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公开(公告)号：US06770708B2
公开(公告)日：2004-08-03
申请号：US10229739
申请日：2002-08-27
申请人： Donald Anthony Kadlec , Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith , Michael Stephen Starch , Shizhong Zhang
发明人： Donald Anthony Kadlec , Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith , Michael Stephen Starch , Shizhong Zhang
IPC分类号： C08L8304
CPC分类号： C08J3/09 , A61K8/891 , A61Q15/00 , A61Q19/00 , C08G77/50 , C08J2383/04 , C08K5/01 , C08L83/14 , C08L83/04
摘要： This invention is directed to an elastomer composition produced by crosslinking a high molecular weight ≡Si—H containing polysiloxane and a diene, diyne or ene-yne compound in the presence of a diluent. The elastomer composition is suitable for use in forming personal care compositions.
摘要翻译： 本发明涉及通过在稀释剂存在下交联含高分子量=含Si-H的聚硅氧烷和二烯，二炔或烯化合物制备的弹性体组合物。 弹性体组合物适用于形成个人护理组合物。
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公开(公告)号：US5977280A
公开(公告)日：1999-11-02
申请号：US964547
申请日：1997-11-05
IPC分类号： E02D3/00 , A61K8/00 , A61K8/02 , A61K8/31 , A61K8/44 , A61K8/58 , A61K8/72 , A61K8/89 , A61K8/891 , A61Q1/00 , A61Q1/04 , A61Q1/10 , A61Q1/12 , A61Q5/02 , A61Q19/00 , C08G77/32 , C08G77/38 , C08G77/50 , C08K5/01 , C08L83/04 , C08L83/05 , C08L83/14 , C08G77/08
CPC分类号： A61K8/891 , A61K8/042 , A61Q19/00 , C08G77/32 , C08G77/50 , C08L83/04 , C08L83/14 , C08G77/442 , Y10S106/90
摘要： A method of thickening solvents involves reacting (A) an .ident.Si--H containing polysiloxane with (B) an alkene such as an alpha, omega-diene; conducting the reaction in the presence of a platinum catalyst and (C) a solvent; continuing the reaction until a gel is formed by crosslinking and addition of .ident.Si--H across double bonds in the alpha, omega-diene; adding additional solvent and a post cure terminating agent to the gel; and subjecting the solvent, the post cure terminating agent, and the gel to shear force until a paste is formed. The post cure terminating agent is an amino acid ester, preferably a sulfur containing amino acid ester, such as methionine methyl ester, methionine ethyl ester, cysteine methyl ester, cysteine ethyl ester, and cystine dimethyl ester.
摘要翻译： 增稠溶剂的方法包括使（A）含Si-H的聚硅氧烷与（B）烯烃如α，ω-二烯反应; 在铂催化剂和（C）溶剂的存在下进行反应; 继续反应，直到通过交联并在α，ω-二烯中加入= Si-H跨越双键形成凝胶; 向凝胶中加入另外的溶剂和后固化终止剂; 并使溶剂，后固化终止剂和凝胶经受剪切力直到形成糊状物。 后固化终止剂是氨基酸酯，优选含硫氨基酸酯，例如甲硫氨酸甲酯，甲硫氨酸乙酯，半胱氨酸甲酯，半胱氨酸乙酯和胱氨酸二甲酯。
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公开(公告)号：US5948855A
公开(公告)日：1999-09-07
申请号：US228863
申请日：1999-01-12
IPC分类号： A61K6/00 , A61K8/00 , A61K8/06 , A61K8/58 , A61K8/89 , A61K8/891 , A61K8/894 , A61K8/92 , A61Q5/00 , A61Q15/00 , A61Q19/00 , B01F17/00 , C08G77/46 , C08J3/03 , C08J3/075 , C08L83/00 , C08L83/12
摘要： A multiple emulsion of the type W.sub.1 /O/W.sub.2 is made by first preparing a primary emulsion W.sub.1 /O using a silicone fluid as the oil phase (O), and an elastomeric silicone polyether as an emulsifier, for dispersing water phase W.sub.1 into oil phase (O). The primary emulsion W.sub.1 /O is then added and dispersed into a final continuous water phase W.sub.2 to form a multiple emulsion W.sub.1 /O/W.sub.2. The multiple emulsions are useful for treating the hair, the skin, or the underarm areas of the human body. Vitamins or drugs can be included in the oil phase (O) or in either aqueous phase W.sub.1 or W.sub.2 to enhance the benefits of the multiple emulsions in personal care applications.
