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    Method of charging a sorption store with a gas
    42.
    发明授权
    Method of charging a sorption store with a gas 有权
    用气体对吸附物料充电的方法

    公开(公告)号：US09322510B2

    公开(公告)日：2016-04-26

    申请号：US14048358

    申请日：2013-10-08

    Applicant: BASF SE

    Inventor： Mathias Weickert ,  Stefan Marx ,  Ulrich Müller ,  Peter Renze

    IPC: F17C11/00

    CPC classification number: F17C11/005 ,  F17C11/00 ,  F17C11/007

    Abstract: Described is a method of charging a sorption store with a gas. The sorption store comprises a closed container and a feed device which has a passage through the container wall, through which the gas can flow into the container, and the container has at least two parallel, channel-shaped subchambers which are located in its interior and are each at least partly filled with an adsorption medium and whose channel walls are coolable. The method comprises, in a first step, feeding in a gas in such an amount that a pressure in the store of at least 30% of a predetermined final pressure is reached as quickly as possible and, in a second step, subsequently varying the amount of gas fed in in such a way that the course of the pressure in the store approximates the adsorption kinetics of the adsorption medium until the predetermined final pressure in the store is reached after a predetermined period of time.

    Abstract translation: 描述了一种用气体对吸附物料进行充电的方法。 吸附储存器包括密封容器和进料装置，其具有通过容器壁的通道，气体可以通过该通道流入容器中，并且容器具有位于其内部的至少两个平行的通道形子室， 各自至少部分地填充有吸附介质，并且其通道壁是可冷却的。 该方法包括在第一步骤中，将气体供给量使得储存器中的压力达到尽可能快的至少30％的预定最终压力，并且在第二步骤中随后改变量 以这样的方式供给气体，使得商店中的压力过程接近吸附介质的吸附动力学，直到在预定时间段之后达到储存器中的预定最终压力。

    CATALYTICALLY ACTIVE BODY FOR THE SYNTHESIS OF DIMETHYL ETHER FROM SYNTHESIS GAS
    43.
    发明申请
    CATALYTICALLY ACTIVE BODY FOR THE SYNTHESIS OF DIMETHYL ETHER FROM SYNTHESIS GAS 审中-公开
    合成气体合成二甲醚的催化活性体

    公开(公告)号：US20150105479A1

    公开(公告)日：2015-04-16

    申请号：US14396396

    申请日：2013-04-15

    Applicant: BASF SE

    Inventor： Alexander Schäfer ,  Mathias Feyen ,  Andrei-Nicolae Parvulescu ,  Ulrich Müller ,  Bernd Bastian Schaack

    IPC: B01J29/76 ,  C07C41/09 ,  B01J29/46

    CPC classification number: B01J29/76 ,  B01J23/80 ,  B01J29/06 ,  B01J29/40 ,  B01J29/46 ,  C07C41/01 ,  C07C41/09 ,  C07C43/043

    Abstract: The invention relates to a catalytically active body for the synthesis of dimethyl ether from synthesis gas. In particular, the invention relates to an improved catalytically active body for the synthesis of dimethyl ether, whereby the components of the active body comprise a methanol active component and an acid component comprising a zeolitic material being crystallized by means of one or more alkenyltrialkylammonium cation R1R2R3R4N+-containing compounds as structure directing agent. Furthermore, the present invention concerns a method for the preparation of a catalytically active body, the use of the catalytically active body and a method for the preparation of dimethyl ether from synthesis gas.

    Abstract translation: 本发明涉及用于从合成气合成二甲醚的催化活性体。 特别地，本发明涉及用于合成二甲醚的改进的催化活性体，其中活性体的组分包含甲醇活性组分和酸组分，该组分包含通过一个或多个烯基三烷基铵阳离子R1R2R3R4N +结晶的沸石材料， 作为结构导向剂的化合物。 此外，本发明涉及制备催化活性体的方法，催化活性体的用途以及从合成气中制备二甲醚的方法。

    Process for the Conversion of Oxygenates to Olefins
    44.
    发明申请
    Process for the Conversion of Oxygenates to Olefins 有权
    将氧化物转化为烯烃的方法

