公开(公告)号：US20150135603A1

公开(公告)日：2015-05-21

申请号：US14407959

申请日：2013-06-14

Applicant: Element Six Abrasives S.A.

Inventor： Nedret Can ,  Kaveshini Naidoo

IPC: E21B10/46 ,  B32B18/00 ,  C22C26/00 ,  B01J3/06

CPC classification number: E21B10/46 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/0615 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/068 ,  B01J2203/0685 ,  B22F2005/001 ,  B32B18/00 ,  B32B2307/554 ,  B32B2307/704 ,  B82Y30/00 ,  C01B32/25 ,  C04B35/52 ,  C04B35/6261 ,  C04B35/62655 ,  C04B35/6303 ,  C04B35/645 ,  C04B37/021 ,  C04B2235/3813 ,  C04B2235/3839 ,  C04B2235/3843 ,  C04B2235/424 ,  C04B2235/425 ,  C04B2235/427 ,  C04B2235/5436 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/5472 ,  C04B2235/96 ,  C04B2235/9607 ,  C04B2237/588 ,  C04B2237/704 ,  C22C26/00 ,  C22C2026/005 ,  C22C2026/006 ,  E21B10/573

Abstract: A polycrystalline diamond structure comprises a first region and a second region adjacent the first region, the second region being bonded to the first region by intergrowth of diamond grains. The first region comprises a plurality of alternating strata or layers (21), (22), each or one or more strata or layers in the first region having a thickness in the range of around 5 to 300 microns. The polycrystalline diamond (PCD) structure has a diamond content of at most about 95 percent of the volume of the PCD material, a binder content of at least about 5 percent of the volume of the PCD material, and one or more of the layers or strata in the first region comprise and/or the second region comprises diamond grains having a mean diamond grain contiguity of greater than about 60 percent and a standard deviation of less than about 2.2 percent. There is also disclosed a method of making such a poly crystalline diamond structure.

Abstract translation: 多晶金刚石结构包括第一区域和与第一区域相邻的第二区域，第二区域通过金刚石晶粒的共生结合到第一区域。 第一区域包括多个交替的层或层（21），（22），第一区域中的每个或一个或多个层或层具有在约5至300微米范围内的厚度。 多晶金刚石（PCD）结构的金刚石含量至多为PCD材料体积的约95％，粘合剂含量为PCD材料体积的至少约5％，以及一个或多个层或 第一区域中的层包含和/或第二区域包括具有大于约60％的平均金刚石颗粒接触度和小于约2.2％的标准偏差的金刚石晶粒。 还公开了制造这种多晶金刚石结构的方法。

公开(公告)号：US09028573B2

公开(公告)日：2015-05-12

申请号：US13820744

申请日：2011-09-08

Applicant: Yahua Bao ,  Scott Horman ,  Xian Yao ,  Qingyuan Liu

Inventor： Yahua Bao ,  Scott Horman ,  Xian Yao ,  Qingyuan Liu

IPC: B24D3/02 ,  B24D3/06 ,  B01J3/06 ,  C04B35/645 ,  C04B35/5831 ,  B23H7/02 ,  C04B35/63

CPC classification number: B24D3/06 ,  B01J3/062 ,  B01J2203/066 ,  B23B2222/14 ,  B23B2222/41 ,  B23B2226/125 ,  B23H7/02 ,  C04B35/5831 ,  C04B35/6303 ,  C04B35/645 ,  C04B2235/3217 ,  C04B2235/3813 ,  C04B2235/3817 ,  C04B2235/3843 ,  C04B2235/3847 ,  C04B2235/3856 ,  C04B2235/3865 ,  C04B2235/3886 ,  C04B2235/5436 ,  C04B2235/5445 ,  C04B2235/5463 ,  C04B2235/723 ,  C04B2235/80 ,  C04B2235/95

Abstract: The present disclosure relates to cubic boron nitride (cBN) cutting elements that have high cBN content and that are cuttable by electric discharge machining (EDM). A cutting element according to an embodiment includes a self-sintered polycrystalline cubic boron nitride (PCBN) compact, having a first phase of cubic boron nitride (cBN) particles and a ceramic binder phase with titanium compounds. The first phase occupies greater than 80% by volume of the self-sintered PCBN compact. The self-sintered PCBN compact has an electrical conductivity sufficient to be cuttable by electrical discharge machining.

