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1.发明授权公开(公告)号：US06537500B1
公开(公告)日：2003-03-25
申请号：US09350459
申请日：1999-07-09
申请人： Armin Brenner , Armin Lange de Oliveira , Ferdi Schuth , Stephan Schunk , Wolfram Stichert , Klaus Unger
发明人： Armin Brenner , Armin Lange de Oliveira , Ferdi Schuth , Stephan Schunk , Wolfram Stichert , Klaus Unger
IPC分类号： G01N3096
CPC分类号： G01N21/17 , B01J19/0046 , B01J2219/00286 , B01J2219/00313 , B01J2219/00333 , B01J2219/00423 , B01J2219/00495 , B01J2219/00585 , B01J2219/0059 , B01J2219/00704 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , Y10T436/255 , Y10T436/25875
摘要： Process for the detection of a product in the discharge of a catalytic material of a plurality of catalytic materials which are exposed to a reaction gas, whereby an adsorbent selective for the product to be determined is disposed in the discharge of each catalytic material, which changes at least one of its properties through the contact with the product to be determined and the change in the property of the adsorbent is then ascertained. The process serves in particular to determine the selectivity and activity of catalytic materials.
摘要翻译： 用于检测在暴露于反应气体中的多种催化材料的催化材料的排出中的产物的检测方法，由此在每种催化材料的排出中设置对待测产物有选择性的吸附剂， 然后确定通过与要测定的产物的接触和吸附剂的性质变化的其性质中的至少一种。该方法尤其用于确定催化材料的选择性和活性。
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公开(公告)号：US08383050B2
公开(公告)日：2013-02-26
申请号：US12892449
申请日：2010-09-28
申请人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
发明人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
CPC分类号： B01J19/0006 , B01J19/0046 , B01J2219/00038 , B01J2219/00162 , B01J2219/00164 , B01J2219/00286 , B01J2219/00389 , B01J2219/00391 , B01J2219/00423 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00689 , B01J2219/00707 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , C40B60/14 , Y10T436/21
摘要： A method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces is provided. A device for the parallel study of chemical reactions includes at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.
摘要翻译： 提供了在至少两个空间分离的反应空间中并行研究化学反应的方法和装置。 用于平行研究化学反应的装置至少包括以下组分：（a）至少两个空间分离的反应空间; （b）在反应空间输入侧，根据（a）的反应空间的至少一种普通的喷射进料; （d）在反应空间输出侧，每个反应空间至少一个连接到所有反应空间或它们的子集共同的至少一个保持气体进料; （e）在反应空间输出侧和根据（d）在产品流动方向上与保持气体进料的连接的下游，每个反应空间至少有一个限制器。
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公开(公告)号：US20110014718A1
公开(公告)日：2011-01-20
申请号：US12892449
申请日：2010-09-28
申请人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
发明人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
CPC分类号： B01J19/0006 , B01J19/0046 , B01J2219/00038 , B01J2219/00162 , B01J2219/00164 , B01J2219/00286 , B01J2219/00389 , B01J2219/00391 , B01J2219/00423 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00689 , B01J2219/00707 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , C40B60/14 , Y10T436/21
摘要： The present invention relates to a method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces. In particular, the invention is suitable for reactions which are not constant volume reactions and/or for reactions in which fluid flows through at least two spatially separated reaction spaces are intended to be controlled together for all the reaction spaces, or for related subsets of them, in the most straightforward way possible.According to one embodiment, the device according to the invention for the parallel study of chemical reactions comprises at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.
