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1.发明授权Process for preparing biaryl compounds via coupling of an arylamine with an arene 失效通过芳基胺与芳烃的偶联制备联芳基化合物的方法
公开(公告)号：US4542233A
公开(公告)日：1985-09-17
申请号：US515498
申请日：1983-07-20
申请人： Oreste Piccolo , Aldo Belli , Giovanni Villa , Enrico Zen , Attilio Citterio
发明人： Oreste Piccolo , Aldo Belli , Giovanni Villa , Enrico Zen , Attilio Citterio
IPC分类号： C07C69/65 , B01J23/72 , B01J31/00 , B01J31/02 , C07B31/00 , C07B37/04 , C07B61/00 , C07C17/00 , C07C17/26 , C07C17/263 , C07C25/18 , C07C51/00 , C07C51/353 , C07C51/377 , C07C57/58 , C07C67/00 , C07C67/333 , C07C201/00 , C07C201/12 , C07C205/06 , C07C67/343 , C07C2/68 , C07C37/14 , C07C41/18 , C07C45/69 , C07C76/02 , C07C120/00 , C07C148/00
CPC分类号： C07C17/263 , C07C201/12 , C07C51/377
摘要： Improvement in the process for preparing biaryl compounds via coupling of an arylamine with an arene in the presence of a nitrite, an acid and copper metal or a derivative thereof; the improvement is consisting in adding to the reaction mixture a trialkylorthoformate. The process may be used for preparing drugs such as Flurbiprofen and Xenbucin or intermediate compounds particularly useful for preparing Flurbiprofen, Flufenisal, Chlordimorin, Xenbucin, Xenysalate, Xenyhexenic acid and the like.
摘要翻译： 在亚硝酸盐，酸和铜金属或其衍生物的存在下，通过芳基胺与芳烃的偶合制备联芳基化合物的方法的改进; 改进之处在于向反应混合物中加入三烷基酯酸酯。 该方法可用于制备药物，例如氟比洛芬和Xenbucin或特别适用于制备氟比洛芬，氟芬尼，勒立莫宁，Xenbucin，Xenysalate，Xenyhexenic acid等药物。
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2.发明授权Process for the preparation of arylalkanoic acids by oxidative rearrangement of arylalkanones 失效通过芳基链烷酮的氧化重排制备芳基链烷酸的方法
公开(公告)号：US4608441A
公开(公告)日：1986-08-26
申请号：US754538
申请日：1985-07-12
申请人： Attilio Citterio , Laura Tinucci , Aldo Belli , Lucio Filippini
发明人： Attilio Citterio , Laura Tinucci , Aldo Belli , Lucio Filippini
IPC分类号： C07C51/00 , C07C65/11 , C07D333/24
摘要： Process for preparing an arylalkanoic acid by adding iodine to a mixture of an arylalkanone and an excess of an orthoester, heating of the mixture thus obtained, adding an inorganic base and finally an acid.
摘要翻译： 通过向芳基酮和过量原酸酯的混合物中加入碘制备芳基链烷酸的方法，加热所得混合物，加入无机碱，最后加入酸。
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公开(公告)号：US08766003B2
公开(公告)日：2014-07-01
申请号：US13702223
申请日：2011-06-09
申请人： Attilio Citterio , Elisa Battistini , Davide Belnome , Federica Buonsanti , Luciano Lattuada , Gabriella Leonardi , Fulvio Uggeri , Evelin Vignale , Massimo Visigalli
发明人： Attilio Citterio , Elisa Battistini , Davide Belnome , Federica Buonsanti , Luciano Lattuada , Gabriella Leonardi , Fulvio Uggeri , Evelin Vignale , Massimo Visigalli
IPC分类号： C07C231/12 , C07C231/14 , C07B39/00
CPC分类号： C07B39/00 , C07C231/10 , C07C231/12 , C07C231/14 , C07C235/48 , C07C237/46
摘要： The present invention relates to a process for the preparation of iodinated phenols; in particular; it relates to a process including the direct iodination, with suitably activated iodine, of 3,5-disubstituted phenol compounds to the corresponding 3,5-disubstituted-2,4,6-triiodophenols, which are useful intermediates for the synthesis of x-ray contrast media, and to the preparation of the contrast media themselves.
摘要翻译： 本发明涉及一种制备碘化酚的方法; 尤其是; 它涉及一种方法，包括将适当活化的碘直接碘化为3,5-二取代的苯酚化合物与相应的3,5-二取代-2,4,6-三碘苯酚的有用的中间体， 射线造影剂，以及造影剂本身的制备。
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公开(公告)号：US20130072719A1
公开(公告)日：2013-03-21
申请号：US13702223
申请日：2011-06-09
申请人： Attilio Citterio , Elisa Battistini , Davide Belnome , Federica Buonsanti , Luciano Lattuada , Gabriella Leonardi , Fulvio Uggeri , Evelin Vignale , Massimo Visigalli
发明人： Attilio Citterio , Elisa Battistini , Davide Belnome , Federica Buonsanti , Luciano Lattuada , Gabriella Leonardi , Fulvio Uggeri , Evelin Vignale , Massimo Visigalli
IPC分类号： C07B39/00 , C07C231/14 , C07C231/12
CPC分类号： C07B39/00 , C07C231/10 , C07C231/12 , C07C231/14 , C07C235/48 , C07C237/46
摘要： The present invention relates to a process for the preparation of iodinated phenols; in particular; it relates to a process including the direct iodination, with suitably activated iodine, of 3,5-disubstituted phenol compounds to the corresponding 3,5-disubstituted-2,4,6-triiodophenols, which are useful intermediates for the synthesis of x-ray contrast media, and to the preparation of the contrast media themselves.
摘要翻译： 本发明涉及一种制备碘化酚的方法; 尤其是; 它涉及一种方法，包括将适当活化的碘直接碘化为3,5-二取代的苯酚化合物与相应的3,5-二取代-2,4,6-三碘苯酚的有用的中间体， 射线造影剂，以及造影剂本身的制备。
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公开(公告)号：US20060155077A1
公开(公告)日：2006-07-13
申请号：US10534545
申请日：2002-12-12
IPC分类号： C08C19/00
CPC分类号： C08K5/19 , B60C1/0016 , C08L21/00 , C08L2666/06 , C08L2666/08
摘要： A crosslinkable elastomeric composition includes at least one diene elastomeric polymer and at least one organic quaternary ammonium salt. The at least one diene elastomeric polymer may have a glass transition temperature (Tg) below 20° C. The at least one organic quaternary ammonium salt may be present in an amount from 0.1 phr to 10 phr. The elastomeric composition may include at least one primary accelerator selected from thiazoles, sulphenamides, and/or xanthogenates. The elastomeric composition may be substantially free of additional secondary accelerators. The elastomeric composition may include at least one reinforcing filler, such as carbon black and/or silica. A tyre for a vehicle wheel includes at least one structural element including the elastomeric composition. The tyre may include a carcass structure, a belt structure, a tread band, and a pair of sidewalls. The at least one structural element including the elastomeric composition may be the tread band.
摘要翻译： 可交联的弹性体组合物包括至少一种二烯弹性体聚合物和至少一种有机季铵盐。 所述至少一种二烯弹性体聚合物可以具有低于20℃的玻璃化转变温度（T g）。所述至少一种有机季铵盐可以以0.1phr至10phr的量存在。 弹性体组合物可以包括至少一种选自噻唑，噻吩酰胺和/或黄原酸酯的主促进剂。 弹性体组合物可以基本上不含附加的二次加速剂。 弹性体组合物可以包括至少一种增强填料，例如炭黑和/或二氧化硅。 用于车轮的轮胎包括至少一个包括弹性体组合物的结构元件。 轮胎可以包括胎体结构，带结构，胎面带和一对侧壁。 包括弹性体组合物的至少一个结构元件可以是胎面带。
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6.发明授权Methods for surface modification of silica for use in capillary zone electrophoresis and chromatography 失效用于毛细管区带电泳和色谱法的二氧化硅表面改性方法公开(公告)号：US06776911B2
公开(公告)日：2004-08-17
申请号：US10069567
申请日：2002-07-03
IPC分类号： B01D1508
CPC分类号： G01N27/44752
摘要： The present invention refers to the use of novel molecules able to bind tenaciously to silica, borosilicate and silicate surfaces, and thus to modify their properties and characteristics. When applied to silica-based chromatography, it offers important advantages in all cases in which it is necessary to modulate the interaction of analytes with the stationary phase. In capillary zone electrophoresis (CZE), such compounds will eliminate or invert the electroendoosmostic (EEO) flow, greatly simplifying the analysis of negatively-charged compounds and permitting the analysis of bio(macro)molecules via the direct use of naked capillaries.
摘要翻译： 本发明涉及能够牢固地结合二氧化硅，硼硅酸盐和硅酸盐表面，从而改变其性质和特性的新型分子的用途。 当应用于二氧化硅基色谱时，它在所有需要调节分析物与固定相的相互作用的情况下提供重要的优点。 在毛细管区带电泳（CZE）中，这种化合物将消除或反转电活性（EEO）流，大大简化了带负电荷的化合物的分析，并允许通过直接使用裸露毛细管分析生物（宏观）分子。
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公开(公告)号：US5175318A
公开(公告)日：1992-12-29
申请号：US866108
申请日：1992-04-07
申请人： Francesco Minisci , Attilio Citterio , Elena Vismara , Silvia De Bernardinis , Carlo Neri , Luciano Pallini , Mariano Correale
发明人： Francesco Minisci , Attilio Citterio , Elena Vismara , Silvia De Bernardinis , Carlo Neri , Luciano Pallini , Mariano Correale
摘要： Phenols are oxidated to quinones with hydrogen peroxide in the presence of catalytic amounts of bromine, iodine, hydrogen bromide and hydrogen iodide.