摘要翻译： 通过首先使用硅油作为油相（O）和作为乳化剂的弹性体硅氧烷聚醚制备用于将水相W1分散到油中的初级乳液W1 / O，制备W1 / O / W2型多重乳液 相（O）。 然后将主乳液W1 / O加入并分散到最终的连续水相W2中以形成多重乳液W1 / O / W2。 多重乳液可用于治疗人体的头发，皮肤或腋下区域。 维生素或药物可以包含在油相（O）或水相W1或W2中，以增强个人护理应用中多重乳液的益处。
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公开(公告)号：US5811487A
公开(公告)日：1998-09-22
申请号：US768064
申请日：1996-12-16
IPC分类号： A61K8/00 , A61K8/89 , A61K8/891 , A61Q5/00 , C08G77/12 , C08G77/46 , C08G77/50 , C08K5/01 , C08L83/05 , C08L83/12 , C08J83/02 , C08F283/00 , C08G77/06
摘要： Low molecular weight siloxane fluids are thickened by silicone elastomers. The silicone elastomers are made by crosslinking reactions of .tbd.Si--H containing siloxanes and an unsaturated hydrocarbon such as an alpha, omega-diene, in the presence of a low molecular weight siloxane fluid. The .tbd.SiH siloxane is first partially reacted with a mono-alkenyl functionalized polyether. It is then crosslinked by the alpha, omega-diene, in the presence of the low molecular weight siloxane fluid. An elastomer, i.e. gel, with polyether groups is produced. The elastomer can be swollen with the low molecular weight siloxane fluid under shear force, to provide a uniform silicone paste. The silicone paste has excellent spreadability upon rubbing, and possesses unique rheological properties in being thixotropic and shear thinning. The silicone paste can be easily emulsified with water to form a stable uniform emulsion, without using a surfactant to allow normally immiscible materials to become intimately mixed.
摘要翻译： 低分子硅氧烷流体由硅氧烷弹性体增稠。 硅氧烷弹性体是通过在低分子量硅氧烷流体存在下，通过含有SiTHH的硅氧烷和不饱和烃如α，ω-二烯的交联反应来制备的。 3BOND SiH硅氧烷首先与单烯基官能化聚醚部分反应。 然后在低分子量硅氧烷流体的存在下，通过α，ω-二烯交联。 制备具有聚醚基团的弹性体，即凝胶。 弹性体可以在剪切力下用低分子量硅氧烷流体溶胀，以提供均匀的硅胶。 硅胶糊在摩擦时具有优异的铺展性，并且在触变和剪切变稀中具有独特的流变性能。 硅胶糊可以容易地用水乳化以形成稳定的均匀乳液，而不使用表面活性剂以允许通常不混溶的材料变得紧密混合。
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公开(公告)号：US5880210A
公开(公告)日：1999-03-09
申请号：US829867
申请日：1997-04-01
摘要： Silicone gels are made by reacting an .tbd.Si--H containing polysiloxane with an alpha-olefin and an alpha, omega-diene. The reaction is conducted in the presence of a platinum catalyst and in the presence of a low molecular weight silicone oil. First, an .tbd.Si--H containing polysiloxane is grafted by long chain alkyl groups from the alpha-olefin onto the .tbd.Si--H containing polysiloxane, and then crosslinked with double bonds in the alpha, omega-diene, in the presence of the low molecular weight silicone oil. The formed silicone gel can then be crumbled into a silicone powder using mechanical force. When additional amounts of the low molecular weight silicone oil are added to the gel, and the silicone oil and the gel are subjected to shear force, a silicone paste can be formed.
