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    Composition for the recovery of lithium values from brine and process of making/using said composition
    3.
    发明授权
    Composition for the recovery of lithium values from brine and process of making/using said composition 失效
    用于从盐水中回收锂值的组合物和制备/使用所述组合物的方法

    公开(公告)号：US06280693B1

    公开(公告)日：2001-08-28

    申请号：US08716954

    申请日：1996-09-20

    申请人： William C. Bauman ,  John L. Burba, III

    发明人： William C. Bauman ,  John L. Burba, III

    IPC分类号： C01D1500

    CPC分类号： C01D15/04 ,  B01J39/17 ,  B01J47/018 ,  C01F7/002

    摘要： The present invention is a composition comprising pellets, each of said pellets consisting essentially of an integral mass of polycrystalline material of randomly disposed crystals of hydrated alumina infused with an amount of LiX to produce LiX/Al(OH)3 having up to a mol fraction of 0.33 of LiX in the so-produced LiX/Al(OH)3, wherein LiX is at least one compound selected from the group consisting of Li hydroxide, Li halide, Li nitrate, Li sulfate, and Li bicarbonate. The present invention further includes methods of preparing the composition and methods of recovery lithium values from brine using the composition.

    摘要翻译： 本发明是一种包含颗粒的组合物，每个所述颗粒基本上由整体的多晶材料组成，其随机排列的水合氧化铝晶体注入一定量的LiX以产生具有高达摩尔分数的LiX / Al（OH）3 在生产的LiX / Al（OH）3中LiX为0.33，其中LiX为选自Li氢氧化物，Li卤化物，Li硝酸盐，Li硫酸盐和Li碳酸氢盐中的至少一种化合物。 本发明还包括使用该组合物制备组合物的方法和从盐水中回收锂值的方法。

    Recovery of lithium values from brines
    7.
    发明授权
    Recovery of lithium values from brines 失效
    从盐水中回收锂值

    公开(公告)号：US5599516A

    公开(公告)日：1997-02-04

    申请号：US387178

    申请日：1995-02-13

    申请人： William C. Bauman ,  John L. Burba, III

    发明人： William C. Bauman ,  John L. Burba, III

    IPC分类号： B01J39/16 ,  B01J47/00 ,  C01D15/04 ,  C01F7/00 ,  C01D15/00 ,  B01J20/00 ,  C09K3/00

    CPC分类号： C01D15/04 ,  B01J39/165 ,  B01J47/007 ,  C01F7/002

    摘要： Pellets of a polycrystalline hydrated alumina, especially Gibbsite, are infused with LiOH to obtain loadings up to 0.33 mol fraction of LiOH in the LiOH/Al(OH).sub.3. The so-prepared material is useful for mixing with a LiX-containing brine solution, producing an interaction of the LiOH infused in the alumina pellets with the X ion (where X represents an acid salt moiety, especially halide) of the LiX-containing brine. The LiX interaction product is efficiently removed from the alumina pellets by water washing, leaving rejuvenated LiOH which can be used in yet another cycling of LiX formation/water removal. A plurality of loading and unloading cycles are achieved, yielding an appreciable amount of the lithium values derived from the brine.

    摘要翻译： 将多晶水合氧化铝，特别是三水铝矿的颗粒注入LiOH，以在LiOH / Al（OH）3中获得高达0.33摩尔份量的LiOH的负载。 如此制备的材料可用于与含LiX的盐水溶液混合，产生在氧化铝颗粒中输入的LiOH与含LiX的盐水的X离子（其中X表示酸盐部分，特别是卤化物）的相互作用 。 LiX相互作用产物通过水洗有效地从氧化铝颗粒中除去，留下可再用于LiX形成/除水循环中的再生LiOH。 实现了多个加载和卸载循环，产生了从盐水得到的相当数量的锂值。

    Recovery of lithium values from brines
    8.
    发明授权
    Recovery of lithium values from brines 失效
    从盐水中回收锂值