Abstract translation: 本公开涉及具有高cBN含量并且可通过放电加工（EDM）切割的立方氮化硼（cBN）切割元件。 根据实施例的切割元件包括具有立方氮化硼（cBN）颗粒的第一相和具有钛化合物的陶瓷粘结相的自烧结多晶立方氮化硼（PCBN）压块。 第一相占据自烧结PCBN压块的80体积％以上。 自烧结PCBN压块具有足以通过放电加工切割的电导率。

公开(公告)号：US09022750B2

公开(公告)日：2015-05-05

申请号：US13729699

申请日：2012-12-28

Applicant: Mauricio Eduardo Mulet Martinez

Inventor： Mauricio Eduardo Mulet Martinez

IPC: F04B17/00 ,  F04B35/00 ,  F04B1/02 ,  B01J3/06 ,  B30B11/00 ,  F04B3/00 ,  F04B25/00 ,  F04B37/12

CPC classification number: F04B1/02 ,  B01J3/065 ,  B01J3/067 ,  B01J2203/0655 ,  B01J2203/068 ,  B01J2203/0685 ,  B30B11/004 ,  F04B3/00 ,  F04B25/00 ,  F04B37/12

Abstract: A multichamber pressure-increasing device is comprised of a plurality of chambers disposed in series one inside the other, wherein the innermost chamber is configured so as to place objects or samples therein to subject them to ultra-high pressures. An external hydraulic pump pumps fluid into the outermost chamber while a plurality of elemental hydraulic motor pump systems (EHMPS) are mounted in each chamber for increasing the pressure from one chamber to the next one disposed more to the interior of the device through an iterative process, each EHMPS consisting of two cylinder-piston assemblies operatively joined together in such a way that both pistons extend or retract simultaneously within their respective cylinders, the motor part driving the pump part as pressurized fluid admitted into the motor cylinder is subsequently discharged so fluid admitted into the pumping part cylinder is compressed therein and impelled at a higher pressure into the succeeding chamber.

Abstract translation: 多室增压装置由多个室内组成的多个室组成，其中最内室被配置为将物体或样品放置在其中以使其达到超高压。 外部液压泵将流体泵送到最外室中，而在每个室中安装多个元件液压马达泵系统（EHMPS），用于通过迭代过程增加从一个室到另一个更多设置在装置内部的压力 每个EHMPS由两个气缸活塞组件组成，两个气缸 - 活塞组件以两个活塞在其各自的气缸内同时延伸或缩回的方式可操作地接合在一起，驱动泵部件的电动机部件随后进入电动机气缸的加压流体随后被排出，从而使流体进入 泵送部分气缸被压缩并且在更高的压力下推动到随后的室中。

公开(公告)号：US08968436B2

公开(公告)日：2015-03-03

申请号：US13330805

申请日：2011-12-20

Applicant: Abhijit Prabhakar Suryavanshi

Inventor： Abhijit Prabhakar Suryavanshi

IPC: B24D18/00 ,  C22C26/00 ,  B22F5/00 ,  B22F7/06 ,  B24D99/00 ,  E21B10/567 ,  E21B10/573 ,  B01J3/06

CPC classification number: B24D3/06 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0655 ,  B01J2203/0685 ,  B22F5/00 ,  B22F7/06 ,  B24D18/0009 ,  B24D99/005 ,  C22C26/00 ,  E21B10/567 ,  E21B10/573

Abstract: A cutting element include a substrate and a diamond compact including at least two polycrystalline diamond portions separated by at least one metal carbide foil portion. The cutting element is made by placing diamond powder in a reaction container, placing a thin metal layer in the reaction container above or around the diamond powder and binder, placing additional diamond powder in the reaction container above or around the thin metal layer, and placing a pre-sintered substrate containing binder into the reaction container above all diamond powder and thin metal layer components. The assembled reaction container is put into a reactor and is subjected to a high-temperature high-pressure sintering process. The binder in the pre-sintered substrate sweeps through to sinter the first diamond portion, and then reacts with the thin metal layer to form a metal carbide, and then the binder continues to sweep through to sinter the second diamond portion.

