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    Thermal break systems
    1.
    发明授权
    Thermal break systems 失效
    热断裂系统

    公开(公告)号：US5137788A

    公开(公告)日：1992-08-11

    申请号：US410211

    申请日：1989-09-21

    申请人： Jan L. R. Clatty ,  Neil H. Nodelman ,  Robert M. Loring ,  Michael F. Palmosina, II

    发明人： Jan L. R. Clatty ,  Neil H. Nodelman ,  Robert M. Loring ,  Michael F. Palmosina, II

    IPC分类号： C08G18/48 ,  C08G18/65 ,  C08G18/66

    CPC分类号： C08G18/482 ,  C08G18/6511 ,  C08G18/6674 ,  C08G2130/00 ,  Y10T428/31551 ,  Y10T428/31678

    摘要： Homogeneous storable mixtures containing small quantities of a potassium halide, having a high mixed hydroxyl number or mixed hydroxyl/amine number and an average functionality of at least 2.0 are made by mixing (a) a polyoxyalkylene polyol and/or polyolamine and/or polyamine based on an alkyloxirane having a molecular weight of from 400 to 12,000 and (b) a low molecular weight polyol which is not completely miscible with (a) wherein these mixtures are reacted with a prepolymer or a polyisocyanate to produce shrink stable thermal break urethanes having good adhesion to substrate properties and wherein the use of such mixtures increases processing flexibility without detrimentally affecting the physical properties of the thermal break urethanes produced.

    摘要翻译： 通过混合（a）聚氧化烯多元醇和/或多元胺和/或多胺基，制备含有少量卤化钾，具有高混合羟基数或混合羟基/胺数，平均官能度至少为2.0的均匀的可储存混合物 在分子量为400至12,000的烷基环氧乙烷上和（b）与（a）不完全混溶的低分子量多元醇，其中这些混合物与预聚物或多异氰酸酯反应以产生具有良好的收缩稳定的热断裂氨基甲酸酯 与基材性质的粘合性，并且其中使用这种混合物增加了加工柔性，而不会有害地影响所生产的热断裂聚氨酯的物理性能。

    High modulus, high impact polyurethane/polyurea RIM
    2.
    发明授权
    High modulus, high impact polyurethane/polyurea RIM 失效
    高模量，高抗冲聚氨酯/聚脲RIM

    公开(公告)号：US5668239A

    公开(公告)日：1997-09-16

    申请号：US657512

    申请日：1996-06-04

    申请人： Neil H. Nodelman ,  David D. Steppan ,  Jan L. R. Clatty ,  A. Donald Meltzer

    发明人： Neil H. Nodelman ,  David D. Steppan ,  Jan L. R. Clatty ,  A. Donald Meltzer

    IPC分类号： C08G18/10 ,  C08G18/16 ,  C08G18/75 ,  C08G18/80

    CPC分类号： C08G18/8038 ,  C08G18/10 ,  C08G18/16 ,  C08G18/758 ,  C08G18/8032 ,  C08G2120/00

    摘要： This invention relates to a process for the production of polyurethane/urea moldings which exhibit both high flexural modulus and high impact strength. The process comprises reaction injection molding of a reaction mixture in the presence of a catalyst via the one-shot process. The isocyanate component of this invention is a prepolymer of methylenebis(cyclohexyl isocyanate) having an NCO content of 12-27%, an average isocyanate functionality of less than 2.3, a monomer content of greater than about 25% by weight, and containing urethane or urea groups. The isocyanate-reactive blend comprises a high molecular weight polyether polyol and a low molecular weight chain extender, wherein the isocyanate-reactive blend has an OH:NH equivalent ratio of from 1:1 to 15:1. This invention also relates to the polyurethane/urea molded article produced by the above process.

    摘要翻译： 本发明涉及生产具有高弯曲模量和高冲击强度的聚氨酯/尿素模塑制品的方法。 该方法包括通过一步法在催化剂存在下反应注射成型反应混合物。 本发明的异氰酸酯组分是NCO含量为12-27％，平均异氰酸酯官能度小于2.3，单体含量大于约25重量％的亚甲基双（环己基异氰酸酯）的预聚物，并含有氨基甲酸酯或 尿素组。 异氰酸酯反应性共混物包含高分子量聚醚多元醇和低分子量扩链剂，其中异氰酸酯反应性共混物的OH:NH当量比为1:1至15:1。 本发明还涉及通过上述方法制备的聚氨酯/尿素模塑制品。

    Aliphatic rim elastomers
    3.
    发明授权
    Aliphatic rim elastomers 失效
    脂肪族边缘弹性体