    公开(公告)号：US5389349A

    公开(公告)日：1995-02-14

    申请号：US65586

    申请日：1993-05-24

    申请人： William C. Bauman ,  John L. Burba, III

    发明人： William C. Bauman ,  John L. Burba, III

    IPC分类号： B01J39/16 ,  B01J47/00 ,  C01D15/04 ,  C01F7/00 ,  C01D15/00 ,  B01J20/00 ,  C09K3/00

    CPC分类号： C01F7/002 ,  B01J39/165 ,  B01J47/007 ,  C01D15/04

    摘要： Morphologically altered pellets of a polycrystalline hydrated alumina, intercalated with LiX (where LiX is a lithium salt, preferably LiCl), is prepared by contacting the polycrystalline structure with LiX solution carried in NaCl brine, the LiX creating lithium-specific sites of intercalation in the crystalline structure, and the material is used in a LiX absorption process involving unloading LiX from the pellets, and then passing a LiX-containing brine through the pellets to capture more LiX in the Li-depleted active sites, and repeating the unloading and loading of the LiX a plurality of cycles. The unloaded LiX is collected as crude product which can be concentrated by evaporation and removing precipitated NaCl.

    摘要翻译： 通过使多晶结构与NaCl盐水中携带的LiX溶液接触，制备插入LiX（其中LiX为锂盐，优选LiCl）的多晶水合氧化铝的形态学改变的颗粒，将LiX形成插入的锂特异性位点 晶体结构，并且该材料用于涉及从颗粒中卸载LiX的LiX吸收过程，然后使含LiX的盐水通过该颗粒以在Li-贫化的活性位点捕获更多的LiX，并重复卸载和装载 LiX多个周期。 收集未加载的LiX作为粗产物，通过蒸发浓缩并除去沉淀的NaCl。

    Method and apparatus to improve perforating effectiveness using a unique multiple point initiated shaped charge perforator
    10.
    发明授权
    Method and apparatus to improve perforating effectiveness using a unique multiple point initiated shaped charge perforator 有权
    使用独特的多点起动成形电荷穿孔器来改善穿孔效果的方法和装置

    公开(公告)号：US06925924B2

    公开(公告)日：2005-08-09

    申请号：US10684858

    申请日：2003-10-14

    申请人： Ernest L. Baker ,  David C. Daniel ,  David S. Wesson ,  John L. Burba, III ,  Arthur S. Daniels ,  Robert E. Davis

    发明人： Ernest L. Baker ,  David C. Daniel ,  David S. Wesson ,  John L. Burba, III ,  Arthur S. Daniels ,  Robert E. Davis

    IPC分类号： E21B43/117 ,  F24B1/00 ,  F42B1/02 ,  E21B43/116

    CPC分类号： E21B43/117 ,  F42B1/02

    摘要： A non-linear shaped charge perforator for use in perforating an oil and gas formation into which a wellbore has been drilled comprises a monolithic, axisymmetric metal case in which is disposed a main explosive charge between the front of the case, which is closed with a concave metal liner, and the closed back end of the case. The main explosive charge contains multiple initiation points, preferably two initiation points located about 180° apart on the outside surface of the charge, so that when the perforator is detonated the main charge is initiated such that the metal liner is collapsed into a non-circular jet, preferably a fan-shaped jet, that pierces the casing of the wellbore and forms non-circular perforations, preferably slot-shaped perforations, in the surrounding formation.

    摘要翻译： 一种用于穿孔钻井的油气层的非线性形状的充气穿孔器包括一个整体式的轴对称金属壳体，其中在壳体的前部之间设置主要的炸药， 凹形金属衬里和封闭的后端。 主要的炸药包含多个起始点，优选地在电荷的外表面上分开约180°的两个起始点，使得当穿孔器被引爆时，引起主电荷使得金属衬垫被折叠成非圆形 喷射，优选是扇形喷射器，其刺穿井眼的壳体并在周围地层中形成非圆形穿孔，优选为狭缝形穿孔。