    公开(公告)号：US20140142361A1

    公开(公告)日：2014-05-22

    申请号：US14076723

    申请日：2013-11-11

    Applicant: BASF SE

    Inventor： Manuela Gaab ,  Ulrich Müller ,  Milan Kostur ,  Kirsten Spannhoff ,  Kerem Bay ,  Andrei-Nicolae Parvulescu

    IPC: C07C1/22

    CPC classification number: C07C1/20 ,  C07C2529/40 ,  C07C11/02

    Abstract: The present invention relates to a process for the conversion of oxygenates to olefins comprising (i) providing a gas stream comprising one or more oxygenates; and (ii) contacting the gas stream with a catalyst; wherein the catalyst comprises a zeolitic material having an MFI, MEL, and/or MWW-type framework structure comprising YO2 and X2O3, wherein Y is a tetravalent element, and X is a trivalent element, said zeolitic material being obtainable and/or obtained according to a method comprising (1) preparing a mixture comprising one or more sources for YO2, one or more sources for X2O3, and one or more solvents; and (2) crystallizing the mixture obtained in step (1) to obtain a zeolitic material having an MFI, MEL and/or MWW-type framework structure; wherein the mixture crystallized in step (2) contains 3 wt.-% or less of the one or more elements M based on 100 wt.-% of YO2, wherein M stands for sodium.

    Abstract translation: 本发明涉及一种将含氧化合物转化为烯烃的方法，包括（i）提供包含一种或多种含氧化合物的气流; 和（ii）使气流与催化剂接触; 其中所述催化剂包含具有包含YO 2和X 2 O 3的MFI，MEL和/或MWW型骨架结构的沸石材料，其中Y是四价元素，X是三价元素，所述沸石材料可根据 涉及一种方法，包括（1）制备包含一种或多种YO源的混合物，一种或多种X 2 O 3源和一种或多种溶剂的混合物; 和（2）使步骤（1）中获得的混合物结晶，得到具有MFI，MEL和/或MWW型骨架结构的沸石材料; 其中在步骤（2）中结晶的混合物含有基于100重量％的YO 2的一种或多种元素M的3重量％或更少，其中M代表钠。

    Catalyst for the Conversion of Syngas to Olefins and Preparation Thereof
    45.
    发明申请
    Catalyst for the Conversion of Syngas to Olefins and Preparation Thereof 审中-公开
    合成气转化为烯烃及其制备的催化剂

    公开(公告)号：US20140113981A1

    公开(公告)日：2014-04-24

    申请号：US14056002

    申请日：2013-10-17

    Applicant: BASF SE

    Inventor： Bilge Yilmaz ,  Ulrich Müller ,  Xinhe Bao ,  Weiping Zhang ,  Dirk de Vos ,  Takashi Tatsumi ,  Feng-Shou Xiao ,  Hermann Gies ,  Hiroyuki Imai

    IPC: C07C1/04 ,  B01J29/76

    CPC classification number: C07C1/044 ,  B01J29/76 ,  B01J29/89 ,  B01J35/1019 ,  B01J35/1028 ,  B01J35/1038 ,  B01J35/1042 ,  B01J2229/186 ,  C10G25/003 ,  C10G25/03

    Abstract: Described is a process for the production of a pillared silicate. The process comprises (i) providing a layered silicate; (ii) interlayer expanding the layered silicate provided in step (i) comprising a step of treating the layered silicate with one or more swelling agents; (iii) treating the interlayer expanded silicate obtained in step (ii) with one or more hydrolyzable silicon containing compounds; (iv) treating the interlayer expanded compound obtained in step (iii) with an aqueous solution to obtain a pillared silicate; (v) removing at least a portion of the one or more swelling agents from the pillared silicate obtained in step (iv); and (vi) impregnating the pillared silicate obtained in step (v) with one or more elements selected from the group consisting of Fe, Ru, Ir, and combinations of two or more thereof. Also described is a pillared silicate optionally obtainable from said process and its use, in particular, in a process for the production of one or more olefins according to the invention.