    公开(公告)号：US5502147A

    公开(公告)日：1996-03-26

    申请号：US171282

    申请日：1993-12-21

    申请人： Neil H. Nodelman ,  David D. Steppan ,  Albert Magnotta ,  Robert M. Loring ,  Richard E. Keegan ,  William E. Slack

    发明人： Neil H. Nodelman ,  David D. Steppan ,  Albert Magnotta ,  Robert M. Loring ,  Richard E. Keegan ,  William E. Slack

    IPC分类号： C08G18/16 ,  C08G18/65 ,  C08G18/73 ,  C08G18/75 ,  C08G18/78 ,  C08G18/79 ,  C08G18/18

    CPC分类号： C08G18/6505 ,  C08G18/78 ,  C08G18/79 ,  C08G2120/00

    摘要： The present invention is directed to polyurethane moldings produced via the RIM process. These polyurethane moldings have excellent reactivity, demold properties (at a 30 s demold), and good elongation and tear strength, and comprise the reaction product of an aliphatic polyisocyanate having a viscosity of less than about 20,000 mPa.multidot.s at 25.degree. C. and a NCO functionality of 2.3 to 4.0 with an isocyanatereactive component comprising b1) a relatively high molecular weight organic compound containing at least one of the groups selected from the group consisting of hydroxy groups and amine groups; and b2) a low molecular weight chain extender selected from the group consisting of diols, triols, primary amines, secondary amines, aminoalcohols, and mixtures thereof; in the presence of a catalyst. The OH:NH ratio of the chain extender is from 1:1 to 25:1.

    摘要翻译： 本发明涉及通过RIM工艺生产的聚氨酯模制品。 这些聚氨酯模制品具有优异的反应性，脱模性（30秒脱模）和良好的伸长率和撕裂强度，并且包括在25℃下具有小于约20,000mPax的粘度的脂族多异氰酸酯与NCO的反应产物 具有异氰酸酯反应性组分的2.3至4.0的官能度包含：b1）含有至少一种选自羟基和胺基的基团的相对高分子量的有机化合物; 和b2）选自二醇，三醇，伯胺，仲胺，氨基醇及其混合物的低分子量增链剂; 在催化剂存在下。 扩链剂的OH:NH比为1:1至25:1。

    Process for the production of molded products using internal mold release agents
    6.
    发明授权
    Process for the production of molded products using internal mold release agents 失效

    公开(公告)号：US4868224A

    公开(公告)日：1989-09-19

    申请号：US260650

    申请日：1988-10-21

    申请人： Stephen J. Harasin ,  Michael F. Hurley ,  Timothy J. Kelly ,  Kenneth J. Naleppa ,  Neil H. Nodelman ,  Donald W. Schumacher ,  Gregory H. Slocum ,  David F. Sounik

    发明人： Stephen J. Harasin ,  Michael F. Hurley ,  Timothy J. Kelly ,  Kenneth J. Naleppa ,  Neil H. Nodelman ,  Donald W. Schumacher ,  Gregory H. Slocum ,  David F. Sounik

    IPC分类号： C08G18/50 ,  C08G18/80 ,  C08K5/098

    CPC分类号： C08G18/8051 ,  C08G18/5024 ,  C08K5/098

    摘要： The present invention is directed to a process for producing a molded product comprising(A) reacting:(i) an organic polyisocyanate having an isocyanate group content of from 5 to 45% by weight, preferably from 15 to 35% by weight, and most preferably from 20 to 35% by weight, prepared by reacting:(a) an organic di- and/or polyisocyanate, and(b) an active hydrogen containing fatty acid ester prepared by reacting an alcohol or polyol with an aliphatic, saturated or unsaturated fatty acid, said ester being characterized in that at least one aliphatic acid which contains more than 8 carbon atoms is built into the molecule, said ester further characterized as having an acid number of from 0 to 100 and a hydroxyl number of from 0 to 150 with at least one of said numbers being greater than zero, said ester having an average molecular weight of from 500 to 5000,(ii) an isocyanate reactive component comprising:(a) from about 0.5 to about 10% by weight based on the weight of components (ii)(b) and (ii)(c), of a zinc carboxylate containing from 8 to 24 carbon atoms per carboxylate group,(b) from about 0.3 to 100% by weight, preferably from 0.5 to 95% by weight, more preferably from 5 to 45% by weight, and most preferably from 10 to 35% by weight, based on the weight of components (ii)(b) and (ii)(c), of a compatibilizer which compatibilizes said carboxylate in component (ii), and(c) 0 to about 99.5% by weight, preferably from 5 to 99.5% by weight, more preferably from 55 to 95% by weight, and most preferably from 65 to 90% by weight, based on the weight of components (ii)(b), and (ii)(c), of at least one active hydrogen containing compound other than said compatibilizer,at an isocyanate index of from about 90 to about 400 and preferably from about 95 to about 115, in a closed mold,(B) allowing the components to react, and(C) removing the product from the mold.

