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    Fluorinated nonionic surfactants
    2.
    发明申请
    Fluorinated nonionic surfactants 失效
    氟化非离子表面活性剂

    公开(公告)号：US20090043133A1

    公开(公告)日：2009-02-12

    申请号：US11890375

    申请日：2007-08-06

    申请人： Peter Michael Murphy ,  Andrew Edward Feiring ,  Stephan James McLain ,  Jessica Sinks

    发明人： Peter Michael Murphy ,  Andrew Edward Feiring ,  Stephan James McLain ,  Jessica Sinks

    IPC分类号： C07C409/00

    CPC分类号： C07C43/126 ,  C07C43/137 ,  C08G65/337 ,  C08L71/02 ,  C11D1/004 ,  C11D1/722

    摘要： A compound comprising Formula I, or a mixture thereof, Rf—OCFHCF2O—[CH2CH2O]x—[C3H7O]y-A   Formula I wherein Rf is CnF2n+1, n is 1 to about 6, x is a mixture of positive integers and is 4 or greater, y is 0 to about 4, provided that the ratio of y to x is equal to or less than 0.25, A is RfOCHFCF2 or CmH2m+1, and m is 0 to about 24 and its use in lowering surface tension and imparting improved surface effects is disclosed.

    摘要翻译： 包含式I或其混合物的化合物<？在线公式描述=“在线式”末端=“铅”→Rf-OCFHCF 2 O- [CH 2 CH 2 O] x - [C 3 H 7 O] y A式I < in-line-formula description =“In-line Formulas”end =“tail”？>其中Rf为CnF2n + 1，n为1至约6，x为正整数的混合物，为4或更大，y为0 至约4，条件是y与x的比例等于或小于0.25，A为RfOCHFCF2或CmH2m + 1，m为0至约24，并且其用于降低表面张力并赋予改善的表面效果。

    Fluorinated sulfonate surfactants
    3.
    发明授权
    Fluorinated sulfonate surfactants 失效
    氟化磺酸盐表面活性剂

    公开(公告)号：US07399887B1

    公开(公告)日：2008-07-15

    申请号：US11890374

    申请日：2007-08-06

    申请人： Peter Michael Murphy ,  Andrew Edward Feiring ,  Stephan James McLain ,  Jessica Sinks

    发明人： Peter Michael Murphy ,  Andrew Edward Feiring ,  Stephan James McLain ,  Jessica Sinks

    IPC分类号： C07C321/00 ,  C07C323/00 ,  C07C381/00

    CPC分类号： C07C309/14 ,  A61K8/466 ,  C09D5/027 ,  C09D7/47 ,  C09G1/04 ,  C11D1/004

    摘要： A compound comprising Formula I, or a mixture thereof, wherein Y is a bond or CmH2m−p(OA)p wherein m is 0 to 4, and p is 0 or 1, X′ is X or H, X is CH2CH2OA, CH(CH2OA)2, C(CH2OA)3, or X and X′ combine to form (CH2CH2)2NCH2CH2OA or (CH2CH2)2O, provided that when X and X′ combine to form (CH2CH2)2O then Y is CH2CH(OA)CH2, A is CF2CFHO—Rf or H, Rf is CnF2n+1 wherein n is an integer of 1 to about 6, M is a cation having a charge equal to a, and a is a positive integer equal to 1 or 2, provided that at least one of X, X′, or Y contains A equal to CF2CFHO—Rf, and its use in lowering surface tension and imparting improved surface effects.

    摘要翻译： 包含式I或其混合物的化合物，其中Y是键或C m H 2 m-p（OA）p p其中m 为0〜4，p为0或1，X'为X或H，X为CH 2 CH 2 OA，CH（CH 2） C（CH 2 OA）3，或X和X'结合形成（CH 2）2， 2/2个2或2个或2个或更多个（CH 2）2 其中X和X'组合形成（CH 2 CH 2 CH 2）2 O， ）2 O，则Y是CH 2 CH（OA）CH 2，A是CF 2 CO 2 -OR 2 或H，R f是C n H 2n + 1，其中n是1至约的整数 如图6所示，M是电荷等于a的阳离子，a是等于1或2的正整数，条件是X，X'或Y中的至少一个包含等于CF 2 CFHO-R f的A， / SUB>，其用于降低表面张力并赋予改善的表面效果。

    Polyfluorosulfonamido amine and intermediate
    4.
    发明授权
    Polyfluorosulfonamido amine and intermediate 失效
    多氟磺酰胺和中间体