摘要翻译： 硅氧烷凝胶是通过使含有SiTHH的聚硅氧烷与α-烯烃和α，ω-二烯反应制得的。 该反应在铂催化剂存在下和在低分子量硅油存在下进行。 首先，将含有SiONDTH的含SiTHH的聚硅氧烷通过长链烷基从α-烯烃接枝到含有3BOND Si-H的聚硅氧烷上，然后在α，ω-二烯的双键存在下，以低的 分子量硅油。 然后可以使用机械力将形成的硅胶凝胶粉碎成硅酮粉末。 当将另外量的低分子量硅油加入到凝胶中，并且硅油和凝胶受到剪切力时，可以形成硅氧烷糊。
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6.发明授权Thermally conductive grease and methods and devices in which said grease is used 有权导热油脂及使用所述润滑脂的方法和装置公开(公告)号：US07695817B2
公开(公告)日：2010-04-13
申请号：US10571956
申请日：2004-09-16
申请人： Zuchen Lin , Shizhong Zhang , Mark Fisher
发明人： Zuchen Lin , Shizhong Zhang , Mark Fisher
IPC分类号： B32B25/20
CPC分类号： C08K3/22 , C08K3/013 , C08K3/38 , C08K2003/2227 , C08K2003/2296 , C08K2003/382 , C08L83/04 , C09K5/14 , H01L23/3737 , H01L2224/16 , H01L2224/16225 , H01L2224/32225 , H01L2224/32245 , H01L2224/73204 , H01L2224/73253 , H01L2224/83192 , H01L2924/01004 , H01L2924/01019 , H01L2924/01079 , H01L2924/01322 , H01L2924/15311 , H01L2924/16152 , H01L2924/3011 , Y10T428/259 , Y10T428/31663 , H01L2924/00
摘要： A thermally conductive grease includes (A) a polyorganosiloxane having a viscosity less than 50 cSt (mm2/s) at 25° C. and (B) a thermally conductive filler. The thermally conductive grease is useful as a thermal interface material for electronic devices.
摘要翻译： 导热性油脂包含（A）在25℃下粘度小于50cSt（mm2 / s）的聚有机硅氧烷，（B）导热性填料。 导热油脂可用作电子设备的热界面材料。
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7.发明申请Thermally conductive grease and methods and devices in which said grease is used 有权导热油脂及使用所述润滑脂的方法和装置公开(公告)号：US20060292840A1
公开(公告)日：2006-12-28
申请号：US10571956
申请日：2004-09-16
申请人： Zuchen Lin , Shizhong Zhang , Mark Fisher
发明人： Zuchen Lin , Shizhong Zhang , Mark Fisher
CPC分类号： C08K3/22 , C08K3/013 , C08K3/38 , C08K2003/2227 , C08K2003/2296 , C08K2003/382 , C08L83/04 , C09K5/14 , H01L23/3737 , H01L2224/16 , H01L2224/16225 , H01L2224/32225 , H01L2224/32245 , H01L2224/73204 , H01L2224/73253 , H01L2224/83192 , H01L2924/01004 , H01L2924/01019 , H01L2924/01079 , H01L2924/01322 , H01L2924/15311 , H01L2924/16152 , H01L2924/3011 , Y10T428/259 , Y10T428/31663 , H01L2924/00
摘要： A thermally conductive grease includes (A) a polyorganosiloxane having a viscosity less than 50 cSt (mm2/s) at 25° C. and (B) a thermally conductive filler. The thermally conductive grease is useful as a thermal interface material for electronic devices.
摘要翻译： 导热油脂包括（A）在25℃下粘度小于50cSt（mm 2 / s）的聚有机硅氧烷，（B）导热填料。 导热油脂可用作电子设备的热界面材料。
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公开(公告)号：US6020409A
公开(公告)日：2000-02-01
申请号：US934180
申请日：1997-09-19
申请人： Khristopher Edward Alvarez , Roger Allen Frazer , Myron Timothy Maxson , Ann Walstrom Norris , Michael Raymond Strong , Beth Ann Witucki , Shizhong Zhang
发明人： Khristopher Edward Alvarez , Roger Allen Frazer , Myron Timothy Maxson , Ann Walstrom Norris , Michael Raymond Strong , Beth Ann Witucki , Shizhong Zhang
CPC分类号： H01L23/296 , C08L83/04 , C08G77/12 , C08G77/20 , H01L2924/0002 , Y10T428/31663
摘要： Polyorganosiloxane gels are prepared using compositions curable by a platinum catalyzed hydrosilation reaction that are characterized by the presence of a non-functional silicone fluid. The gel may contain additional components and may also be formulated into a multi-part system.
