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    Rheometer for rapidly measuring small quantity samples
    71.
    发明申请
    Rheometer for rapidly measuring small quantity samples 审中-公开
    用于快速测量小批量样品的流变仪

    公开(公告)号：US20040093932A1

    公开(公告)日：2004-05-20

    申请号：US10712617

    申请日：2003-11-12

    Applicant: Symyx Technologies, Inc.

    Inventor： Damian Hajduk ,  Eric Carlson ,  Ravi Srinivasan

    IPC: G01N011/10 ,  G01N011/14 ,  G01N003/24

    CPC classification number: G01N3/24 ,  G01N11/16 ,  G01N2203/0051 ,  G01N2203/0286 ,  G01N2203/0623

    Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element. Moreover, a rheometer is provided which comprises a force sensor based on stress-optic material.

    Abstract translation: 本发明涉及微型流变仪，平行流变仪和改进的力传感器元件，其可有利地与微型流变仪和平行流变仪组合使用。 微型流变仪适用于确定以少量样品形式提供的材料的流变特性。 微型流变仪包括致动元件，感测元件和反馈电路，以提供由样品施加到感测元件的剪切力的重新平衡，这确保了确定剪切应变的特殊刚度，从而允许高精度的测量。 本发明的并行流变仪允许多个样本的同时测量，以便在短时间内允许多个样本。 根据本发明的力传感器元件允许同时测量施加到传感器元件的剪切力和法向力。 此外，提供了一种流变仪，其包括基于应力光学材料的力传感器。

    High throughput permeability testing of materials libraries
    72.
    发明申请
    High throughput permeability testing of materials libraries 有权
    材料库的高通量渗透率测试

    公开(公告)号：US20040077091A1

    公开(公告)日：2004-04-22

    申请号：US10274184

    申请日：2002-10-18

    Applicant: Symyx Technologies, Inc.

    Inventor： Damian A. Hajduk ,  Oleg Kolosov

    IPC: G01N033/00

    CPC classification number: G01N33/442 ,  G01N7/10 ,  G01N15/0826 ,  G01N2015/086 ,  Y10T436/11 ,  Y10T436/20 ,  Y10T436/207497 ,  Y10T436/209163 ,  Y10T436/25875

    Abstract: A library of material samples is screened for properties such as permeability. A library of material samples is provided. A stimulus such as an exposure to a permeate fluid is provided to each member of the library. A response of each of the material samples due to the stimulus is measured and the response, the stimulus or both are recorded and related to provide data. Thereafter, the data is analyzed to reach conclusions regarding the properties of the material samples.

    Abstract translation: 对材料样品库进行筛选，例如渗透性等。 提供材料样本库。 向图书馆的每个成员提供诸如暴露于渗透液的刺激。 测量由于刺激引起的每个材料样品的响应，并记录响应，刺激或两者以提供数据。 此后，分析数据以得出关于材料样品的性质的结论。

    Parallel reactor for sampling and conducting in situ flow-through reactions and a method of using same
    73.
    发明申请
    Parallel reactor for sampling and conducting in situ flow-through reactions and a method of using same 有权
    用于取样和进行原位流通反应的并联反应器及其使用方法

    公开(公告)号：US20040063208A1

    公开(公告)日：2004-04-01

    申请号：US10665796

    申请日：2003-09-19

    Applicant: Symyx Technologies, Inc.

    Inventor： William H. Chandler JR.

    IPC: G01N031/10

    CPC classification number: F28F27/00 ,  B01J19/0046 ,  B01J2219/00155 ,  B01J2219/00283 ,  B01J2219/00308 ,  B01J2219/00351 ,  B01J2219/00477 ,  B01J2219/00481 ,  B01J2219/00495 ,  B01J2219/00585 ,  B01J2219/0059 ,  B01J2219/00698 ,  B01J2219/00718 ,  C40B60/14 ,  Y10T436/11 ,  Y10T436/142222

    Abstract: An apparatus for parallel processing of reaction mixtures, including a reactor block including reaction chambers for containing reaction mixtures under pressure, the reactor block further including a first sidewall, a second sidewall, and a first plurality of fluid flow paths providing fluid communication with the first sidewall and respective reaction chambers and the second sidewall and respective reaction chambers;; a stirring system including a base plate defining a second plurality of flow paths, wherein respective flow paths of said second plurality of flow paths are in fluid communication with respective reaction chambers and respective fluid flow paths of said first plurality of flow paths, and the base plate also supports a plurality of stirring blade assemblies for mixing the reaction mixtures; interchangeable manifolds supported by the first sidewall and the second sidewall, the interchangeable manifolds defining a plurality of manifold inlet/outlet ports, wherein respective inlet/outlet ports of said plurality of inlet/outlet ports are in communication with respective fluid flow paths of said first plurality of fluid flow paths and permit fluid to be introduced into or vented from the respective reaction chambers; and a sampling manifold assembly coupled in fluid communication with the respective reaction chambers, wherein a portion of the reaction mixture retained in the respective reaction chambers can be withdrawn from the respective reaction chamber through respective fluid flow paths of said first plurality of fluid flow paths and respective flow paths of said second plurality of flow paths, or both, without depressurizing or lowering the pressure in the respective reaction chamber.