Abstract translation: 切割元件包括基底和金刚石致密体，其包括由至少一个金属碳化物箔部分分开的至少两个多晶金刚石部分。 切割元件通过将金刚石粉末放置在反应容器中，将金属薄层放置在金刚石粉末和粘合剂上方或周围的反应容器中，在金属层上方或周围将反应容器中的另外的金刚石粉末放置在反应容器中， 将包含粘合剂的预烧结基材置于反应容器中，高于所有金刚石粉末和薄金属层组分。 将组装的反应容器放入反应器中并进行高温高压烧结工艺。 预烧结衬底中的粘合剂扫过以烧结第一金刚石部分，然后与薄金属层反应形成金属碳化物，然后粘合剂继续扫过以烧结第二金刚石部分。

公开(公告)号：US08936659B2

公开(公告)日：2015-01-20

申请号：US13275872

申请日：2011-10-18

Applicant: Soma Chakraborty ,  Gaurav Agrawal ,  Anthony A. DiGiovanni

Inventor： Soma Chakraborty ,  Gaurav Agrawal ,  Anthony A. DiGiovanni

IPC: C09K3/14 ,  B01J3/06 ,  B82Y30/00 ,  B24D99/00

CPC classification number: C09K3/1436 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685 ,  B24D99/005 ,  B82Y30/00 ,  C01B32/28 ,  Y10T428/2982

Abstract: A substance includes diamond particles having a maximum linear dimension of less than about 1 μm and an organic compound attached to surfaces of the diamond particles. The organic compound may include a surfactant or a polymer. A method of forming a substance includes exposing diamond particles to an organic compound, and exposing the diamond particles in the presence of the organic compound to ultrasonic energy. The diamond particles may have a maximum linear dimension of less than about 1 μm. A composition includes a liquid, a plurality of diamond nanoparticles dispersed within the liquid, and an organic compound attached to surfaces of the diamond nanoparticles. A method includes mixing a plurality of diamond particles with a solution comprising a liquid solvent and an organic compound, and exposing the mixture including the plurality of diamond nanoparticles and the solution to ultrasonic energy.

Abstract translation: 物质包括具有小于约1μm的最大线性尺寸的金刚石颗粒和附着到金刚石颗粒表面的有机化合物。 有机化合物可以包括表面活性剂或聚合物。 形成物质的方法包括将金刚石颗粒暴露于有机化合物，并将有机化合物存在下的金刚石颗粒暴露于超声波能量。 金刚石颗粒可以具有小于约1μm的最大线性尺寸。 组合物包括液体，分散在液体内的多个金刚石纳米颗粒和附着到金刚石纳米颗粒表面的有机化合物。 一种方法包括将多个金刚石颗粒与包含液体溶剂和有机化合物的溶液混合，并将包括多个金刚石纳米颗粒和溶液的混合物暴露于超声波能量。

公开(公告)号：US08920706B2

公开(公告)日：2014-12-30

申请号：US13238173

申请日：2011-09-21

Applicant: Yang-Kuao Kuo ,  Chia-Yi Hsiang ,  Ching-Hui ChiangLin ,  Fu-Hsing Huang

Inventor： Yang-Kuao Kuo ,  Chia-Yi Hsiang ,  Ching-Hui ChiangLin ,  Fu-Hsing Huang

IPC: C04B35/645 ,  C04B35/581 ,  B01J3/06 ,  B22F3/15

CPC classification number: B01J3/06 ,  B01J2203/067 ,  B22F2003/153 ,  C04B35/581 ,  C04B35/6455 ,  C04B2235/658

Abstract: Disclosed is a method for hot isostatic pressing a substrate. At first, a metal container is provided. Powder is filled in the metal container before the metal container is located in an oven. The metal container is subjected to isostatic pressing that includes heating and pressing. Thus, the metal container shrinks and presses on the powder evenly and turns the powder into a nugget. The metal container is moved out of the oven and broken to release the nugget. A substrate is cut from the nugget. With the hot isostatic pressing, the substrate exhibits only a few flaws and is large, fine, homogenous and strong so that the substrate is not vulnerable to deformation in a high-pressure environment.

