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公开(公告)号：US20130172177A1
公开(公告)日：2013-07-04
申请号：US13824113
申请日：2011-09-13
Applicant: Imme Domke , Wolfgang Rohde , Piotr Antoni Bazula , Norbert Mronga , Yong Liu , Martin Dieterle , Stanley Roth , Curtis Zimmermann , Xinyi Wei , Philipp Raff , Stephan Andreas Schunk , Olga Gerlach , Andreas Strasser , Michael Paul
Inventor： Imme Domke , Wolfgang Rohde , Piotr Antoni Bazula , Norbert Mronga , Yong Liu , Martin Dieterle , Stanley Roth , Curtis Zimmermann , Xinyi Wei , Philipp Raff , Stephan Andreas Schunk , Olga Gerlach , Andreas Strasser , Michael Paul
IPC: B01J23/42
CPC classification number: B01J23/42 , B01D53/945 , B01D2255/1021 , B01D2255/1023 , B01D2255/1025 , B01D2255/1026 , B01D2255/104 , B01D2255/2065 , B01D2255/20707 , B01D2255/20715 , B01D2255/20723 , B01D2255/2073 , B01D2255/20738 , B01D2255/20746 , B01D2255/20753 , B01D2255/20761 , B01D2255/20769 , B01D2255/20784 , B01D2255/20792 , B01D2255/9202 , B01D2255/9205 , B01D2255/9207 , B01D2258/012 , B01J21/04 , B01J21/08 , B01J35/0013 , B01J35/0086 , B01J35/08 , B01J35/1014 , B01J35/1019 , B01J37/0072 , B01J37/0203 , B01J37/0205 , B01J37/0211 , B01J37/036 , B01J37/088 , B01J37/16 , Y02T10/22
Abstract: A catalyst comprising (i) a support, (ii) metal particles and (iii) a shell which is arranged between the metal particles, wherein the shell (iii) comprises silicon oxide.
Abstract translation: 一种催化剂，其包含（i）载体，（ii）金属颗粒和（iii）布置在金属颗粒之间的壳，其中壳（iii）包含氧化硅。
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公开(公告)号：US07202088B2
公开(公告)日：2007-04-10
申请号：US10333850
申请日：2001-07-27
Applicant: Alfred Haas , Stephan Andreas Schunk , Dirk Demuth , Wolfgang Strehlau , Armin Brenner , Wolfram Stichert
Inventor： Alfred Haas , Stephan Andreas Schunk , Dirk Demuth , Wolfgang Strehlau , Armin Brenner , Wolfram Stichert
IPC: G01N31/10
CPC classification number: B01J19/0093 , B01J19/0046 , B01J2219/00313 , B01J2219/00319 , B01J2219/00351 , B01J2219/00495 , B01J2219/00585 , B01J2219/0068 , B01J2219/00698 , B01J2219/00704 , B01J2219/00747 , B01J2219/0081 , B01J2219/00835 , B01J2219/00871 , B01J2219/00873 , B01L7/00
Abstract: The present invention relates to an arrangement, in particular for the parallel testing of a plurality of building blocks of a material library for performance characteristics, in which the arrangement has a block containing at least one reaction module and at least two heating/cooling modules.
Abstract translation: 本发明涉及一种布置，特别是用于并行测试用于性能特征的材料库的多个结构单元，其中该装置具有包含至少一个反应模块和至少两个加热/冷却模块的块。
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3.发明授权公开(公告)号：US06873414B2
公开(公告)日：2005-03-29
申请号：US09773534
申请日：2001-02-02
Applicant: Ferdi Schüth , Armin Brenner , Stephan Andreas Schunk
Inventor： Ferdi Schüth , Armin Brenner , Stephan Andreas Schunk
CPC classification number: G01N21/1702 , B01J19/0046 , B01J2219/00286 , B01J2219/00306 , B01J2219/00313 , B01J2219/00585 , B01J2219/00596 , B01J2219/00659 , B01J2219/00698 , B01J2219/00704 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18
Abstract: Method for determining useful properties of individual building blocks of a material library including a substrate having at least two individual building blocks in at least two sections separated from one another, which method includes: (ii) introducing at least one starting material into at least two sections of a substrate of a material library which are separated from one another, in order to carry out a chemical or physical or chemical and physical reaction of the starting material in the at least two substrate sections separated from another, in each case in the presence of the corresponding building block, obtaining in each case an effluent comprising at least one reaction product and/or starting material and, (iii) analysing the effluent obtained in the reaction according to (ii) comprising at least one reaction product and/or starting material; the effluent being analysed by recording and analysing at least one photoacoustic signal.
Abstract translation: 用于确定材料库的各个构件的有用特性的方法，该材料库包括在彼此分开的至少两个部分中具有至少两个单个结构单元的基底，所述方法包括：（ii）将至少一种起始材料引入至少两个 在彼此分离的材料库的基底的部分，以便在存在的情况下在每种情况下进行与另一个分开的至少两个基底部分中的起始材料的化学或物理或化学和物理反应 在每种情况下获得包含至少一种反应产物和/或起始材料的流出物，和（iii）分析根据（ii）在反应中获得的流出物，其包含至少一种反应产物和/或起始 材料; 通过记录和分析至少一个光声信号来分析流出物。
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公开(公告)号：US08158815B2
公开(公告)日：2012-04-17
申请号：US12735123
申请日：2008-12-16
Applicant: Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
Inventor： Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
CPC classification number: B01J29/90 , B01J29/20 , B01J38/14 , C07C51/12 , C07C67/37 , Y02P20/584 , C07C53/08 , C07C69/14
Abstract: A process for the carbonylation of dimethyl ether, dimethyl carbonate and/or methanol with carbon monoxide and hydrogen in the presence of a mordenite catalyst to produce at least one of acetic acid and methyl acetate in which process the mordenite catalyst is regenerated in-situ by contacting the catalyst with a regenerating gas comprising a molecular oxygen-containing gas and an inert diluent at a total pressure in the range 1 to 100 bar and wherein the partial pressure of the molecular oxygen-containing gas is such that the temperature of the catalyst is maintained within the range 225 to 325° C.
Abstract translation: 一种在丝光沸石催化剂存在下用一氧化碳和氢气二甲醚，二甲基碳酸酯和/或甲醇羰基化的方法，以产生乙酸和乙酸甲酯中的至少一种，其中丝光沸石催化剂原位再生 使催化剂与包含含分子氧的气体和惰性稀释剂的再生气体在1至100巴的总压下接触，并且其中分子氧气体的分压使得催化剂的温度为 维持在225至325℃的范围内
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5.发明授权Process and apparatus for the combinatorial production and testing of catalyst material libraries by using at least two analytical methods 失效通过使用至少两种分析方法组合生产和测试催化剂材料库的方法和设备公开(公告)号：US07374942B2
公开(公告)日：2008-05-20
申请号：US09809423
申请日：2001-03-16
Applicant: Jens Klein , Wolfram Stichert , Wolfgang Strehlau , Armin Brenner , Stephan Andreas Schunk , Dirk Demuth
Inventor： Jens Klein , Wolfram Stichert , Wolfgang Strehlau , Armin Brenner , Stephan Andreas Schunk , Dirk Demuth
CPC classification number: G01N31/10 , B01J19/0046 , B01J2219/00286 , B01J2219/00313 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00689 , B01J2219/00704 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , Y10T436/21 , Y10T436/212 , Y10T436/214 , Y10T436/216 , Y10T436/24 , Y10T436/25875
Abstract: A process and apparatus for testing material libraries, in particular catalysts, by means of coupled use of at least two analytical methods, preferably IR thermography and mass spectrometry. Owing to the selected arrangement, the disadvantages of the two previously known individual methods are compensated for: the subsequent selectivity determination for selected sections by means of mass spectrometry invalidates the argument against IR thermography, of only being able to determine activities; the rapid integrated determination of potentially “good” materials via IR thermography prevents an excessive loss of time by needing to test all materials of a library successively with the mass spectrometer. The reactor design permits, firstly, the integral recording of the entire reactor through a window which is transparent for the corresponding method and, secondly, permits the simultaneous, automated application of a second analytical method (for example mass spectrometry) to selected materials of a material library, which have been rated as active by the optical method. In the case described, the optical method provides information on the material activity for a set problem, and the second analytical method determines the selectivity of the materials.
