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    Substrate coated with a composite film, method for making same and uses thereof
    5.
    发明授权
    Substrate coated with a composite film, method for making same and uses thereof 失效
    用复合膜涂覆的基材，其制造方法及其用途

    公开(公告)号：US07348054B2

    公开(公告)日：2008-03-25

    申请号：US10484721

    申请日：2002-07-25

    申请人： Catherine Jacquiod ,  Jean-Marc Berquier ,  Sophie Besson ,  Jean-Pierre Boilot ,  Christian Ricolleau ,  Thierry Gacoin

    发明人： Catherine Jacquiod ,  Jean-Marc Berquier ,  Sophie Besson ,  Jean-Pierre Boilot ,  Christian Ricolleau ,  Thierry Gacoin

    IPC分类号： B32B3/00

    CPC分类号： C03C17/007 ,  C03C2217/425 ,  C03C2217/45 ,  C03C2217/475 ,  Y10S977/811 ,  Y10T428/249953 ,  Y10T428/249967 ,  Y10T428/249969 ,  Y10T428/24997 ,  Y10T428/24999

    摘要： This substrate is coated with a composite film based on a mesoporous mineral layer containing nanoparticles formed in situ inside the layer. The composite film has a periodic lattice structure over a major portion of the thickness in which the nanoparticles are present, in which structure the nanoparticles are arranged in a periodic manner on the scale of domains of at least 4 periods in the thickness of the film.This structure can be obtained from a mesoporous mineral layer of periodic structure on the scale of domains of at least 4 periods of pores, forming a matrix on the substrate, by: depositing at least one precursor in the pores of the matrix layer; and growing particles derived from the precursor with the spatial distribution and the dimensions being controlled by the structure of the pores of the matrix. Applications to materials for electronics, nonlinear optics and magnetism.

    摘要翻译： 该基底用基于在层内原位形成的纳米颗粒的介孔矿物层的复合膜涂覆。 复合膜在其中存在纳米颗粒的厚度的主要部分上具有周期性晶格结构，其中纳米颗粒以膜的厚度在至少4个周期的范围内以周期性方式排列。 该结构可以从具有至少4个时期的孔的尺度的周期结构的介孔矿物层获得，通过在基质层的孔中沉积至少一种前体，在基底上形成基质; 并且来自前体的生长颗粒的空间分布和尺寸由基质的孔的结构控制。 应用于电子，非线性光学和磁性材料。

    COMPOSITION FOR HYDROPHOBIC TREATMENT AND GLAZING
    6.
    发明申请
    COMPOSITION FOR HYDROPHOBIC TREATMENT AND GLAZING 有权
    组合物用于水处理和玻璃化

    公开(公告)号：US20090324968A1

    公开(公告)日：2009-12-31

    申请号：US12307927

    申请日：2007-07-10

    申请人： Arnaud Huignard ,  Khalid Lahlil ,  Sandrine Ithurria ,  Thierry Gacoin ,  Jean-Pierre Boilot

    发明人： Arnaud Huignard ,  Khalid Lahlil ,  Sandrine Ithurria ,  Thierry Gacoin ,  Jean-Pierre Boilot

    IPC分类号： B32B17/06 ,  C09D5/00

    CPC分类号： C07F7/0836 ,  C07F7/0838 ,  Y10T428/31612 ,  Y10T428/31663

    摘要： Hydrophobic treatment composition comprising one or more compounds, as a mixture, corresponding to the formula in which at least one R is a CaF2a+1 group, a being an integer, it being possible for another R to be an SiX3-bRCb1 group, b being 0, 1 or 2X being a hydrolysable group, such as alkoxy, hydroxyl or halo R1 being a hydrocarbon group, such as lower alkyl S is a hydrogen atom, an OH group, an alkyl group, in particular a lower alkyl group, such as CH3, or an OSiR2R3R4 group, R2, R3 and R4 being identical or different and consisting in particular of one of the abovementioned groups carried by an Si atom, such as (CH2)2—R, a hydrogen atom, an alkyl group or OSIR2R3R4, n is an integer≧1, the total number of Si atoms not exceeding 20. Process for treatment by this composition.Hydrophobic glass substrate thus obtained and its application, in particular as glazing.