摘要翻译： 本发明涉及在至少两个空间分离的反应空间中并行研究化学反应的方法和装置。 特别地，本发明适用于不是恒定的体积反应和/或其中流体流过至少两个空间分离的反应空间的反应旨在一起控制所有反应空间或其相关子集的反应 ，以最直接的方式可能。 根据一个实施方案，根据本发明的用于平行研究化学反应的装置至少包括以下组分：（a）至少两个空间分离的反应空间; （b）在反应空间输入侧，根据（a）的反应空间的至少一种普通的喷射进料; （d）在反应空间输出侧，每个反应空间至少一个连接到所有反应空间或它们的子集共同的至少一个保持气体进料; （e）在反应空间输出侧和根据（d）在产品流动方向上与保持气体进料的连接的下游，每个反应空间至少有一个限制器。
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公开(公告)号：US20090258431A1
公开(公告)日：2009-10-15
申请号：US12424744
申请日：2009-04-16
申请人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
发明人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
CPC分类号： B01J19/0006 , B01J19/0046 , B01J2219/00038 , B01J2219/00162 , B01J2219/00164 , B01J2219/00286 , B01J2219/00389 , B01J2219/00391 , B01J2219/00423 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00689 , B01J2219/00707 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , C40B60/14 , Y10T436/21
摘要： The present invention relates to a method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces. In particular, the invention is suitable for reactions which are not constant volume reactions and/or for reactions in which fluid flows through at least two spatially separated reaction spaces are intended to be controlled together for all the reaction spaces, or for related subsets of them, in the most straightforward way possible.According to one embodiment, the device according to the invention for the parallel study of chemical reactions comprises at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.
摘要翻译： 本发明涉及在至少两个空间分离的反应空间中并行研究化学反应的方法和装置。 特别地，本发明适用于不是恒定的体积反应和/或其中流体流过至少两个空间分离的反应空间的反应旨在一起控制所有反应空间或其相关子集的反应 ，以最直接的方式可能。 根据一个实施方案，根据本发明的用于平行研究化学反应的装置至少包括以下组分：（a）至少两个空间分离的反应空间; （b）在反应空间输入侧，根据（a）的反应空间的至少一种普通的喷射进料; （d）在反应空间输出侧，每个反应空间至少一个连接到所有反应空间或它们的子集共同的至少一个保持气体进料; （e）在反应空间输出侧和根据（d）在产品流动方向上与保持气体进料的连接的下游，每个反应空间至少有一个限制器。
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公开(公告)号：US07537739B2
公开(公告)日：2009-05-26
申请号：US10583753
申请日：2004-12-20
申请人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
发明人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
CPC分类号： B01J19/0006 , B01J19/0046 , B01J2219/00038 , B01J2219/00162 , B01J2219/00164 , B01J2219/00286 , B01J2219/00389 , B01J2219/00391 , B01J2219/00423 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00689 , B01J2219/00707 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , C40B60/14 , Y10T436/21
摘要： The present invention relates to a method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces. In particular, the invention is suitable for reactions which are not constant volume reactions and/or for reactions in which fluid flows through at least two spatially separated reaction spaces are intended to be controlled together for all the reaction spaces, or for related subsets of them, in the most straightforward way possible.According to one embodiment, the device according to the invention for the parallel study of chemical reactions comprises at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.
摘要翻译： 本发明涉及在至少两个空间分离的反应空间中并行研究化学反应的方法和装置。 特别地，本发明适用于不是恒定的体积反应和/或其中流体流过至少两个空间分离的反应空间的反应旨在一起控制所有反应空间或其相关子集的反应 ，以最直接的方式可能。 根据一个实施方案，根据本发明的用于平行研究化学反应的装置至少包括以下组分：（a）至少两个空间分离的反应空间; （b）在反应空间输入侧，根据（a）的反应空间的至少一种普通的喷射进料; （d）在反应空间输出侧，每个反应空间至少一个连接到所有反应空间或它们的子集共同的至少一个保持气体进料; （e）在反应空间输出侧和根据（d）在产品流动方向上与保持气体进料的连接的下游，每个反应空间至少有一个限制器。
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6.发明授权Process and apparatus for the combinatorial production and testing of catalyst material libraries by using at least two analytical methods 失效通过使用至少两种分析方法组合生产和测试催化剂材料库的方法和设备公开(公告)号：US07374942B2
公开(公告)日：2008-05-20
申请号：US09809423
申请日：2001-03-16
申请人： Jens Klein , Wolfram Stichert , Wolfgang Strehlau , Armin Brenner , Stephan Andreas Schunk , Dirk Demuth
发明人： Jens Klein , Wolfram Stichert , Wolfgang Strehlau , Armin Brenner , Stephan Andreas Schunk , Dirk Demuth
CPC分类号： G01N31/10 , B01J19/0046 , B01J2219/00286 , B01J2219/00313 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00689 , B01J2219/00704 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , Y10T436/21 , Y10T436/212 , Y10T436/214 , Y10T436/216 , Y10T436/24 , Y10T436/25875
摘要： A process and apparatus for testing material libraries, in particular catalysts, by means of coupled use of at least two analytical methods, preferably IR thermography and mass spectrometry. Owing to the selected arrangement, the disadvantages of the two previously known individual methods are compensated for: the subsequent selectivity determination for selected sections by means of mass spectrometry invalidates the argument against IR thermography, of only being able to determine activities; the rapid integrated determination of potentially “good” materials via IR thermography prevents an excessive loss of time by needing to test all materials of a library successively with the mass spectrometer. The reactor design permits, firstly, the integral recording of the entire reactor through a window which is transparent for the corresponding method and, secondly, permits the simultaneous, automated application of a second analytical method (for example mass spectrometry) to selected materials of a material library, which have been rated as active by the optical method. In the case described, the optical method provides information on the material activity for a set problem, and the second analytical method determines the selectivity of the materials.