    Abstract translation: 一种用于反应混合物的并行处理的装置，包括反应器块，其包括用于在压力下包含反应混合物的反应室，反应器模块还包括第一侧壁，第二侧壁和第一多个流体流动路径，其提供与第一 侧壁和相应的反应室以及第二侧壁和相应的反应室; 搅拌系统，其包括限定第二多个流动路径的基板，其中所述第二多个流动路径的相应流动路径与所述第一多个流动路径的相应反应室和相应的流体流动路径流体连通，并且所述基部 板还支撑用于混合反应混合物的多个搅拌叶片组件; 可互换歧管由第一侧壁和第二侧壁支撑，可互换歧管限定多个歧管入口/出口，其中所述多个入口/出口端口的相应入口/出口与所述第一侧壁和第二侧壁的相应流体流动路径连通 多个流体流动路径并允许流体从各个反应室引入或排出; 以及与各个反应室流体连通地连接的采样歧管组件，其中保留在各个反应室中的反应混合物的一部分可以通过所述第一多个流体流路的相应流体流动路径从相应的反应室中排出， 所述第二多个流动路径或两者的相应流动路径，而不减压或降低各个反应室中的压力。

    Control agents for living-type free radical polymerization, methods of polymerizing and polymers with same
    74.
    发明申请
    Control agents for living-type free radical polymerization, methods of polymerizing and polymers with same 失效
    活性自由基聚合的控制剂，聚合方法和与其相同的聚合物

    公开(公告)号：US20040019163A1

    公开(公告)日：2004-01-29

    申请号：US10407614

    申请日：2003-04-03

    Applicant: Symyx Technologies, Inc.

    Inventor： Dominique Charmot ,  Han Ting Chang ,  Wenyue Wang

    IPC: C08F004/52

    CPC classification number: C08F2/38

    Abstract: Control agents that have a nitrogen-nitrogen bond covalently bonded to a thiocarbonyl moiety are provided for living-type free radical polymerization of a wide variety of monomers. These control agents provide superior properties for control of the polymerization and/or the properties of the polymers obtained and/or the monomers that may be polymerized. In some embodiments, a bulky group is pendant off the activated thiocarbonyl portion of the control agents. Multifunctional control agents provide the opportunity for a variety of structurally unique polymers, including block copolymers, stars and hyper-branched polymers.

    Abstract translation: 提供了与硫代羰基部分共价连接的氮 - 氮键的对照试剂，用于各种单体的活性自由基聚合。 这些控制剂提供了用于控制聚合的优异性质和/或所获得的聚合物和/或可被聚合的单体的性质。 在一些实施方案中，大体积基团从控制剂的活化的硫代羰基部分脱落。 多功能控制剂为各种结构独特的聚合物，包括嵌段共聚物，恒星和超支化聚合物提供了机会。

    Apparatus and method for characterizing libraries of different materials using x-ray scattering
    75.
    发明申请
    Apparatus and method for characterizing libraries of different materials using x-ray scattering 审中-公开
    使用X射线散射来表征不同材料的文库的装置和方法

    公开(公告)号：US20040017896A1

    公开(公告)日：2004-01-29

    申请号：US10448039

    申请日：2003-05-22

    Applicant: Symyx Technologies, Inc.

    Inventor： Damian Hajduk ,  James Bennett ,  Rakesh Jain

    IPC: H05G001/00

    CPC classification number: G01N23/20 ,  B01J19/0046 ,  B01J2219/00315 ,  B01J2219/00511 ,  B01J2219/00585 ,  B01J2219/00596 ,  B01J2219/00659 ,  B01J2219/00704 ,  B01J2219/00707 ,  B01J2219/00745 ,  C40B40/18 ,  Y10T436/25

    Abstract: An apparatus for characterizing a library containing an array of samples. The apparatus includes an x-ray beam directed at the library, a chamber housing the library and a beamline for directing the x-ray beam onto the library in the chamber. The chamber may include a translation stage that holds the library and that is programmable to change the position of the library relative to the x-ray beam and a controller that controls the movement of the translation stage to expose an element to the x-ray beam in order to rapidly characterize the element in the library. During the characterization, the x-ray beam diffracts upon impinging the element and a detector detects the diffracted x-ray beam in order to generate characterization data for the element.

