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    Silicone resin compositions having good solution solubility and stability
    7.
    发明授权
    Silicone resin compositions having good solution solubility and stability 失效
    具有良好溶液溶解性和稳定性的硅酮树脂组合物

    公开(公告)号：US06359096B1

    公开(公告)日：2002-03-19

    申请号：US09425306

    申请日：1999-10-25

    申请人： Bianxiao Zhong ,  Russell Keith King ,  Kyuha Chung ,  Shizhong Zhang

    发明人： Bianxiao Zhong ,  Russell Keith King ,  Kyuha Chung ,  Shizhong Zhang

    IPC分类号： C08G7712

    CPC分类号： C08G77/12 ,  C08G77/02 ,  C09D183/04

    摘要： Soluble silicone resin compositions having good solution stability and a method for their preparation. The silicone resin comprises the reaction product of a mixture comprising (A) 15-70 mol % of a tetraalkoxysilane described by formula Si(OR1)4, where each R1 is an independently selected alkyl group comprising 1 to about 6 carbon atoms, (B) 12 to 60 mol % of a hydrosilane described by formula HSiX3, where each X is an independently selected hydrolyzable substituent, (C) 15 to 70 mole percent of an organotrialkoxysilane described by formula R2Si(OR3)3, where R2 is a hydrocarbon group comprising about 8 to 24 carbon atoms or a substituted hydrocarbon group comprising a hydrocarbon chain having about 8 to 24 carbon atoms and each R3 is an independently selected alkyl group comprising 1 to about 6 carbon atoms; in the presence of (D) water, (E) hydrolysis catalyst, and (F) organic solvent for the reaction product.

    摘要翻译： 具有良好溶液稳定性的可溶性有机硅树脂组合物及其制备方法。 有机硅树脂包括由（A）15-70mol％的四烷氧基硅烷所组成的混合物的反应产物，每个R 1是独立选择的含有1至约6个碳原子的烷基，（B）12至60mol％ 由式X表示的氢硅烷，每个X是独立选择的可水解取代基，（C）15-70摩尔％的由通式R 2表示的有机三烷氧基硅烷是包含约8至24个碳原子的烃基或包含烃链的取代烃基， 约8至24个碳原子，并且每个R 3是独立选择的包含1至约6个碳原子的烷基; 在（D）水，（E）水解催化剂和（F）反应产物的有机溶剂的存在下。

    Soluble silicone resin compositions having good solution stability
    8.
    发明授权
    Soluble silicone resin compositions having good solution stability 有权
    具有良好溶液稳定性的可溶性有机硅树脂组合物

    公开(公告)号：US06232424B1

    公开(公告)日：2001-05-15

    申请号：US09460102

    申请日：1999-12-13

    申请人： Bianxiao Zhong ,  Russell Keith King ,  Kyuha Chung ,  Shizhong Zhang

    发明人： Bianxiao Zhong ,  Russell Keith King ,  Kyuha Chung ,  Shizhong Zhang

    IPC分类号： C08G7718

    CPC分类号： C09D183/04 ,  C08G77/02 ,  C08G77/12

    摘要： Soluble silicone resin compositions having good solution stability and a method for their preparation. The silicone resin comprises the reaction product of a mixture comprising (A) 15-70 mol % of a tetraalkoxysilane described by formula Si(OR1)4,  where each R1, is an independently selected alkyl group comprising 1 to about 6 carbon atoms, (B) 12 to 60 mol % of an organosilane described by formula R4SiX3,  where R4, is selected from the group consisting of alkyl groups comprising 1 to about 6 carbon atoms and phenyl and each X is an independently selected hydrolyzable substituent, (C) 15 to 70 mole percent of an organotrialkoxysilane described by formula R2Si(OR3)3,  where R2, is a hydrocarbon group comprising about 8 to 24 carbon atoms or a substituted hydrocarbon group comprising a hydrocarbon chain having about 8 to 24 carbon atoms and each R3, is an independently selected alkyl group comprising 1 to about 6 carbon atoms; in the presence of (D) water, (E) hydrolysis catalyst, and (F) organic solvent for the reaction product.

    摘要翻译： 具有良好溶液稳定性的可溶性有机硅树脂组合物及其制备方法。 有机硅树脂包括含有（A）15-70摩尔％四烷氧基硅烷的混合物的反应产物，其中每个R 1是独立选择的包含1至约6个碳原子的烷基，（B）12至60摩尔 ％的有机硅烷由下式表示：其中R4选自包含1至约6个碳原子的烷基和苯基，每个X为独立选择的可水解取代基，（C）15至70摩尔％的所述有机三烷氧基硅烷 其中R 2是含有约8至24个碳原子的烃基或含有约8-24个碳原子的烃链的取代烃基，每个R 3是独立选择的包含1至约6个碳原子的烷基; 在（D）水，（E）水解催化剂和（F）反应产物的有机溶剂的存在下。

    Thickening silicones with elastomeric silicone polyethers
    9.
    发明授权
    Thickening silicones with elastomeric silicone polyethers 失效
    用弹性硅氧烷聚醚增稠硅酮

    公开(公告)号：US5811487A

    公开(公告)日：1998-09-22

    申请号：US768064

    申请日：1996-12-16

    申请人： William James Schulz, Jr. ,  Shizhong Zhang

    发明人： William James Schulz, Jr. ,  Shizhong Zhang

    IPC分类号： A61K8/00 ,  A61K8/89 ,  A61K8/891 ,  A61Q5/00 ,  C08G77/12 ,  C08G77/46 ,  C08G77/50 ,  C08K5/01 ,  C08L83/05 ,  C08L83/12 ,  C08J83/02 ,  C08F283/00 ,  C08G77/06

    CPC分类号： A61K8/895 ,  A61Q19/00 ,  C08G77/46 ,  C08G77/50 ,  C08K5/01 ,  C08L83/12

    摘要： Low molecular weight siloxane fluids are thickened by silicone elastomers. The silicone elastomers are made by crosslinking reactions of .tbd.Si--H containing siloxanes and an unsaturated hydrocarbon such as an alpha, omega-diene, in the presence of a low molecular weight siloxane fluid. The .tbd.SiH siloxane is first partially reacted with a mono-alkenyl functionalized polyether. It is then crosslinked by the alpha, omega-diene, in the presence of the low molecular weight siloxane fluid. An elastomer, i.e. gel, with polyether groups is produced. The elastomer can be swollen with the low molecular weight siloxane fluid under shear force, to provide a uniform silicone paste. The silicone paste has excellent spreadability upon rubbing, and possesses unique rheological properties in being thixotropic and shear thinning. The silicone paste can be easily emulsified with water to form a stable uniform emulsion, without using a surfactant to allow normally immiscible materials to become intimately mixed.

    摘要翻译： 低分子硅氧烷流体由硅氧烷弹性体增稠。 硅氧烷弹性体是通过在低分子量硅氧烷流体存在下，通过含有SiTHH的硅氧烷和不饱和烃如α，ω-二烯的交联反应来制备的。 3BOND SiH硅氧烷首先与单烯基官能化聚醚部分反应。 然后在低分子量硅氧烷流体的存在下，通过α，ω-二烯交联。 制备具有聚醚基团的弹性体，即凝胶。 弹性体可以在剪切力下用低分子量硅氧烷流体溶胀，以提供均匀的硅胶。 硅胶糊在摩擦时具有优异的铺展性，并且在触变和剪切变稀中具有独特的流变性能。 硅胶糊可以容易地用水乳化以形成稳定的均匀乳液，而不使用表面活性剂以允许通常不混溶的材料变得紧密混合。