    公开(公告)号：US08258341B2

    公开(公告)日：2012-09-04

    申请号：US12500817

    申请日：2009-07-10

    申请人： Alexander Borisovich Shtarov ,  Peter Michael Murphy ,  Brent Ryan Gonska ,  Stephan James McLain

    发明人： Alexander Borisovich Shtarov ,  Peter Michael Murphy ,  Brent Ryan Gonska ,  Stephan James McLain

    IPC分类号： C07C311/09

    CPC分类号： C07C311/09 ,  C07C303/38 ,  C07C303/40

    摘要： Current methods for making polyfluorosulfonamido amines, which involve the use of a diamine reactant, provide low yields and produce an undesirable fluorine containing bis-sulfonamide by-product representing an economic loss. The bis-sulfonamide by-product is particularly undesirable because it shares very similar physical properties with the desired monoamine product thus making isolation of the desired polyfluorosulfonamido amine product difficult and costly. Furthermore, instead of the efficient incorporation of fluorine to make the desired polyfluorosulfonamido amine product, the bis-sulfonamide by-product constitutes a substantial loss of costly fluorinated starting material. The bis-sulfonamide by-product also constitutes an undesirable impurity that can worsen surfactancy, repellency, or other performance characteristics of the desired polyfluorosulfonamido amine product. The present invention provides a method of making a polyfluorosulfonamido amine without the production of a bis-sulfonamide by-product by reacting a polyfluoroalkylsulfonic compound with a monoamino amide rather than with a diamine reactant as in previously known methods.

    摘要翻译： 涉及使用二胺反应物的制备多氟磺酰氨基胺的现有方法提供低产率并产生表示经济损失的不希望的含氟双磺酰胺副产物。 双磺酰胺副产物是特别不希望的，因为它与所需的单胺产物分享非常相似的物理性质，从而使所需的多氟磺酰胺胺产物的分离困难且昂贵。 此外，代替有效地引入氟以制备所需的多氟磺酰氨基胺产物，双磺酰胺副产物构成昂贵的氟化原料的显着损失。 双磺酰胺副产物也构成可恶化期望的多氟磺酰氨基胺产物的表面活性，排斥性或其它性能特征的不期望的杂质。 本发明提供了如先前已知的方法，通过使多氟烷基磺酸化合物与单氨基酰胺而不是二胺反应物反应而制备多氟磺酰胺，不产生双磺酰胺副产物的方法。

    POLYFLUOROSULFONAMIDO AMINE AND INTERMEDIATE
    5.
    发明申请
    POLYFLUOROSULFONAMIDO AMINE AND INTERMEDIATE 失效
    聚氟虫胺和中间体

    公开(公告)号：US20110009668A1

    公开(公告)日：2011-01-13

    申请号：US12500817

    申请日：2009-07-10

    申请人： Alexander Borisovich Shtarov ,  Peter Michael Murphy ,  Brent Ryan Gonska ,  Stephan James McLain

    发明人： Alexander Borisovich Shtarov ,  Peter Michael Murphy ,  Brent Ryan Gonska ,  Stephan James McLain

    IPC分类号： C07C311/01

    CPC分类号： C07C311/09 ,  C07C303/38 ,  C07C303/40

    摘要： Current methods for making polyfluorosulfonamido amines, which involve the use of a diamine reactant, provide low yields and produce an undesirable fluorine containing bis-sulfonamide by-product representing an economic loss. The bis-sulfonamide by-product is particularly undesirable because it shares very similar physical properties with the desired monoamine product thus making isolation of the desired polyfluorosulfonamido amine product difficult and costly. Furthermore, instead of the efficient incorporation of fluorine to make the desired polyfluorosulfonamido amine product, the bis-sulfonamide by-product constitutes a substantial loss of costly fluorinated starting material. The bis-sulfonamide by-product also constitutes an undesirable impurity that can worsen surfactancy, repellency, or other performance characteristics of the desired polyfluorosulfonamido amine product. The present invention provides a method of making a polyfluorosulfonamido amine without the production of a bis-sulfonamide by-product by reacting a polyfluoroalkylsulfonic compound with a monoamino amide rather than with a diamine reactant as in previously known methods.

    摘要翻译： 涉及使用二胺反应物的制备多氟磺酰氨基胺的现有方法提供低产率并产生表示经济损失的不希望的含氟双磺酰胺副产物。 双磺酰胺副产物是特别不希望的，因为它与所需的单胺产物分享非常相似的物理性质，从而使所需的多氟磺酰胺胺产物的分离困难且昂贵。 此外，代替有效地引入氟以制备所需的多氟磺酰氨基胺产物，双磺酰胺副产物构成昂贵的氟化原料的显着损失。 双磺酰胺副产物也构成可恶化期望的多氟磺酰氨基胺产物的表面活性，排斥性或其它性能特征的不期望的杂质。 本发明提供了如先前已知的方法，通过使多氟烷基磺酸化合物与单氨基酰胺而不是二胺反应物反应而制备多氟磺酰胺，不产生双磺酰胺副产物的方法。

    Air activated organotin catalysts for polyurethane synthesis
    9.
    发明授权
    Air activated organotin catalysts for polyurethane synthesis 有权
    用于聚氨酯合成的空气活化有机锡催化剂

    公开(公告)号：US07919423B2

    公开(公告)日：2011-04-05

    申请号：US12698288

    申请日：2010-02-02

    申请人： Jerald Feldman ,  Stephan James McLain

    发明人： Jerald Feldman ,  Stephan James McLain

    IPC分类号： B01J31/00 ,  B01J27/135 ,  B01J21/04 ,  B01J23/02

    CPC分类号： C09D175/04 ,  B01J31/0202 ,  B01J31/0207 ,  B01J31/0211 ,  B01J31/28 ,  B01J2531/42 ,  C07F7/2208 ,  C07F7/2288 ,  C08G18/242 ,  C08G18/792

    摘要： This invention relates to an organotin-based catalyst system for polyurethane synthesis that is useful in coatings applications. The catalyst has low activity in the absence of oxygen. When a coating mixture comprising the catalyst is sprayed and/or applied to a substrate as a thin film in air, the catalyst is activated. For solvent-based refinish systems comprising hydroxyl and isocyanate species at high solids levels, the catalyst system therefore provides extended viscosity stability, i.e., pot life.

    摘要翻译： 本发明涉及用于聚氨酯合成的有机锡基催化剂体系，其可用于涂料应用。 催化剂在不存在氧的情况下具有低活性。 当包含催化剂的涂料混合物在空气中作为薄膜喷涂和/或施加到基材上时，催化剂被活化。 对于含有高固体含量的羟基和异氰酸酯物质的基于溶剂的修补体系，催化剂体系因此提供了延长的粘度稳定性，即适用期。

    PROCESS AND MATERIALS FOR MAKING CONTAINED LAYERS AND DEVICES MADE WITH SAME
    10.
    发明申请
    PROCESS AND MATERIALS FOR MAKING CONTAINED LAYERS AND DEVICES MADE WITH SAME 失效
    用于制造包含层的工艺和材料及其制品

    公开(公告)号：US20100213454A1

    公开(公告)日：2010-08-26

    申请号：US12738460

    申请日：2008-10-24

    申请人： Charles D. Lang ,  Paul Anthony Sant ,  Jerald Feldman ,  Steven Dale Ittel ,  Stephan James McLain

    发明人： Charles D. Lang ,  Paul Anthony Sant ,  Jerald Feldman ,  Steven Dale Ittel ,  Stephan James McLain

    IPC分类号： H01L51/30 ,  H01L51/40 ,  H01L51/54 ,  H01L51/56

    CPC分类号： H01L51/0005 ,  G03F7/0046 ,  G03F7/027 ,  H01G11/48 ,  H01G11/56 ,  H01L51/0003 ,  H01L51/0012 ,  H01L51/5048 ,  H01L51/56 ,  Y02E60/13

    摘要： There is provided a process for forming a contained second layer over a first layer. The process comprises forming the first layer having a first surface energy and then treating the first layer with a photocurable surface-active composition which is a fluorinated ester or fluorinated imide of an α,β-unsaturated polyacid; exposing the photocurable surface-active composition patternwise with radiation resulting in exposed areas and unexposed areas; developing the photocurable surface-active composition to remove the unexposed areas resulting in a first layer having untreated portions in the unexposed areas and treated portions in the exposed areas, where the treated portions have a second surface energy that is lower than the first surface energy; and forming the second layer on the untreated portions of the first layer. There is also provided an organic electronic device made by the process.

    摘要翻译： 提供了一种用于在第一层上形成包含的第二层的方法。 该方法包括形成具有第一表面能的第一层，然后用可光固化的表面活性组合物处理第一层，该组合物是α，β-不饱和多元酸的氟化酯或氟化酰亚胺; 用辐射曝光可光固化的表面活性组合物，导致曝光区域和未曝光区域; 显影可光固化表面活性组合物以除去未曝光区域，从而在未曝光区域中具有未处理部分的第一层和暴露区域中的处理部分，其中处理部分具有低于第一表面能的第二表面能; 以及在所述第一层的未处理部分上形成所述第二层。 还提供了通过该方法制造的有机电子装置。