    摘要翻译： 疏水性处理组合物，其包含一种或多种化合物，作为混合物，其中至少一个R为CaF 2 a + 1基团，a为整数，另外R为SiX 3-bRC b 1基团的式 0或1或2个X为可水解基团，例如烷氧基，羟基或卤素R 1为烃基，例如低级烷基S为氢原子，OH基团，烷基，特别是低级烷基， 例如CH 3或OSiR 2 R 3 R 4基团，R 2，R 3和R 4相同或不同，特别由上述基团之一由Si原子例如（CH 2）2 -R，氢原子，烷基 或OSIR2R3R4，n为整数> = 1，Si原子总数不超过20.用该组合物处理的方法。 这样得到的疏水玻璃基板及其应用，特别是玻璃。

    Method of Producing a Substrate Which is Coated With a Mesoporous Layer and Use Thereof in Ophthalmic Optics
    7.
    发明申请
    Method of Producing a Substrate Which is Coated With a Mesoporous Layer and Use Thereof in Ophthalmic Optics 有权
    产生介孔层的基板的制造方法及其在眼科用途中的应用

    公开(公告)号：US20080079894A1

    公开(公告)日：2008-04-03

    申请号：US11573137

    申请日：2005-05-03

    申请人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    发明人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    IPC分类号： C08J7/04 ,  G02C7/02

    CPC分类号： C09D183/04 ,  C09D183/02

    摘要： The invention relates to a method of producing a substrate which is coated with a mesoporous layer and to the use thereof in ophthalmic optics. The inventive method comprises the following steps consisting in: preparing a precursor sol containing (i) a precursor agent that is selected from compounds having formula M(X)4 (I), in which X is a hydrolysable group and M represents silicon or a tetravalent metal and mixtures thereof, (ii) at least one organic solvent, (iii) at least one pore-forming agent and (iv) water; depositing a film of the precursor sol on a main surface of the substrate; optionally consolidating the mesoporous structure of the deposited film; eliminating the pore-forming agent; and recovering the substrate coated with the mesoporous layer. The method is characterized in that: (i) the pore-forming agent is eliminated at a temperature of less than or equal to 150° C.; and (ii) the method comprises a step involving the introduction of at least one reactive agent bearing at least one hydrophobic group, before the deposition step (b) and/or after said step.

    摘要翻译： 本发明涉及一种制造涂覆有介孔层的基材的方法及其在眼科光学中的用途。 本发明的方法包括以下步骤：制备前体溶胶，所述前体溶胶含有（i）选自具有式M（X）4（I）的化合物的前体试剂，其中X是可水解基团，M代表硅或 四价金属及其混合物，（ii）至少一种有机溶剂，（iii）至少一种成孔剂和（iv）水; 在所述基板的主表面上沉积所述前体溶胶的膜; 可选地固结沉积膜的介孔结构; 消除造孔剂; 并回收涂有介孔层的基材。 该方法的特征在于：（i）在小于或等于150℃的温度下除去成孔剂; 和（ii）该方法包括在沉积步骤（b）和/或所述步骤之后引入至少一种带有至少一个疏水基团的反应剂的步骤。

    Method of producing a substrate which is coated with a mesoporous layer and use thereof in ophthalmic optics
    8.
    发明授权
    Method of producing a substrate which is coated with a mesoporous layer and use thereof in ophthalmic optics 有权
    制备涂覆有介孔层的基材的方法及其在眼科光学中的用途

    公开(公告)号：US08182866B2

    公开(公告)日：2012-05-22

    申请号：US11573137

    申请日：2005-05-03

    申请人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    发明人： Muriel Matheron ,  John Biteau ,  Jean-Paul Cano ,  Jean-Pierre Boilot ,  Thierry Gacoin

    IPC分类号： B05D5/06 ,  C09D183/02 ,  C09D183/04 ,  G02B1/04

    CPC分类号： C09D183/04 ,  C09D183/02

    摘要： The invention relates to a method of producing a substrate which is coated with a mesoporous layer and to the use thereof in ophthalmic optics. The inventive method comprises the following steps comprising: preparing a precursor sol containing (i) a precursor agent that is selected from compounds having formula M(X)4 (I), in which X is a hydrolysable group and M represents silicon or a tetravalent metal and mixtures thereof, (ii) at least one organic solvent, (iii) at least one pore-forming agent and (iv) water; depositing a film of the precursor sol on a main surface of the substrate; optionally consolidating the mesoporous structure of the deposited film; eliminating the pore-forming agent; and recovering the substrate coated with the mesoporous layer. The method is characterized in that: (i) the pore-forming agent is eliminated at a temperature of less than or equal to 150° C.; and (ii) the method comprises a step involving the introduction of at least one reactive agent bearing at least one hydrophobic group, before the deposition step and/or after said step.

    摘要翻译： 本发明涉及一种制造涂覆有介孔层的基材的方法及其在眼科光学中的用途。 本发明的方法包括以下步骤：制备前体溶胶，该前体溶胶含有（i）选自具有式M（X）4（I）的化合物的前体试剂，其中X是可水解基团，M代表硅或四价 金属及其混合物，（ii）至少一种有机溶剂，（iii）至少一种造孔剂和（iv）水; 在所述基板的主表面上沉积所述前体溶胶的膜; 可选地固结沉积膜的介孔结构; 消除造孔剂; 并回收涂有介孔层的基材。 该方法的特征在于：（i）在小于或等于150℃的温度下除去成孔剂; 和（ii）该方法包括在沉积步骤之前和/或在所述步骤之后引入至少一种带有至少一个疏水基团的活性剂的步骤。