Device and process for the simultaneous agitation of reaction mixtures
    3.
    发明申请
    Device and process for the simultaneous agitation of reaction mixtures 审中-公开
    用于同时搅拌反应混合物的装置和方法

    公开(公告)号:US20060182667A1

    公开(公告)日:2006-08-17

    申请号:US10543074

    申请日:2004-02-06

    Abstract: The present invention is in the field of the high-throughput research for liquid and multi-phase reactions. Thereby, the invention relates to a process for the simultaneous realization of at least one chemical reaction in at least two separate reaction vessels (10), wherein said process comprises at least the following steps: (i) providing at least one reaction mixture per reaction vessel (10); to (ii) pneumatic agitation of the reaction mixture in at least one reaction vessel by means of bringing the reaction mixture into contact with at least one fluid phase (18), wherein the at least one chemical reaction is carried out in at least one of the reaction vessels (10) in the batch mode and the reaction mixture contains at least one liquid phase (14). Thereby, the fluid phase (18) is supplied to the at least one reaction vessel (10) within a defined period and is at least partially discharged from the reaction vessel. The reaction mixturee may further comprise another immiscible liquid phase (14′) and/or solid phase (16). Furthermore, the present invention relates to the device, which pertains to the process.

    Abstract translation: 本发明在液相和多相反应的高通量研究领域。 因此,本发明涉及在至少两个分离的反应容器(10)中同时实现至少一种化学反应的方法,其中所述方法至少包括以下步骤:(i)每次反应提供至少一种反应混合物 容器(10); (ii)通过使反应混合物与至少一个流化相(18)接触,在至少一个反应容器中气动搅拌反应混合物,其中至少一个化学反应在 分批模式的反应容器(10)和反应混合物含有至少一个液相(14)。 因此,流体相(18)在规定的时间内被供给到至少一个反应容器(10),并且至少部分地从反应容器排出。 反应混合物还可以包含另一个不混溶的液相(14')和/或固相(16)。 此外,本发明涉及与该方法有关的装置。

    Metering Station and Process for Metering Highly Viscous Liquids
    5.
    发明申请
    Metering Station and Process for Metering Highly Viscous Liquids 审中-公开
    计量站和高粘度液体计量流程

    公开(公告)号:US20100300181A1

    公开(公告)日:2010-12-02

    申请号:US12223842

    申请日:2007-02-09

    Abstract: The present invention relates to a metering station (10) which allows liquids with elevated viscosity to be metered, especially liquids with a viscosity which is more than one hundred times the viscosity of water. The metering station is operated partly or fully automatically and has a modular structure. A metering module (1, 1′) comprises at least one plug connecting element (8), with whose aid the metering module (1, 1′) can be made to engage with a corresponding receiving device (9) for the plug connecting element. The plug connecting elements (8) are preferably multifunctional plugs which have at least one fluidic connecting element. In a further preferred embodiment, the plug connecting element (8), in addition to the at least one fluidic connecting element, also has at least one electrical connecting element for process control. The present invention further relates to a process which allows, in a very flexible manner and with a very high throughput, a multitude of (optionally different) components which have an elevated viscosity to be metered into a sampling vessel. The process uses a metering algorithm which is tailored to the high-throughput metering of liquids of elevated viscosity.

    Abstract translation: 本发明涉及一种计量站(10),其允许计量具有高粘度的液体,特别是粘度大于水粘度的百倍的液体。 计量站部分或全部自动运行,并具有模块化结构。 计量模块(1,1')包括至少一个插头连接元件(8),借助于此,可以使计量模块(1,1')与用于插头连接元件的相应接收装置(9)啮合 。 插头连接元件(8)优选是具有至少一个流体连接元件的多功能插头。 在另一优选实施例中,插头连接元件(8)除了至少一个流体连接元件之外,还具有用于过程控制的至少一个电连接元件。 本发明还涉及一种方法,其以非常灵活的方式和非常高的通量允许将具有升高的粘度的许多(任选不同的)组分计量加入到取样容器中。 该过程使用了一种针对高粘度液体的高通量计量量身定制的计量算法。

    Device and method for pressure and flow control in parallel reactors
    6.
    发明申请
    Device and method for pressure and flow control in parallel reactors 有权
    并联反应堆压力和流量控制的装置和方法

    公开(公告)号:US20070148062A1

    公开(公告)日:2007-06-28

    申请号:US10583753

    申请日:2004-12-20

    Abstract: The present invention relates to a method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces. In particular, the invention is suitable for reactions which are not constant volume reactions and/or for reactions in which fluid flows through at least two spatially separated reaction spaces are intended to be controlled together for all the reaction spaces, or for related subsets of them, in the most straightforward way possible. According to one embodiment, the device according to the invention for the parallel study of chemical reactions comprises at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.

    Abstract translation: 本发明涉及用于平行研究至少两个空间分离的反应空间中的化学反应的方法和装置。 特别地,本发明适用于不是恒定的体积反应和/或其中流体流过至少两个空间分离的反应空间的反应旨在一起控制所有反应空间或其相关子集的反应 ,以最直接的方式可能。 根据一个实施方案,根据本发明的用于平行研究化学反应的装置至少包括以下组分:(a)至少两个空间分离的反应空间; (b)在反应空间输入侧,根据(a)的反应空间的至少一种普通的喷射进料; (d)在反应空间输出侧,每个反应空间至少一个连接到所有反应空间或它们的子集共同的至少一个保持气体进料; (e)在反应空间输出侧和根据(d)在产品流动方向上与保持气体进料的连接的下游,每个反应空间至少有一个限制器。

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