METHOD FOR PRODUCING OPTICALLY ACTIVE a-IONONE
    51.
    发明申请
    METHOD FOR PRODUCING OPTICALLY ACTIVE a-IONONE 有权
    用于生产光学活性α-离子的方法

    公开(公告)号:US20110118500A1

    公开(公告)日:2011-05-19

    申请号:US13012199

    申请日:2011-01-24

    摘要: Provided that a method for inexpensively producing optically active α-ionone with a high yield and a high asymmetric yield and with good workability in a short process, and a perfume composition comprising the optically active α-ionone obtained by the aforementioned method. A method for producing optically active α-ionone, comprising allowing α-ionone as a mixture of optical isomers to react with an esterification agent, and hydrolyzing the obtained α-ionone enol ester; a method for producing optically active α-ionone comprising subjecting α-ionone as a mixture of optical isomers to an asymmetric reduction, allowing the obtained optically active α-ionol to react with an esterification agent to give an optically active α-ionol ester, hydrolyzing the obtained optically active α-ionol ester after purification as necessary, and then oxidizing the obtained optically active α-ionol; and a perfume composition comprising thus obtained optically active α-ionone.

    摘要翻译: 本发明提供了一种低成本地生产光学活性α-紫罗兰酮的方法,其具有高产率和高不对称产率,并且在短时间内具有良好的可加工性,以及包含通过上述方法获得的光学活性α-紫罗兰酮的香料组合物。 一种光学活性α-紫罗兰酮的制造方法,其特征在于,使作为旋光异构体的混合物的α-紫罗烯酮与酯化反应,水解得到的α-紫罗烯酮烯醇酯; 一种光学活性α-紫罗兰酮的制造方法,其特征在于,将α-紫罗烯酮作为光学异构体的混合物进行不对称还原,使得所得光学活性α-离子酚与酯化反应,得到光学活性α-离子醇酯,水解 根据需要纯化后得到的光学活性α-离子醇酯,然后氧化所得光学活性α-离子醇; 和包含这样得到的光学活性α-紫罗兰酮的香料组合物。

    Method for producing optically active α-ionone

    公开(公告)号:US07902404B2

    公开(公告)日:2011-03-08

    申请号:US11991966

    申请日:2006-09-13

    IPC分类号: C07C45/42

    摘要: Provided that a method for inexpensively producing optically active α-ionone with a high yield and a high asymmetric yield and with good workability in a short process, and a perfume composition comprising the optically active α-ionone obtained by the aforementioned method. A method for producing optically active α-ionone, comprising allowing α-ionone as a mixture of optical isomers to react with an esterification agent, and hydrolyzing the obtained α-ionone enol ester; a method for producing optically active α-ionone comprising subjecting α-ionone as a mixture of optical isomers to an asymmetric reduction, allowing the obtained optically active α-ionol to react with an esterification agent to give an optically active α-ionol ester, hydrolyzing the obtained optically active α-ionol ester after purification as necessary, and then oxidizing the obtained optically active α-ionol; and a perfume composition comprising thus obtained optically active α-ionone.

    MANUFACTURING METHOD OF SEMICONDUCTOR DEVICE, INSULATING FILM FOR SEMICONDUCTOR DEVICE, AND MANUFACTURING APPARATUS OF THE SAME
    55.
    发明申请
    MANUFACTURING METHOD OF SEMICONDUCTOR DEVICE, INSULATING FILM FOR SEMICONDUCTOR DEVICE, AND MANUFACTURING APPARATUS OF THE SAME 审中-公开
    半导体器件的制造方法,半导体器件的绝缘膜及其制造装置

    公开(公告)号:US20100181654A1

    公开(公告)日:2010-07-22

    申请号:US12664605

    申请日:2009-06-13

    IPC分类号: H01L23/58 H01L21/471

    摘要: An object to provide an insulating film for a semiconductor device, which has characteristics of low permittivity, a low leak current, and high mechanical strength, undergoes small time-dependent change of these characteristics, and has excellent water resistance, and to provide a manufacturing apparatus of the same, and a manufacturing method of the semiconductor device using the insulating film. The production process comprises a film forming step of supplying a mixed gas containing a carrier gas and a raw material gas, which is a gasified material having borazine skeletal molecules, into a chamber, causing the mixed gas to be in a plasma state, applying a bias to the substrate placed in the chamber, and carrying out gas-phase polymerization by using the borazine skeletal molecule as a fundamental unit so as to form the insulating film on the substrate; and a reaction promoting step of, after the film forming step, bringing the bias applied to the substrate to a different magnitude from the bias in the film forming step, supplying the mixed gas while gradually reducing only the raw material gas, which is the gasified material having the borazine skeletal molecules, treating the insulating film with a plasma mainly comprising the carrier gas.

    摘要翻译: 提供具有低介电常数,低泄漏电流和高机械强度特性的半导体器件绝缘膜的目的是经历这些特性的小的时间依赖性变化,并且具有优异的耐水性,并且提供制造 以及使用该绝缘膜的半导体器件的制造方法。 制造方法包括:将含有载气的混合气体和作为具有环硼氮烷骨架分子的气化材料的原料气体供给到室中的成膜工序,使混合气体处于等离子体状态, 偏置于放置在室内的基板上,通过使用环硼氮烷骨架分子作为基本单元进行气相聚合,以在基板上形成绝缘膜; 以及反应促进步骤,在成膜步骤之后,使得施加到基板上的偏压与成膜步骤中的偏压大小不同,供给混合气体,同时逐渐减少气化的原料气体 具有环硼烷骨架分子的材料,以主要包含载气的等离子体处理绝缘膜。

    METHOD FOR MANUFACTURING FLUID DYNAMIC BEARING DEVICE
    57.
    发明申请
    METHOD FOR MANUFACTURING FLUID DYNAMIC BEARING DEVICE 有权
    制造流体动力轴承装置的方法

    公开(公告)号:US20100132197A1

    公开(公告)日:2010-06-03

    申请号:US12595198

    申请日:2008-03-24

    IPC分类号: F16C43/02 F16C17/10 B21D53/10

    摘要: Easy and precise setting of a predetermined thrust bearing gap is made possible.An axial gap 13 having a dimension that is equal to the sum of two thrust bearing gaps is first provided between the flange part 2b of the shaft member 2 and the bearing member or bearing sleeve 8. The shaft member 2 and the bearing sleeve 8 are accommodated inside the housing 7 with this gap dimension 8 being kept, and the bearing sleeve 8 is secured to the housing 7.

    摘要翻译: 可以容易且精确地设定预定的推力轴承间隙。 首先,在轴构件2的凸缘部2b与轴承构件或轴承套筒8之间设置尺寸等于两个推力轴承间隙的总和的轴向间隙13.轴构件2和轴承套筒8是 容纳在壳体7内,保持该间隙尺寸8,并且轴承套筒8固定到壳体7。