Abstract translation: 公开了一种用于热等静压基板的方法。 首先，提供金属容器。 在金属容器位于烤箱中之前，将粉末填充在金属容器中。 对金属容器进行包括加热和压制在内的等静压。 因此，金属容器收缩并均匀地压在粉末上，并将粉末变成熔核。 将金属容器从烘箱中移出并破碎以释放熔核。 从熔核切割基材。 通过热等静压，基板只有少量缺陷，大而细，均匀而坚固，因此基板在高压环境下不易变形。

公开(公告)号：US08747798B2

公开(公告)日：2014-06-10

申请号：US13517921

申请日：2011-08-10

Applicant: Hitoshi Sumiya ,  Katsuko Yamamoto ,  Takeshi Sato ,  Keiko Arimoto

Inventor： Hitoshi Sumiya ,  Katsuko Yamamoto ,  Takeshi Sato ,  Keiko Arimoto

IPC: B01J3/06 ,  B26D3/08 ,  B31B1/25 ,  B26D11/00 ,  B24B21/18 ,  B23F21/03 ,  B21C3/00 ,  B23H7/00 ,  A62C31/02 ,  B32B7/02 ,  G11B5/64

Abstract: Polycrystalline diamond includes cubic diamond and hexagonal diamond, and a ratio of X-ray diffraction peak intensity of a (100) plane of the hexagonal diamond to X-ray diffraction peak intensity for a (111) plane of cubic diamond is not lower than 0.01%. In addition, a present method of manufacturing polycrystalline diamond includes the steps of preparing a non-diamond carbon material having a degree of graphitization not higher than 0.58 and directly converting the non-diamond carbon material to cubic diamond and hexagonal diamond and sintering the non-diamond carbon material, without adding any of a sintering agent and a binder, under pressure and temperature conditions at which diamond is thermodynamically stable.

公开(公告)号：US08728429B2

公开(公告)日：2014-05-20

申请号：US12820230

申请日：2010-06-22

Applicant: Olga Shenderova

Inventor： Olga Shenderova

IPC: B01J3/06 ,  B01J19/08 ,  E21C37/00 ,  B22F3/08 ,  B82Y40/00 ,  B82Y5/00 ,  B82Y30/00 ,  B82Y15/00

CPC classification number: B82Y40/00 ,  B82Y5/00 ,  B82Y15/00 ,  B82Y30/00 ,  C01B32/25 ,  Y10S977/70 ,  Y10S977/734 ,  Y10S977/773 ,  Y10S977/775

Abstract: In certain implementations, a method of manufacturing electrically conductive nanodiamond particles involves providing at least one type of carbon-containing explosive material and at least one type of non-explosive material; wherein the non-explosive material contains at least one or more than one element or species other than nitrogen that serve as a nanodiamond dopant; mixing the carbon containing explosive material with the non-explosive material; detonating the mixture under conditions of negative oxygen balance in the presence of a cooling medium; purifying the product of detonation from incombustible impurities; and carrying out additional processing for activation or enhancement of electrical conductance. This abstract is not to be considered limiting, since other embodiments may deviate from the features described in this abstract.

