Preparation of aqueous medium suitable for preparing microcapsules
    4.
    发明授权
    Preparation of aqueous medium suitable for preparing microcapsules 失效
    适用于制备微胶囊的水性介质的制备

    公开(公告)号:US4349454A

    公开(公告)日:1982-09-14

    申请号:US115915

    申请日:1980-01-28

    摘要: A hydrophobic organic solvent containing a compound of the formula ##STR1## is dispersed and emulsified in an aqueous medium containing a sulfinic acid of the formulaR.sub.5 --SO.sub.2 H (I)and serving as an aqueous medium for preparing microcapsules to react the compounds of the formulae (I) and (II) and synthesize a diarylmethane derivative of the formula ##STR2## while encapsulating oily droplets of the resulting hydrophobic organic solvent solution of the diarylmethane derivative. Colorless chromogenic materials can be synthesized and encapsulated at the same time by this process.

    摘要翻译: 将含有式(II)化合物的疏水性有机溶剂分散并乳化在含有式R 5 -SO 2 H(I)的亚磺酸的水性介质中,并用作制备微胶囊以使化合物 的式(I)和(II)的化合物,并合成式(III)的二芳基甲烷衍生物,同时包封所得的二芳基甲烷衍生物的疏水性有机溶剂溶液的油滴。 无色发色材料可以通过该方法同时合成和包封。

    Heat-sensitive recording material
    5.
    发明授权
    Heat-sensitive recording material 失效
    热敏记录材料

    公开(公告)号:US4226912A

    公开(公告)日:1980-10-07

    申请号:US9083

    申请日:1979-02-02

    IPC分类号: B41M5/327 B41M5/18

    摘要: The black color developing heat-sensitive recording material comprises a base sheet and a color developing layer formed on at least one surface of the base sheet, the color developing layer including colorless or light-colored chromogenic material and acceptor which is reactive with said chromogenic material to develop a black color. At least 60% by weight of the chromogenic material comprises at least two kinds of black color developing fluoran compounds having the eneral formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, X.sub.l and Ym are described hereinafter and the amount of each of said black color developing fluoran compounds is not larger than 90% by weight of the total amount of said black color developing fluoran compounds.

    摘要翻译: 黑色显影热敏记录材料包括基片和形成在基片的至少一个表面上的彩色显影层,彩色显影层包括无色或浅色显色材料和与所述显色材料反应的受体 开发黑色。 至少60重量%的显色材料包含至少两种具有下式的R 1,R 2,R 3,R 4,R 5,R 6,X 1和Y m的具有下式的R 1,R 2,R 3,R 4,R 5,R 6,X 1和Y m的具有下式的黑色显色荧烷化合物, 的所述黑色显影性荧烷化合物的比例不大于所述黑色显影性荧烷化合物总量的90重量%。

    Chromogenic compounds and method for preparation thereof
    9.
    发明授权
    Chromogenic compounds and method for preparation thereof 失效
    显色化合物及其制备方法

    公开(公告)号:US3970671A

    公开(公告)日:1976-07-20

    申请号:US491133

    申请日:1974-07-23

    摘要: Chromogenic compounds for use in pressure sensitive recording sheets represented by the formula: ##SPC1##Are disclosed, wherein R.sub.1 and R.sub.2 are independently, hydrogen substituted or unsubstituted lower alkyl, aliphatic acyl, phenyl substituted aliphatic acyl, benzoyl, aralky, phenyl (the benzene nuclei of those substituents may be further substituted by chlorine, bromine, lower alkyl, lower alkoxy or nitro), allyl, allyl substituted by lower alkyl or phenyl, propargyl, or propargyl substituted by lower alkyl or a phenyl; R.sub.3 and R.sub.4 are independently lower alkyl, benzyl and phenyl (the benzene nuclei or those substiutents may be further substituted by chlorine, bromine, lower alkyl or lower alkoxy), either R.sub.1 or R.sub.2 being other than hydrogen when R.sub.3 and R.sub.4 are both ethyl groups.

    摘要翻译: 用于由下式表示的压敏记录片材的显色化合物: