Anilines as markers for mineral oils
    1.
    发明授权
    Anilines as markers for mineral oils 失效
    苯胺作为矿物油的标记物

    公开(公告)号:US5627077A

    公开(公告)日:1997-05-06

    申请号:US424497

    申请日:1995-06-22

    摘要: Anilines of the formula ##STR1## where R.sup.1 and R.sup.2 are each hydrogen, unsubstituted or substituted alkyl, alkenyl or unsubstituted or substituted phenyl orR.sup.1 and R.sup.2, together with the nitrogen atom linking them are a heterocyclic radical or R.sup.1 may furthermore be unsubstituted or substituted hydroxyl or unsubstituted or substituted amino,R.sup.3 and R.sup.7 are each hydrogen, unsubstituted or substituted alkyl, alkenyl, cyano, nitro, acyl, acylamino, unsubstituted or substituted hydroxyl, unsubstituted or substituted carboxymethyl, unsubstituted or substituted amino, unsubstituted or substituted mercapto or unsubstituted or substituted sulfamoyl or, together with R.sup.2, are alkylene, alkenylene or phenylalkenylene,R.sup.4 is hydrogen, unsubstituted or substituted alkyl, alkenyl, unsubstituted or substituted hydroxyl, unsubstituted or substituted amino, unsubstituted or substituted carboxyl or unsubstituted or substituted sulfamoyl andR.sup.5 and R.sup.6 are each hydrogen, unsubstituted or substituted alkyl, alkenyl, unsubstituted or substituted phenyl, nitro, acylamino, unsubstituted or substituted hydroxyl, unsubstituted or substituted amino, unsubstituted or substituted sulfamoyl, alkyl-, alkenyl- or arylsulfonyl, acyl or unsubstituted or substituted carboxyl,with the proviso that at least one of the radicals R.sup.3, R.sup.5 or R.sup.7 is hydrogen,are used for marking mineral oils, and the above-mentioned anilines are detected in mineral oils.

    摘要翻译: PCT No.PCT / EP93 / 03133 Sec。 371日期:1995年6月22日 102(e)日期1995年6月22日PCT 1993年11月9日PCT公布。 公开号WO94 / 11466 日期:1994年5月26日公式其中R 1和R 2各自为氢,未取代或取代的烷基,烯基或未取代或取代的苯基或R 1和R 2与其连接的氮原子的式(I)的氨基是杂环基或 R 1还可以是未取代的或取代的羟基或未取代或取代的氨基,R 3和R 7各自为氢,未取代或取代的烷基,烯基,氰基,硝基,酰基,酰氨基,未取代或取代的羟基,未取代或取代的羧甲基,未取代或取代的氨基 未取代或取代的巯基或未取代或取代的氨磺酰基,或与R2一起为亚烷基,亚烯基或苯基亚烯基,R4为氢,未取代或取代的烷基,烯基,未取代或取代的羟基,未取代或取代的氨基,未取代或取代的羧基或未取代的 或取代的氨磺酰基,且R 5和R 6各自为未经取代或未取代的氢 取代的烷基,烯基,未取代或取代的苯基,硝基,酰基氨基,未取代或取代的羟基,未取代或取代的氨基,未取代或取代的氨磺酰基,烷基 - ,烯基 - 或芳基磺酰基,酰基或未取代或取代的羧基,条件是至少 基团R3,R5或R7之一是氢,用于标记矿物油,并且在矿物油中检测到上述苯胺。

    Detection of marked mineral oils and novel azo dyes
    2.
    发明授权
    Detection of marked mineral oils and novel azo dyes 失效
    检测标记矿物油和新偶氮染料

    公开(公告)号:US5487770A

    公开(公告)日:1996-01-30

    申请号:US321629

    申请日:1994-10-12

    摘要: Method for detecting marked mineral oils by treating the marked mineral oil with an extractant comprising water, a solvent and a base comprises using as marker an azo dye of the formula ##STR1## where ring A may be benzofused,m is from 1 to 4,X.sup.1 is hydrogen, C.sub.1 -C.sub.4 -alkyl, cyano or nitro,X.sup.2 is hydrogen, C.sub.1 -C.sub.4 -alkyl, cyano, nitro, C.sub.1 -C.sub.4 -alkoxy or C.sub.1 -C.sub.16 -alkoxycarbonyl,X.sup.3 is hydrogen, C.sub.1 -C.sub.4 -alkyl, cyano or C.sub.1 -C.sub.16 -alkoxycarbonyl, andX.sup.4 is hydrogen, hydroxyl, substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.4 -alkoxy, amino, C.sub.1 -C.sub.4 -dialkylamino or substituted or unsubstituted C.sub.1 -C.sub.16 -monoalkylamino,as solvent a partially or completely water-miscible organic solvent, and as base an alkali or alkaline earth metal hydroxide, an alkali metal carbonate or a quaternary ammonium hydroxide, the use of azo dyes as markers for mineral oils, and novel azo dyes.

    摘要翻译: 通过用包含水,溶剂和碱的萃取剂处理标记的矿物油来检测标记的矿物油的方法包括使用式为“IMAGE”的偶氮染料作为标记,其中环A可被苯并稠合,m为1至4, X 1是氢,C 1 -C 4 - 烷基,氰基或硝基,X 2是氢,C 1 -C 4 - 烷基,氰基,硝基,C 1 -C 4 - 烷氧基或C 1 -C 16 - 烷氧羰基,X 3是氢,C 1 -C 4烷基, 氰基或C 1 -C 16 - 烷氧基羰基,X 4是氢,羟基,取代或未取代的C 1 -C 8 - 烷基,C 1 -C 4 - 烷氧基,氨基,C 1 -C 4 - 二烷基氨基或取代或未取代的C 1 -C 16单烷基氨基,作为溶剂a 部分或完全水溶性有机溶剂,碱金属或碱土金属氢氧化物,碱金属碳酸盐或季铵氢氧化物作为碱,使用偶氮染料作为矿物油的标记物和新型偶氮染料。

    PAPER SIZE MIXTURES
    7.
    发明申请
    PAPER SIZE MIXTURES 审中-公开
    纸尺寸混合

    公开(公告)号:US20100016478A1

    公开(公告)日:2010-01-21

    申请号:US12518312

    申请日:2007-12-11

    摘要: Paper size mixtures comprising a reactive size dispersed in water and a polymer, which are obtainable by mixing (a) an aqueous dispersion of a reactive size whose dispersed particles have a mean particle diameter of less than 500 nm, the dispersion being obtainable by emulsifying at least one reactive size in water in the presence of at least one surfactant, and (b) at least one emulsion polymer and/or at least one water-soluble polymer which does not have a dispersing effect with respect to reactive sizes and/or a water-dispersible polymer, and use of said paper size mixtures for the engine sizing and surface sizing of paper and paper products.

    摘要翻译: 通过混合(a)具有平均粒径小于500nm的分散颗粒的反应性尺寸的水性分散体可以获得的分散在水中的反应尺寸的聚合物的纸尺寸混合物,所述分散体可通过乳化在 在至少一种表面活性剂存在下,在水中至少一种反应性大小,和(b)至少一种乳液聚合物和/或至少一种水溶性聚合物,其对于反应性大小和/或不具有分散作用 水分散性聚合物,以及使用所述纸尺寸混合物用于纸和纸产品的发动机尺寸和表面施胶。

    2-ethylhexylamine salts of anionic monoazo dyes
    8.
    发明授权
    2-ethylhexylamine salts of anionic monoazo dyes 失效
    阴离子单偶氮染料的2-乙基己基胺盐

    公开(公告)号:US4668774A

    公开(公告)日:1987-05-26

    申请号:US726372

    申请日:1985-04-23

    CPC分类号: C09B69/04 Y10S534/02

    摘要: Novel dye salts of anionic dyes of the general formula I ##STR1## where F is a radical of an anionic dye, n is 1, 2, 3 or 4, and B.sup.1 and B.sup.2 independently of one another are each unsubstituted or substituted branched alkyl or alkyl-substituted cycloalkyl having a total of 10 to 36 carbon atoms, are very useful for dyeing solvents, printing inks or polymeric film-forming materials.

