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    Synthesis and use of MSE-framework type molecular sieves
    32.
    发明授权
    Synthesis and use of MSE-framework type molecular sieves 有权
    合成和使用MSE-框架型分子筛

    公开(公告)号：US08025863B2

    公开(公告)日：2011-09-27

    申请号：US12214631

    申请日：2008-06-20

    申请人： Karl G. Strohmaier ,  Simon C. Weston ,  James C. Vartuli ,  J. Thomas Ippoliti

    发明人： Karl G. Strohmaier ,  Simon C. Weston ,  James C. Vartuli ,  J. Thomas Ippoliti

    IPC分类号： C01B39/04 ,  C01B39/48

    CPC分类号： C07D295/023 ,  C01B37/02 ,  C01B39/48

    摘要： A method of synthesizing a crystalline molecular sieve having an MSE framework type comprises crystallizing a reaction mixture comprising a source of water, a source of an oxide of a tetravalent element, Y, selected from at least one of silicon, tin, titanium, vanadium and germanium, a source of an alkali or alkaline earth metal, M, and a source of organic cations, Q, having the following general structure: in which R1 is hydrogen or an alkyl group, and R2 and R3 are alkyl groups.

    摘要翻译： 合成具有MSE骨架类型的结晶分子筛的方法包括将包含水源，四价元素的氧化物源Y的反应混合物结晶，Y选自硅，锡，钛，钒和 锗，碱金属或碱土金属的源，M和有机阳离子源Q，具有以下一般结构：其中R1是氢或烷基，R2和R3是烷基。

    Thermally stable, high surface area, modified mesoporous aluminophosphate material
    35.
    发明授权
    Thermally stable, high surface area, modified mesoporous aluminophosphate material 有权
    热稳定，高表面积，改性介​​孔磷酸铝材料

    公开(公告)号：US06447741B1

    公开(公告)日：2002-09-10

    申请号：US09468451

    申请日：1999-12-21

    申请人： Arthur W. Chester ,  Frederick E. Daugherty ,  Charles T. Kresge ,  Hye-Kyung C. Timken ,  James C. Vartuli

    发明人： Arthur W. Chester ,  Frederick E. Daugherty ,  Charles T. Kresge ,  Hye-Kyung C. Timken ,  James C. Vartuli

    IPC分类号： C01B2536

    CPC分类号： B01J35/1061 ,  B01J27/16 ,  B01J27/1804 ,  B01J27/1853 ,  B01J27/187 ,  B01J29/084 ,  B01J35/0006 ,  B01J35/10 ,  B01J35/1019 ,  B01J35/108 ,  B01J37/03 ,  B01J2229/42 ,  C10G11/02 ,  C10G2400/02 ,  Y10S423/30

    摘要： A mesoporous aluminophosphate material includes a solid aluminophosphate composition modified with at least one element selected from zirconium, cerium, lanthanum, manganese, cobalt, zinc, and vanadium. This mesoporous aluminophosphate material has a specific surface area of at least 100 m2/g, an average pore size less than or equal to 100 Å, and a pore size distribution such that at least 50% of the pores have a pore diameter less than 100 Å. The material can be used as a support for a catalytic cracking catalyst. Additionally, a method for making such a mesoporous aluminophosphate material is disclosed. The method, which preferably avoids use of organic reagents or solvents, includes providing an aqueous solution containing an inorganic phosphorus component; an inorganic aluminum containing component; and an inorganic modifying component containing at least one element selected from zirconium, cerium, lanthanum, manganese, cobalt, zinc, and vanadium. A solid mesoporous aluminophosphate material is formed in the solution by adjusting the pH of the solution to the range of 7 to 12 and is then recovered.

    摘要翻译： 介孔磷酸铝材料包括用至少一种选自锆，铈，镧，锰，钴，锌和钒的元素改性的固体磷酸铝组合物。 该介孔磷酸铝材料的比表面积为至少100m 2 / g，平均孔径小于或等于100，孔径分布使孔至少50％的孔径小于100 一个。 该材料可用作催化裂化催化剂的载体。 另外，公开了制造这种中孔磷酸铝材料的方法。 优选避免使用有机试剂或溶剂的方法包括提供含有无机磷组分的水溶液; 无机含铝组分; 和含有选自锆，铈，镧，锰，钴，锌和钒中的至少一种元素的无机改性成分。 通过将溶液的pH调节至7至12的范围，在溶液中形成固体介孔磷酸铝材料，然后回收。