    Abstract translation: 描述了生产柱状硅酸盐的方法。 该方法包括（i）提供层状硅酸盐; （ii）层间膨胀步骤（i）中提供的层状硅酸盐，包括用一种或多种溶胀剂处理层状硅酸盐的步骤; （iii）用一种或多种可水解含硅化合物处理在步骤（ii）中获得的层间发泡硅酸盐; （iv）用水溶液处理步骤（iii）中得到的层间发泡化合物，得到柱状硅酸盐; （v）从步骤（iv）中获得的柱状硅酸盐中去除至少一部分一种或多种溶胀剂; 和（vi）用步骤（v）中获得的柱状硅酸盐浸渍一种或多种选自Fe，Ru，Ir的元素，以及两种或更多种的组合。 还描述了可任意地从所述方法获得的柱状硅酸盐及其用途，特别是用于生产根据本发明的一种或多种烯烃的方法。

    Sorption Store for Storing Gaseous Substances
    46.
    发明申请
    Sorption Store for Storing Gaseous Substances 有权
    用于储存气态物质的吸附库

    公开(公告)号：US20140097099A1

    公开(公告)日：2014-04-10

    申请号：US14048231

    申请日：2013-10-08

    Applicant: BASF SE

    Inventor： Mathias Weickert ,  Stefan Marx ,  Ulrich Müller ,  Peter Renze

    IPC: F17C11/00 ,  F17C13/00

    CPC classification number: F17C11/007 ,  F17C11/00 ,  F17C13/005

    Abstract: Describes is a sorption store for storing gaseous substances. The sorption store for storing gaseous substances comprises a closed tank and a feeding device, which comprises a passage through the tank wall, through which a gas can flow into the tank. The tank has inside it at least one separating element, which is configured in such a way that the interior of the tank is divided into at least one pair of channels comprising two parallel running channel-shaped compartments, the ends of which are in connection with one another in each case by way of a common space, each channel-shaped compartment being filled at least partially with an adsorption medium. The feeding device is designed in such a way that inflowing gas is diverted almost exclusively into one of the two compartments of each pair of channels.

    Abstract translation: 描述是用于储存气态物质的吸附存储。 用于储存气态物质的吸附存储器包括封闭的罐和进料装置，其包括通过罐壁的通道，气体可以通过该通道流入罐中。 该罐内有至少一个分离元件，其被构造成使得罐的内部被分成至少一对通道，其包括两个平行的行进的通道形隔室，其两端与 在每种情况下通过公共空间彼此相互隔开，每个通道形隔室至少部分地被吸附介质填充。 进料装置设计成使得流入的气体几乎完全转移到每对通道的两个隔室中的一个中。

    Organotemplate-free solid-state synthetic method for zeolite molecular sieves
    49.
    发明授权
    Organotemplate-free solid-state synthetic method for zeolite molecular sieves 有权

    公开(公告)号：US10160656B2

    公开(公告)日：2018-12-25

    申请号：US14649637

    申请日：2013-12-05

    Applicant: BASF SE

    Inventor： Stefan Maurer ,  Ulrich Müller ,  Feng-Shou Xiao ,  Xiangju Meng ,  Qinming Wu

    IPC: C01B39/46 ,  C01B39/02 ,  C01B39/38 ,  C01B39/20 ,  C01B39/26 ,  B01J29/08 ,  B01J29/18 ,  B01J29/70 ,  B01J35/00 ,  B01J35/10 ,  B01J29/40 ,  B01J37/00 ,  B01J37/04 ,  C01B39/14

    Abstract: Described is a preparation method for zeolite molecular sieves by means of solid-state reactions without the usage of organic templates. The method comprises the following steps: grinding and mixing the solid raw materials comprising the silicon source, the aluminum source and the alkali source, transferring the obtained mixture into an autoclave, conducting the crystallization for a period of 5 hours-20 days at a temperature of 50-200° C. After filtering and drying the crystallized products, molecular sieves in a powder form can be obtained. The method provides different molecular sieves, including ZSM-5 zeolite, Beta zeolite, FAU zeolite, MOR zeolite, LTA zeolite, and GIS zeolite, with a high crystallinity and an adjustable Si/Al ratio within a certain range. The obtained products exhibit a high crystallinity and a high purity, and the method does not require the use of organic templates and solvents, which avoids unnecessary consumptions during the production, simplifies the synthetic process, and also increases the yield from the autoclave reactor.

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