Abstract translation: 在某些实施方案中，制造导电纳米金刚石颗粒的方法包括提供至少一种类型的含碳爆炸材料和至少一种类型的非爆炸材料; 其中所述非爆炸材料包含用作纳米金刚石掺杂剂的除了氮之外的至少一种或多种元素或物质; 将含碳的炸药与非爆炸性材料混合; 在存在冷却介质的情况下，在负氧平衡的条件下引爆混合物; 净化爆炸产物不可燃杂质; 并执行用于激活或增强电导的附加处理。 该摘要不被认为是限制性的，因为其他实施例可能偏离本摘要中描述的特征。

公开(公告)号：US08506919B2

公开(公告)日：2013-08-13

申请号：US11813738

申请日：2006-01-01

Applicant: Nobuyuki Saito ,  Hisao Shirasawa ,  Hiroshi Yamanaka ,  Hiroshi Ishizuka

Inventor： Nobuyuki Saito ,  Hisao Shirasawa ,  Hiroshi Yamanaka ,  Hiroshi Ishizuka

IPC: B01J3/06 ,  A01K43/04 ,  C22B11/10 ,  B03B11/00

CPC classification number: C30B29/04 ,  B01D21/02 ,  B82Y30/00 ,  C01B32/28 ,  C01P2004/64 ,  C09K3/1409 ,  C30B29/605

Abstract: An object of this invention is to provide a fine powder of diamond particles of less than 50 nm with a narrow particle size range. The diamond is single crystalline and characterized with a lot of sharp edges and sharp points. Another object is to provide a method for efficiently producing such fine powder.The method comprises mechanically crushing a raw material of single crystalline diamond particles to prepare starting minute particles of diamond, then imparting hydrophilic quality to the surface of diamond particles. As hydrophilic the diamond particles are dispersed in water to form a slurry, which is set and kept weakly alkaline. The slurry is then subjected to a preliminary grading step, whereby the slurry is removed of a top particle size fraction of the diamond particles that has a D50 size of 60 nm or more. Eliminated of said top particle size fraction, the slurry is then diluted with water to regulate the diamond concentration to 0.1% (by weight) or less. The slurry so conditioned is subjected to a centrifugal force, whereby a coarser particle size fraction of the diamond particles is condensed to a solid cake and removed from the slurry. Effluent slurry is taken out from the centrifugal grading that contains a fraction of the diamond particles having decreased particle sizes.

Abstract translation: 本发明的目的是提供具有窄的粒度范围的小于50nm的金刚石颗粒的细粉末。 钻石是单晶的，其特征是具有很多锋利的边缘和尖锐的点。 另一个目的是提供一种有效生产这种细粉的方法。 该方法包括机械破碎单晶金刚石颗粒的原料，以制备金刚石的起始微小颗粒，然后赋予金刚石颗粒表面亲水性。 作为亲水性，金刚石颗粒分散在水中以形成浆料，其被固化并保持弱碱性。 然后对浆料进行预分级步骤，由此除去具有D50尺寸为60nm或更大的金刚石颗粒的顶部颗粒尺寸级分的浆料。 除去所述顶部颗粒尺寸级分，然后用水稀释浆料以将金刚石浓度调节至0.1％（重量）以下。 将如此调理的浆料经受离心力，由此将金刚石颗粒的较粗颗粒级分冷凝至固体滤饼并从浆料中除去。 从离心分级中取出流出的浆料，其中含有一部分具有降低的粒度的金刚石颗粒。

公开(公告)号：US08501143B2

公开(公告)日：2013-08-06

申请号：US12245002

申请日：2008-10-03

Applicant: Geoffrey Alan Scarsbrook ,  Philip Maurice Martineau ,  John Lloyd Collins ,  Ricardo Simon Sussmann ,  Bärbel Susanne Charlotte Dorn ,  Andrew John Whitehead ,  Daniel James Twitchen

Inventor： Geoffrey Alan Scarsbrook ,  Philip Maurice Martineau ,  John Lloyd Collins ,  Ricardo Simon Sussmann ,  Bärbel Susanne Charlotte Dorn ,  Andrew John Whitehead ,  Daniel James Twitchen

IPC: B01J3/06 ,  B32B9/00 ,  B32B17/10 ,  C30B23/00 ,  C30B25/00 ,  C30B28/14 ,  H05H1/24

CPC classification number: C30B29/04 ,  C30B25/00 ,  C30B25/105 ,  Y10T428/263 ,  Y10T428/30

Abstract: A single crystal diamond prepared by CVD and having one or more electronic characteristics; making the diamond suitable for electronic applications. Also provided is a method of making the single crystal CVD diamond.