    摘要翻译: 通式I的阴离子染料的新型染料盐其中F是阴离子染料的基团,n是1,2,3或4,并且彼此独立的B 1和B 2各自是未取代的或取代的支链烷基 或具有总共10至36个碳原子的烷基取代的环烷基对染色溶剂,印刷油墨或聚合物成膜材料非常有用。

    Method for the production of composite materials
    9.
    发明授权
    Method for the production of composite materials 有权
    复合材料生产方法

    公开(公告)号:US09234098B2

    公开(公告)日:2016-01-12

    申请号:US13262755

    申请日:2010-04-01

    摘要: The present invention relates to a process for producing a nanocomposite material from a) at least one inorganic or organometallic metal phase; and b) an organic polymer phase; comprising the polymerization of at least one monomer M which have at least one first polymerizable monomer unit A which has a metal or semimetal M, and at least one second polymerizable organic monomer unit B which is joined to the polymerizable unit A via a covalent chemical bond, under polymerization conditions under which both the polymerizable monomer unit A and the polymerizable unit B polymerize with breakage of the bond between A and B, the monomers M to be polymerized comprising a first monomer M1 and at least one second monomer M2 which differs at least in one of the monomer units A and B from the monomer M1 (embodiment 1), or the monomers to be polymerized comprising, as well as the at least one monomer M, at least one further monomer other than the monomers M, i.e. a conventional monomer which does not have a monomer unit A and is copolymerizable with the monomer unit B (embodiment 2).

    摘要翻译: 本发明涉及从a)至少一种无机或有机金属金属相制备纳米复合材料的方法; 和b)有机聚合物相; 包括至少一种单体M的聚合,所述单体M具有至少一个具有金属或半金属M的第一可聚合单体单元A和至少一个第二可聚合有机单体单元B,其通过共价化学键连接到可聚合单元A 在可聚合单体单元A和可聚合单元B两者都聚合并且A和B之间的键断裂聚合的聚合条件下,待聚合的单体M包含第一单体M1和至少一个第二单体M2,其至少不同 在单体M1(实施方案1)的单体单元A和B中的一种中,或要聚合的单体以及至少一种单体M至少一种除单体M以外的其它单体,即常规 不具有单体单元A并且可与单体单元B共聚的单体(实施方案2)。

    Process for the homogeneous incorporation of polymer particles into polymeric matrices
    10.
    发明授权
    Process for the homogeneous incorporation of polymer particles into polymeric matrices 失效
    将聚合物颗粒均匀掺入聚合物基质的方法

    公开(公告)号:US08324305B2

    公开(公告)日:2012-12-04

    申请号:US13002515

    申请日:2009-07-03

    IPC分类号: C08K5/01 C08K5/16

    摘要: The invention relates to preparations comprising a wax in which polymer particles are present, where the polymer particles comprise at least one effect substance, obtainable by, by means of a miniemulsion polymerization carried out in the presence of a wax-immiscible solvent, distributing at least one effect substance in polymer particles, and incorporating the polymer particle dispersion obtained in this way into a wax by phase transfer.Furthermore, the invention relates to compositions comprising a polymeric matrix in which, in essentially homogeneous distribution, the aforementioned polymer particles are present, obtainable by incorporating the aforementioned polymer-particle-comprising wax as preparation into a polymeric matrix.

    摘要翻译: 本发明涉及包含其中存在聚合物颗粒的蜡的制剂,其中聚合物颗粒包含至少一种效应物质,其可通过在不溶于蜡的溶剂存在下进行的微乳液聚合获得,至少分布 聚合物颗粒中的一种效应物质,并且通过相转移将以这种方式获得的聚合物颗粒分散体掺入蜡中。 此外,本发明涉及包含聚合物基质的组合物,其中基本上均匀分布存在上述聚合物颗粒,其通过将上述含聚合物颗粒的蜡作为制剂掺入聚合物基质中而获得。