摘要翻译： 聚有机硅氧烷凝胶是使用可通过铂催化氢化硅烷化反应固化的组合物制备的，其特征在于存在非官能的硅氧烷流体。 凝胶可以含有另外的组分，也可以配制成多部分体系。
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公开(公告)号：US5929164A
公开(公告)日：1999-07-27
申请号：US964546
申请日：1997-11-05
申请人： Shizhong Zhang
发明人： Shizhong Zhang
IPC分类号： E02D3/12 , A61K8/00 , A61K8/72 , A61K8/89 , A61K8/891 , A61Q1/00 , A61Q1/04 , A61Q1/10 , A61Q1/12 , A61Q5/02 , A61Q5/10 , A61Q19/00 , C08G77/32 , C08G77/38 , C08G77/50 , C08K5/01 , C08L83/04 , C08L83/05 , C08L83/14 , H01B3/46
CPC分类号： A61Q19/00 , A61K8/895 , C08G77/32 , C08G77/50 , C08L83/04 , C08L83/14 , C08G77/045 , C08G77/12 , C08G77/20 , C08G77/442 , Y10S524/924
摘要： A method of thickening solvents involves reacting (A) an .tbd.Si--H containing polysiloxane with (B) an alpha, omegadiene; conducting the reaction in the presence of a platinum catalyst and (C) a solvent; continuing the reaction until a gel is formed by crosslinking and addition of .tbd.Si--H across double bonds in the alpha, omega-diene; adding additional solvent and a post cure quenching agent to the gel; and subjecting the solvent, the post cure quenching agent, and the gel to shear force until a paste is formed.
摘要翻译： 增稠溶剂的方法包括使（A）含有3BOND Si-H的聚硅氧烷与（B）α，ω-二烯; 在铂催化剂和（C）溶剂的存在下进行反应; 继续反应，直到通过交联并在α，ω-二烯中双键加入3BOND Si-H形成凝胶; 向凝胶中加入另外的溶剂和后固化淬灭剂; 并对溶剂，后固化淬灭剂和凝胶进行剪切力直到形成糊状物。
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10.发明授权公开(公告)号：US06359096B1
公开(公告)日：2002-03-19
申请号：US09425306
申请日：1999-10-25
IPC分类号： C08G7712
CPC分类号： C08G77/12 , C08G77/02 , C09D183/04
摘要： Soluble silicone resin compositions having good solution stability and a method for their preparation. The silicone resin comprises the reaction product of a mixture comprising (A) 15-70 mol % of a tetraalkoxysilane described by formula Si(OR1)4, where each R1 is an independently selected alkyl group comprising 1 to about 6 carbon atoms, (B) 12 to 60 mol % of a hydrosilane described by formula HSiX3, where each X is an independently selected hydrolyzable substituent, (C) 15 to 70 mole percent of an organotrialkoxysilane described by formula R2Si(OR3)3, where R2 is a hydrocarbon group comprising about 8 to 24 carbon atoms or a substituted hydrocarbon group comprising a hydrocarbon chain having about 8 to 24 carbon atoms and each R3 is an independently selected alkyl group comprising 1 to about 6 carbon atoms; in the presence of (D) water, (E) hydrolysis catalyst, and (F) organic solvent for the reaction product.
摘要翻译： 具有良好溶液稳定性的可溶性有机硅树脂组合物及其制备方法。 有机硅树脂包括由（A）15-70mol％的四烷氧基硅烷所组成的混合物的反应产物，每个R 1是独立选择的含有1至约6个碳原子的烷基，（B）12至60mol％ 由式X表示的氢硅烷，每个X是独立选择的可水解取代基，（C）15-70摩尔％的由通式R 2表示的有机三烷氧基硅烷是包含约8至24个碳原子的烃基或包含烃链的取代烃基， 约8至24个碳原子，并且每个R 3是独立选择的包含1至约6个碳原子的烷基; 在（D）水，（E）水解催化剂和（F）反应产物的有机溶剂的存在下。
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