optical constructions are disclosed. A disclosed retroreflecting optical construction includes a retroreflecting layer that has a retroreflecting structured major surface, and an optical film that is disposed on the retroreflecting structured major surface of the retroreflecting layer. The optical film has an optical haze that is not less than about 30%. Substantial portions of each two neighboring major surfaces in the retroreflecting optical construction are in physical contact with each other.

Abstract translation: 公开了反射光学结构。 公开的回射光学构造包括具有回射结构主表面的回射层和设置在回射层的回射结构化主表面上的光学膜。 光学膜的光学雾度不小于约30％。 回射光学结构中的每两个相邻主表面的实质部分彼此物理接触。

公开(公告)号：US20140135206A1

公开(公告)日：2014-05-15

申请号：US14122095

申请日：2012-05-23

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Neeraj Sharma ,  Brant U. Kolb ,  Mark J. Hendrickson

IPC: C07F7/22

CPC classification number: C07F7/2224 ,  B82Y30/00 ,  C01G19/02 ,  C01P2002/50 ,  C01P2004/64 ,  C08K9/04 ,  C09C1/00

Abstract: Plurality of crystalline, surface modified tin oxide nanoparticles, wherein the particles have a largest dimension up to 20 nm, and wherein the surface modifier comprises at least one of an organic carboxylic acid or anion thereof, including a dispersion comprising the crystalline, surface modified tin oxide nanoparticles and methods to make the same. The crystalline surface modified doped tin oxide nanoparticles are useful, for example, for preparing transparent electrodes, heat mirrors and energy storage devices.

Abstract translation: 多种结晶，表面改性的氧化锡纳米颗粒，其中颗粒具有最大20nm的最大尺寸，并且其中表面改性剂包括有机羧酸或其阴离子中的至少一种，包括含有结晶表面改性锡 氧化物纳米粒子和使之相同的方法。 结晶表面改性掺杂的氧化锡纳米颗粒例如用于制备透明电极，加热镜和储能装置是有用的。