    High solids polyester polyols
    7.
    发明授权
    High solids polyester polyols 失效
    高固含量聚酯多元醇

    公开(公告)号：US4859791A

    公开(公告)日：1989-08-22

    申请号：US21106

    申请日：1987-03-03

    申请人： Neil H. Nodelman ,  Robert G. Kelso

    发明人： Neil H. Nodelman ,  Robert G. Kelso

    IPC分类号： C07C69/80 ,  C08G63/20

    CPC分类号： C07C69/80 ,  C08G63/20

    摘要： The present invention is directed to a polyester polyol having a molecular weight between about 850 and 2000, a functionality of about 5 to 9 and an OH number of about 200 to 350, based on 100% solids, which is prepared by reacting(a) an acid component based on at least one polyfunctional cycloaliphatic or aromatic carboxylic acid, anhydride or ester and optionally up to about 50 percent by weight of at least one acyclic, polyfunctional carboxylic acid and(b) a hydroxyl component containing at least a portion of at least one polyol having a functionality of at least 3.The present invention is also directed to a process for preparing these polyester polyols by reacting the above components and is further directed to the use of these polyester polyols in combination with organic polyisocyanates for the production of polyurethanes, particularly polyurethane coatings.

    摘要翻译： 本发明涉及一种聚酯多元醇，其分子量为约850至2000，官能度为约5至9，OH数为约200至350，基于100％固体，其通过使（a） 基于至少一种多官能脂环族或芳族羧酸，酸酐或酯的酸组分，和任选地至多约50重量％的至少一种无环多官能羧酸，和（b）含有至少一部分 至少一种官能度至少为3的多元醇。本发明还涉及通过使上述组分反应制备这些聚酯多元醇的方法，并且还涉及这些聚酯多元醇与有机多异氰酸酯的组合用于制备 聚氨酯，特别是聚氨酯涂料。

    Production of polyurethane moldings by the reaction injection molding process
    8.
    发明授权
    Production of polyurethane moldings by the reaction injection molding process 失效
    通过反应注塑成型工艺生产聚氨酯模塑制品

    公开(公告)号：US4792576A

    公开(公告)日：1988-12-20

    申请号：US76827

    申请日：1987-07-23

    申请人： Neil H. Nodelman

    发明人： Neil H. Nodelman

    IPC分类号： C08G18/38 ,  C08G18/66 ,  C08J9/04 ,  B29C45/14 ,  C08G18/28

    CPC分类号： C08G18/6666 ,  C08G18/3823 ,  C08G18/6674 ,  C08G2120/00 ,  C08G2130/00 ,  Y10S264/83

    摘要： The present invention is directed to a process for the production of polyurethane moldings by reacting a reaction mixture comprising(a) an organic polyisocyanate(b) a compatible polyol blend comprising(i) at least one polyether polyol having an hydroxyl functionality of from 2 to 8, and a molecular weight of from 350 to below 1800, and(ii) at least one hydroxyl functional organic material containing from 2 to 8 hydroxyl groups and having a molecular weight below 350, components (i) and (ii) being used in a weight ratio of component (b)(i) to (b)(ii) of from about 10:1 to about 1:10, and(iii) no more than 45% by weight based on the weight of component (b) of an active hydrogen containing compound having a molecular weight of 1800 or more,said reaction mixture being processed as a one-shot system by the RIM process at an isocyanate index of from about 70 to about 130.

    摘要翻译： 本发明涉及通过使包含（a）有机多异氰酸酯（b）相容的多元醇共混物的反应混合物反应生产聚氨酯模制品的方法，所述共混物包含（i）至少一种具有2个羟基官能团的聚醚多元醇2 8，分子量为350至1800以下，和（ii）至少一种羟基官能有机材料，其含有2至8个羟基并且分子量低于350，组分（i）和（ii）用于 组分（b）（i）至（b）（ii）的重量比为约10:1至约1:10，和（iii）基于组分（b）的重量计不超过45重量％ 的分子量为1800或更高的含活性氢的化合物，所述反应混合物通过RIM方法以约70至约130的异氰酸酯指数作为单次注射系统加工。