    Abstract translation: 用于表征包含样本阵列的库的装置。 该装置包括指向文库的x射线束，容纳库的腔室和用于将x射线束引导到腔室中的文库的束线。 所述腔室可以包括平移台，其保持所述库并且可编程以改变所述库相对于所述X射线束的位置;以及控制器，所述控制器控制所述平移台的运动以将元件暴露于所述X射线束 以便快速表征图书馆中的元素。 在表征期间，x射线束在撞击元件时衍射，并且检测器检测衍射的X射线束，以便产生元件的表征数据。

    Cleaving and replacing thio control agent moieties from polymers made by living-type free radical polymerization
    76.
    发明申请
    Cleaving and replacing thio control agent moieties from polymers made by living-type free radical polymerization 失效
    从活性自由基聚合制备的聚合物中切割和取代硫代控制剂部分

    公开(公告)号：US20030232938A1

    公开(公告)日：2003-12-18

    申请号：US10407405

    申请日：2003-04-03

    Applicant: Symyx Technologies, Inc.

    Inventor： Dominique Charmot ,  Han Ting Chang ,  Wenyue Wang ,  Marcelo Piotti

    IPC: C08F004/00

    CPC classification number: C08F2/38

    Abstract: A method of free radical polymerization and for cleaving a thio group from the resulting polymer is provided. The method comprises forming a mixture of one or more monomers, at least one free radical source and a control agent, wherein the control agent comprises a thio moiety. The mixture is polymerized, and the resulting polymer is mixed with a free radical source, and optionally an addition fragmentation agent under cleavage conditions. The thio moiety on the polymer is replaced with a group of interest.

    Abstract translation: 提供了一种自由基聚合和从所得聚合物中切割硫基的方法。 该方法包括形成一种或多种单体，至少一种自由基源和对照剂的混合物，其中控制剂包含硫代部分。 将混合物聚合，并将所得聚合物与裂解条件下的自由基源和任选的加成断裂剂混合。 聚合物上的硫代部分被感兴趣的一组取代。

    High pressure parallel reactor with individually sealable vessels
    79.
    发明申请
    High pressure parallel reactor with individually sealable vessels 有权
    具有单独密封容器的高压并联反应器

    公开(公告)号：US20030202911A1

    公开(公告)日：2003-10-30

    申请号：US10317315

    申请日：2002-12-12

    Applicant: Symyx Technologies, Inc.

    Inventor： Lynn Van Erden ,  William H. Chandler JR.

    IPC: B01J019/00

    CPC classification number: B01J3/04 ,  B01J19/0046 ,  B01J2219/00283 ,  B01J2219/00308 ,  B01J2219/00313 ,  B01J2219/00315 ,  B01J2219/00335 ,  B01J2219/00477 ,  B01J2219/00585 ,  B01J2219/00601 ,  B01J2219/0072 ,  B01J2219/00745 ,  B01J2219/00747 ,  C40B30/08 ,  C40B40/18 ,  C40B60/14 ,  Y10T436/25

    Abstract: An apparatus and method for synthesis and screening of materials are disclosed. According to one aspect of the present invention, a parallel batch reactor for effecting chemical reactions includes a pressure chamber, an inlet port, two or more reaction vessels within the pressure chamber, and a reaction vessel cover. The inlet port is in fluid communication with the pressure chamber, and pressurizes the pressure chamber from an external pressure source. Each of the two or more reaction vessels are in isolatable fluid communication with the pressure chamber such that during a first pressurizing stage of operation, each of the two or more reaction vessels can be simultaneously pressurized through common fluid communication with the pressure chamber. In addition, during at least a second reaction stage of operation, each of the two or more pressurized reaction vessels can be isolated from each other by positioning the reaction vessel cover appropriately.

    Abstract translation: 公开了一种合成和筛选材料的装置和方法。 根据本发明的一个方面，用于实现化学反应的并行批量反应器包括压力室，入口，压力室内的两个或更多个反应容器和反应容器盖。 入口与压力室流体连通，并从外部压力源对压力室加压。 两个或更多个反应容器中的每一个与压力室可分离流体连通，使得在操作的第一加压阶段期间，两个或更多个反应容器中的每一个可以通过与压力室的常见流体连通同时加压。 此外，在操作的至少第二反应阶段中，通过适当地定位反应容器盖，可以将两个或更多个加压反应容器中的每一个彼此隔离。

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