Abstract translation: 用于通过耦合使用至少两种分析方法，优选IR热成像和质谱法来测试材料库，特别是催化剂的方法和装置。 由于所选择的布置，以前已知的两种方法的缺点得到补偿：通过质谱法对所选部分的随后的选择性测定使得仅针对红外热像仪的论证无效地确定活动; 通过红外热像仪快速综合测定潜在的“良好”材料，可以通过质谱连续测试所有材料，从而防止过多的时间损失。 反应器设计首先通过对于相应方法是透明的窗口整体记录整个反应器，其次允许将第二种分析方法（例如质谱法）同时自动应用于所选择的材料 材料库，通过光学方法被评为有效。 在所描述的情况下，光学方法提供关于集合问题的材料活性的信息，第二分析方法确定材料的选择性。
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Patent Agency Ranking
6.发明授权公开(公告)号：US06765118B2
公开(公告)日：2004-07-20
申请号：US10239409
申请日：2002-09-23
Applicant: Rolf-Hartmuth Fischer , Rolf Pinkos , Stephan Andreas Schunk , Joachim Wulff-Döring
Inventor： Rolf-Hartmuth Fischer , Rolf Pinkos , Stephan Andreas Schunk , Joachim Wulff-Döring
IPC: C07L2700
CPC classification number: C07C29/149 , B01J21/18 , B01J23/36 , B01J23/6567 , B01J23/8896 , C07C2601/18 , C07C31/207 , C07C31/205 , C07C31/133 , C07C31/12
Abstract: In a process for the preparation of alcohols by catalytic hydrogenation of carbonyl compounds, the catalyst used is 0.01 to 50% by weight of rhenium and 0 to 20% by weight, in each case based on the total weight of the catalyst, of at least one further metal chosen from Zn, Cu, Ag, Au, Ni, Fe, Cr, V on oxidatively pretreated activated carbon as support.
Abstract translation: 在通过羰基化合物的催化氢化制备醇的方法中，使用的催化剂为0.01-50重量％的铼和0至20重量％，基于催化剂的总重量，至少为 氧化预处理的活性炭作为载体，选自Zn，Cu，Ag，Au，Ni，Fe，Cr，V中的另一种金属。
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公开(公告)号：US06720171B2
公开(公告)日：2004-04-13
申请号：US09734018
申请日：2000-12-12
Applicant: Stephan Andreas Schunk , Dirk Demuth , Hartmut Hibst
Inventor： Stephan Andreas Schunk , Dirk Demuth , Hartmut Hibst
IPC: C12P2108
CPC classification number: B01J37/02 , B01J19/0046 , B01J35/04 , B01J2219/0052 , B01J2219/00585 , B01J2219/00603 , B01J2219/00659 , B01J2219/00704 , B01J2219/00745 , B01J2219/00747 , C40B30/08 , C40B40/18 , Y10T436/175383 , Y10T436/18 , Y10T436/20 , Y10T436/205831 , Y10T436/25875
Abstract: A process for preparing arrays of two or more heterogeneous catalysts, heterogeneous catalyst precursors, or combinations thereof in a body having preferably parallel through-channels. In this process, a solution, emulsion or dispersion of elements present in the catalyst, catalyst precursor, or combination thereof, is first prepared, and is used to simultaneously or successively coat the channels of the body to produce freshly impregnated moist channels. These channels are then treated and reacted with one or more reactive gases, and the coated body is optionally heated in the presence or absence of inert or reactive gases.
Abstract translation: 一种制备两种或更多种非均相催化剂，非均相催化剂前体或其组合的阵列在具有优选平行通过通道的体内的方法。 在该方法中，首先制备存在于催化剂，催化剂前体或其组合中的元素的溶液，乳液或分散体，并且用于同时或连续地涂覆身体的通道以产生新鲜浸渍的湿通道。 然后将这些通道处理并与一种或多种反应性气体反应，并且涂覆体任选地在存在或不存在惰性或反应性气体的情况下加热。
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公开(公告)号：US06525222B2
公开(公告)日：2003-02-25
申请号：US09729458
申请日：2000-12-05
Applicant: Jan Nouwen , Arthur Höhn , Horst Neuhauser , Frank Funke , Stephan Andreas Schunk , Johann-Peter Melder , Knut Eger , Michael Hesse , Joachim Wulff-Döring
Inventor： Jan Nouwen , Arthur Höhn , Horst Neuhauser , Frank Funke , Stephan Andreas Schunk , Johann-Peter Melder , Knut Eger , Michael Hesse , Joachim Wulff-Döring
IPC: C07C20900
CPC classification number: C07C213/02 , C07C209/26 , C07C2601/08 , C07C2602/08 , C07C2602/10 , C07C211/35 , C07C211/42 , C07C217/58
Abstract: Amines are prepared by reacting aldehydes or ketones at elevated temperature under elevated pressure with nitrogen compounds selected from the group of ammonia, primary and secondary amines, and with hydrogen in the presence of a catalyst, wherein the catalytically active mass of the catalyst contains, after its preparation and before the treatment with hydrogen, 22 to 45% by weight of oxygen-containing compounds of zirconium, calculated as ZrO2, 1 to 30% by weight of oxygen-containing compounds of copper, calculated as CuO, 5 to 50% by weight of oxygen-containing compounds of nickel, calculated as NiO, where the molar ratio of nickel to copper is greater than 1, 5 to 50% by weight of oxygen-containing compounds of cobalt, calculated as CoO, 0 to 5% by weight of oxygen-containing compounds of molybdenum, calculated as MoO3, and 0 to 10% by weight of oxygen-containing compounds of aluminum and/or manganese, calculated as Al2O3 or MnO2.