摘要翻译： 用于通过耦合使用至少两种分析方法，优选IR热成像和质谱法来测试材料库，特别是催化剂的方法和装置。 由于所选择的布置，以前已知的两种方法的缺点得到补偿：通过质谱法对所选部分的随后的选择性测定使得仅针对红外热像仪的论证无效地确定活动; 通过红外热像仪快速综合测定潜在的“良好”材料，可以通过质谱连续测试所有材料，从而防止过多的时间损失。 反应器设计首先通过对于相应方法是透明的窗口整体记录整个反应器，其次允许将第二种分析方法（例如质谱法）同时自动应用于所选择的材料 材料库，通过光学方法被评为有效。 在所描述的情况下，光学方法提供关于集合问题的材料活性的信息，第二分析方法确定材料的选择性。
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公开(公告)号：US09708553B2
公开(公告)日：2017-07-18
申请号：US14236994
申请日：2012-07-30
申请人： Josef Find , Alfred Haas , Armin Brenner
发明人： Josef Find , Alfred Haas , Armin Brenner
CPC分类号： C10G65/14 , B01J19/0046 , B01J2219/00286 , B01J2219/00306 , B01J2219/00389 , B01J2219/00418 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00698 , B01J2219/00707 , B01J2219/0072 , B01J2219/00747 , C10G29/02 , C10G45/22 , C40B30/08 , C40B60/12
摘要： The present invention relates to a process for handling product fluid streams which are obtained in the catalytic hydrogenation of liquid feeds in laboratory catalysis apparatuses. The liquid feeds are preferably hydrocarbons comprising sulfur- and nitrogen-comprising compounds as impurities. The hydrogenation serves to convert the impurities into hydrogen sulfide and ammonia which in this form can be readily separated off from the other constituents of the liquid feed. The product fluid streams are contacted with an inert gas stream, with the flow rate of the inert gas being a multiple of the flow rate of the product fluid stream. The formation of deposits in lines of the region on the outlet side of the reaction space can be effectively prevented by means of the process of the invention.
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公开(公告)号：US07867458B2
公开(公告)日：2011-01-11
申请号：US12424744
申请日：2009-04-16
申请人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
发明人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
CPC分类号： B01J19/0006 , B01J19/0046 , B01J2219/00038 , B01J2219/00162 , B01J2219/00164 , B01J2219/00286 , B01J2219/00389 , B01J2219/00391 , B01J2219/00423 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00689 , B01J2219/00707 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , C40B60/14 , Y10T436/21
摘要： The present invention relates to a method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces. In particular, the invention is suitable for reactions which are not constant volume reactions and/or for reactions in which fluid flows through at least two spatially separated reaction spaces are intended to be controlled together for all the reaction spaces, or for related subsets of them, in the most straightforward way possible.According to one embodiment, the device according to the invention for the parallel study of chemical reactions comprises at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.