摘要翻译： 在催化量的溴，碘，溴化氢和碘化氢的存在下，苯酚用过氧化氢氧化成醌。
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公开(公告)号：US20090178748A1
公开(公告)日：2009-07-16
申请号：US11988143
申请日：2005-07-01
申请人： Francesca Baione , Luigi Fino , Maurizio Galimberti , Luca Giannini , Attilio Citterio , Marco Martino
发明人： Francesca Baione , Luigi Fino , Maurizio Galimberti , Luca Giannini , Attilio Citterio , Marco Martino
CPC分类号： B29D30/0681 , B29D30/0602 , B29D2030/0682 , B60C1/00 , B60C1/0008 , Y10T152/10765
摘要： Process for manufacturing tires includes the following steps: forming at least one layer including a crosslinkable elastomeric material on an outer surface of a toroidal support the shape of which substantially matches that of the inner surface of the tire; manufacturing a green tire on the toroidal support bearing the at least one layer, the green tire including at least one structural element including a crosslinkable elastomeric material; wherein one crosslinkable elastomeric material of the at least one layer includes a crosslinkable elastomeric composition including at least one sulfur-curable elastomeric polymer and at least one compound having the following general formula (I): A-(S)p—B wherein: p is an integer of 2 to 10; and A and B, which may be the same or different from each other, represent a group having the following general formula (II):
摘要翻译： 用于制造轮胎的方法包括以下步骤：在环形支撑件的外表面上形成包括可交联弹性体材料的至少一层，其形状基本上与轮胎的内表面的形状匹配; 在承载所述至少一个层的所述环形支撑件上制造生胎，所述生胎包括至少一个包括可交联弹性体材料的结构元件; 其中所述至少一层的一种可交联弹性体材料包括可交联的弹性体组合物，其包含至少一种可硫化的弹性体聚合物和至少一种具有以下通式（I）的化合物：A-（S）pB其中：p是 2〜10的整数; 和A和B可以相同或不同，表示具有以下通式（II）的基团：
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公开(公告)号：US07018433B2
公开(公告)日：2006-03-28
申请号：US10169869
申请日：2001-01-09
CPC分类号： C10L1/1905 , C10L1/1985 , C10L1/328 , C10M129/95 , C10M2209/104 , C10M2209/105 , C10N2230/24 , C10N2250/02 , C10M2209/108 , C10M2209/109
摘要： A fuel of an emulsion between water and a liquid hydrocarbon. The emulsion is stabilized by adding a polymeric surfactant obtainable by reaction between: (i) a polyolefin oligomer functionalized with at least one group deriving from a dicarboxylic acid, or a derivative thereof; and (ii) a polyoxyalkylene of linear oxyalkylene units. The polyoxyalkylene is linked to a long-chain alkyl group optionally containing one or more ethylenic unsaturations. The fuel has high stability over time, without forming carbonaceous deposits which adhere to metal surfaces.
摘要翻译： 水与液态碳氢化合物之间的乳液燃料。 通过加入通过以下反应获得的聚合物表面活性剂来稳定乳液：（i）用至少一种衍生自二羧酸的基团或其衍生物官能化的聚烯烃低聚物; 和（ii）线性氧化烯单元的聚氧化烯。 聚氧化烯与任选含有一个或多个烯属不饱和键的长链烷基连接。 燃料随着时间的推移具有高稳定性，而不会形成附着在金属表面上的碳质沉积物。
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公开(公告)号：US4845281A
公开(公告)日：1989-07-04
申请号：US226017
申请日：1988-07-29
申请人： Attilio Citterio , Daniele Fancelli
发明人： Attilio Citterio , Daniele Fancelli
IPC分类号： C07D209/34 , C07C51/00 , C07C51/16 , C07C51/373 , C07C51/377 , C07C57/30 , C07C59/84 , C07C67/00
CPC分类号： C07C51/16 , C07C51/377
摘要： A method of preparing ketoprofen by reacting aniline with a halide of an alpha-halogen propionic acid, benzylation of 3-methyl-2-indolinone, alkaline hydrolysis of 5-benzyl-3-methyl-2-indolinone, deamination of 2-(3-benzyl-6-aminophenyl)propionic acid and oxidation of 2-(3-benzylphenyl)propionic acid.
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