Abstract translation: 通过使升高的温度下的醛或酮与选自氨，伯和仲胺的氮化合物和在催化剂存在下与氢气反应的醛或酮进行反应来制备胺，其中催化剂的催化活性物质含有 其制备方法和用氢处理之前，按重量计22％至45％的锆的氧含量化合物，按ZrO2计算，按重量计为CuO的含氧化合物为铜，按CuO计为5〜50％ 按NiO计的含镍化合物的重量，其中镍与铜的摩尔比大于1.5至50重量％的以CoO计的含氧化合物的钴，0至5重量％ 按MoO3计算的含氧化合物的钼和0至10重量％的按Al2O3或MnO2计算的含铝和/或锰的含氧化合物。
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公开(公告)号：US08329606B2
公开(公告)日：2012-12-11
申请号：US12735122
申请日：2008-12-16
Applicant: Edo Johann Becker , Evert Jan Ditzel , Harry Kaiser , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
Inventor： Edo Johann Becker , Evert Jan Ditzel , Harry Kaiser , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
CPC classification number: B01J29/06 , B01J29/20 , B01J29/50 , B01J29/65 , B01J29/86 , B01J29/87 , B01J29/88 , B01J29/90 , C07C51/12 , C07C67/37 , Y02P20/584 , C07C53/08 , C07C69/14
Abstract: Process for the in-situ regeneration of a zeolite catalyst in a carbonylation process for the production of at least one of methyl acetate and acetic acid. The process is carried out by (a) contacting a carbonylatable reactant selected from methanol, dimethyl ether and dimethyl carbonate and carbon monoxide in a reactor with a zeolite catalyst and recovering a product stream containing at least one of methyl acetate and acetic acid from the reactor, (b) ceasing contact of the catalyst with the carbonylatable reactant, (c) regenerating the catalyst with a regenerating gas selected from hydrogen or a mixture of hydrogen and carbon monoxide at a temperature in the range 250 to 600 C, and (d) terminating the hydrogen regenerating step and resuming contact of the catalyst with the carbonylatable reactant and carbon monoxide.
Abstract translation: 用于在羰基化方法中原位再生沸石催化剂以生产乙酸甲酯和乙酸中的至少一种的方法。 该方法通过以下步骤进行：（a）在反应器中使沸石催化剂使选自甲醇，二甲醚和碳酸二甲酯的羰基化反应物与一氧化碳接触，并从反应器中回收含有至少一种乙酸甲酯和乙酸的产物流 （b）停止催化剂与可羰基化反应物的接触，（c）在选自氢气或氢气和一氧化碳的混合物中的再生气体在250至600℃的温度范围内再生催化剂，和（d） 终止氢再生步骤并恢复催化剂与可羰基化反应物和一氧化碳的接触。
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公开(公告)号：US20100317888A1
公开(公告)日：2010-12-16
申请号：US12735123
申请日：2008-12-16
Applicant: Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
Inventor： Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
CPC classification number: B01J29/90 , B01J29/20 , B01J38/14 , C07C51/12 , C07C67/37 , Y02P20/584 , C07C53/08 , C07C69/14
Abstract: A process for the carbonylation of dimethyl ether, dimethyl carbonate and/or methanol with carbon monoxide and hydrogen in the presence of a mordenite catalyst to produce at least one of acetic acid and methyl acetate in which process the mordenite catalyst is regenerated in-situ by contacting the catalyst with a regenerating gas comprising a molecular oxygen-containing gas and an inert diluent at a total pressure in the range 1 to 100 bar and wherein the partial pressure of the molecular oxygen-containing gas is such that the temperature of the catalyst is maintained within the range 225 to 325° C.
Abstract translation: 一种在丝光沸石催化剂存在下用一氧化碳和氢气二甲醚，二甲基碳酸酯和/或甲醇羰基化的方法，以产生乙酸和乙酸甲酯中的至少一种，其中丝光沸石催化剂原位再生 使催化剂与包含含分子氧的气体和惰性稀释剂的再生气体在1至100巴的总压力下接触，并且其中分子氧气体的分压使得催化剂的温度为 维持在225至325℃的范围内
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