摘要翻译： 本发明涉及在至少两个空间分离的反应空间中并行研究化学反应的方法和装置。 特别地，本发明适用于不是恒定的体积反应和/或其中流体流过至少两个空间分离的反应空间的反应旨在一起控制所有反应空间或其相关子集的反应 ，以最直接的方式可能。 根据一个实施方案，根据本发明的用于平行研究化学反应的装置至少包括以下组分：（a）至少两个空间分离的反应空间; （b）在反应空间输入侧，根据（a）的反应空间的至少一种普通的喷射进料; （d）在反应空间输出侧，每个反应空间至少一个连接到所有反应空间或它们的子集共同的至少一个保持气体进料; （e）在反应空间输出侧和根据（d）在产品流动方向上与保持气体进料的连接的下游，每个反应空间至少有一个限制器。
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公开(公告)号：US06862533B2
公开(公告)日：2005-03-01
申请号：US09876142
申请日：2001-06-08
申请人： Wolfgang Strehlau , John Michael Newsam , Dirk Demuth , Wolfram Stichert , Armin Brenner , Stephan A. Schunk , Jens Klein
发明人： Wolfgang Strehlau , John Michael Newsam , Dirk Demuth , Wolfram Stichert , Armin Brenner , Stephan A. Schunk , Jens Klein
CPC分类号： B01J19/0046 , B01J2219/00689 , B01J2219/00695 , B01J2219/007 , B01J2219/00702 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , B01J2219/00754 , C40B30/08 , C40B40/18 , G06F19/16
摘要： The invention relates to a method for the automated production and iterative automated optimization of a substance library and/or at least one reaction parameter relating to a performance characteristic comprising at least two substances comprising the steps of: a) defining at least one production parameter and at least one test parameter; b) automated preparation of a substance library by producing at least two substances on the basis of the at least one production parameter; c) automated testing of the at least two substances of the substance library with respect to at least one performance characteristic on the basis of the at least one test parameter; d) evaluating the test using electronic data analysis; e) varying the at least one production parameter and/or the at least one test parameter for optimizing the performance characteristics, and single or repeated repetition of steps b) to e) or c) to e); characterized in that the steps b) to e) are carried out in an integrated automated process.
摘要翻译： 本发明涉及用于物质文库的自动生产和迭代自动优化的方法和/或与包括至少两种物质的性能特征相关的至少一个反应参数的方法，包括以下步骤：a）定义至少一个生产参数和 至少一个测试参数; b）通过基于至少一个生产参数生产至少两种物质来自动制备物质文库; c）基于所述至少一个测试参数，相对于至少一个性能特征自动测试所述物质文库的至少两种物质; d）使用电子数据分析评估测试; e）改变所述至少一个生产参数和/或所述至少一个测试参数以优化所述性能特征，以及步骤b）至e）或c）至e）的单个或重复重复; 其特征在于步骤b）至e）以综合自动化过程进行。
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公开(公告)号：US20070148062A1
公开(公告)日：2007-06-28
申请号：US10583753
申请日：2004-12-20
申请人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
发明人： Alfred Haas , Wolfgang Strehlau , Armin Brenner , Oliver Koechel , Markus Friess , Torsten Zech
CPC分类号： B01J19/0006 , B01J19/0046 , B01J2219/00038 , B01J2219/00162 , B01J2219/00164 , B01J2219/00286 , B01J2219/00389 , B01J2219/00391 , B01J2219/00423 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00601 , B01J2219/00689 , B01J2219/00707 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , C40B60/14 , Y10T436/21
摘要： The present invention relates to a method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces. In particular, the invention is suitable for reactions which are not constant volume reactions and/or for reactions in which fluid flows through at least two spatially separated reaction spaces are intended to be controlled together for all the reaction spaces, or for related subsets of them, in the most straightforward way possible. According to one embodiment, the device according to the invention for the parallel study of chemical reactions comprises at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.
摘要翻译： 本发明涉及用于平行研究至少两个空间分离的反应空间中的化学反应的方法和装置。 特别地，本发明适用于不是恒定的体积反应和/或其中流体流过至少两个空间分离的反应空间的反应旨在一起控制所有反应空间或其相关子集的反应 ，以最直接的方式可能。 根据一个实施方案，根据本发明的用于平行研究化学反应的装置至少包括以下组分：（a）至少两个空间分离的反应空间; （b）在反应空间输入侧，根据（a）的反应空间的至少一种普通的喷射进料; （d）在反应空间输出侧，每个反应空间至少一个连接到所有反应空间或它们的子集共同的至少一个保持气体进料; （e）在反应空间输出侧和根据（d）在产品流动方向上与保持气体进料的连接的下游，每个反应空间至少有一个限制器。
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